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Cooperative study for micro crystal and cluster, and its growth process using the synchrotron radiation beam

Research Project

Project/Area Number 01045006
Research Category

Grant-in-Aid for international Scientific Research

Allocation TypeSingle-year Grants
SectionUniversity-to-University Cooperative Research
Research InstitutionUniversity of Tsukuba and State University of New York at Stony Brook

Principal Investigator

WAKATSUKI Masao  University of Tsukuba, Institute of materials science, 物質工学系, 教授 (50114153)

Co-Investigator(Kenkyū-buntansha) WEIDENR D. J.  State Univ. New York at Stony Brook, Dept. earth & space sciences, State Univ, Proffessor
VAUGHAN M. T  State Univ. New York at Stony Brook, Dept. earth & space sciences, State Univ, Professor
PARISE J. B.  State Univ. New York at Stony Brook, Dept. earth & space sciences, State Univ, Professor
YURIMOTO Hisayoshi  University of Tsukuba, Institute of geoscience, 地球科学系, 助手 (80191485)
NAKAI Izumi  University of Tsukuba, Institute of chemistry, 化学系, 講師 (90155648)
TAKANO Kaoru  University of Tsukuba, Institute of materials science, 物質工学系, 助教授 (60133005)
KURITA Kei  University of Tsukuba, Institute of geoscience, 地球科学系, 助教授 (00111451)
FUKUTANI Hirohito  University of Tsukuba, Institute of physics, 物理学系, 教授 (40011580)
OHSHIMA Kenichi  University of Tsukuba, Institute of applied physics, 物理工学系, 助教授 (70109271)
AOKI Sadao  University of Tsukuba, Institute of applied physics, 物理工学系, 助教授 (50016804)
FUJII Yasuhiko  University of Tsukuba, Institute of materials science, 物質工学系, 教授 (00013524)
SUENO Shigeho  University of Tsukuba, Institute of geoscience, 地球科学系, 教授 (30110513)
PARISE John  State University of New York―SB, Dept. Ear, Assistan P
WEIDNER Dona  State University of New York―SB, Dept. Ear, Professor
CHU Benjamin  State University of New York―SB, Dept. Che, Professor
浜谷 望  筑波大学, 物質工学系, 講師 (70156420)
Project Period (FY) 1989 – 1991
Project Status Completed (Fiscal Year 1991)
Budget Amount *help
¥6,000,000 (Direct Cost: ¥6,000,000)
Fiscal Year 1991: ¥2,000,000 (Direct Cost: ¥2,000,000)
Fiscal Year 1990: ¥2,000,000 (Direct Cost: ¥2,000,000)
Fiscal Year 1989: ¥2,000,000 (Direct Cost: ¥2,000,000)
KeywordsSynchrotron radiation / Crystal synthesis / X-ray diffraction / High pressure experiment / Phase transition / Multiple thin film / Earth's deep material / Na-matal / 地球深部物質 / 微細粒子 / 結晶成長 / 高圧力 / 地球深部 / 物質合成
Research Abstract

University of Tsukuba (UT) and State University of New York at Stony Brook (SB) have advanced several cooperative researches in connection with the field of growth mechanism of micro particles and micro crystals for both experimental and theoretical view points. Last three years, both universities have exchanged two to four researchers every year in the period of several days to one month for the cooperative researches, lectures, and discussion. Main mutually interested research fields are as follows :
(a) High temperature-high pressure material research : This research is popular for both universities in the field of geoscience. Experiments of crystal synthesis under static high pressure condition were carried out mostly in SB (Liebermann, Weidner and Kurita), and in situ observations of high pressure synthesis using SOR beam were performed in KEK, Tsukuba (Kurita, Wakatsuki, Liebermann, Weidner and Vaughan).
(b) Single crystal structure analysis and chemical composition analysis : Hydr … More ogen and trace elements analysis were carried out (Yurimoto, Sueno and Nakai) in UT for the mineral specimens synthesized in SB.
(c) Small angle scattering : Application of CCD detector on the scattering experiments were discussed and cooperatively studies (Chu, Sueno).
(d) Micro crystal analysis : Techniques on the sub-micron size single crystal structure analysis were studied. Especially, techniques for making a micro-beam and method for holding a specimen were the object of mutual interest.
(e) EXAFS : EXAFS spectra analysis using SOR beam were carried out in NSLS for the metal elements in a amorphous material (Parise and Nakai).
(f) X-ray microscope : Development of X-ray microscope continuing using SOR beam in NSLS and KEK (Aoki and Kirtz),
(g) Phase transition and X-ray diffuse scattering : Martensite transition on Na and other metal elements were studied cooperatively by Stephens and Ohsima.
(h) Lecture : Exchange researchers most of time had chances to have lectures in both universities. Most fruitful effects of this exchange program is the establishment of the mutual confidence and the friendship. Less

Report

(3 results)
  • 1991 Annual Research Report   Final Research Report Summary
  • 1990 Annual Research Report
  • Research Products

    (43 results)

All Other

All Publications (43 results)

  • [Publications] 若槻 雅男: "An optical high pressure cell with spherical sapphire anvils" Rev.Sci.Instrum.62. 1576-1580 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] 末野 重穂: "Impurities dislocation diffusion in singleーcrystal MgO" Mater.Sci.Eng.B. (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] 藤井 保彦: "Systematics in the modulated phases of 〔N(CH_3)_4〕_2MnCl_4" J.Phys.:Condens.Matter. 3. 3387-3391 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] 大嶋 建一: "Xーray diffraction study of Fe/MgO multilayered films with an enhanced magnetization" J.Phys.:Condens.Matter. 3. 5921-5927 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Weidner,D.J.: "Phase transition and thermal expansion of MgSiO perovskite:Implications for the compositon of the Earth's lower mantle" Science. 251. 410-413 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Vaughan,M.T.: "Large volume high pressure research using the wiggler port at NSLS" High Pressure Research. (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Wakatsuki, Masao: "An optical high pressure cell with spherical sapphire anvils" Rev. Sci. Instrum.62. 1576-1580 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Sueno, Shigeho: "Impurities dislocation diffusion in single-crystal MgO" Mater. Sci. Eng. B. (1992)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Fujii, Yasuhiko: "Systematics in the modulated phases of N (CH_3) _4 _2 MnCl_4" J. Phys. : Condens. Matter. 3. 3387-3391 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Ohshima, Kenichi: "X-ray diffraction study of Fe/MgO multilayered films with an enhanced magnetization" J. Phys. : Condens. Matter. 3. 5921-5927 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Weidner, D. J.: "Phase transition and thermal expansion of MgSiO_3 perovskite : Implications for the composition of the Earth's lower mantle" Science. 251. 410-413 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] 若槻 雅男: "An optical high pressure cell with spherical sapphire anvils" Rev.Sci.Instrum.62. 1576-1580 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] 末野 重穂: "Impurities dislocation diffusion in singleーcrystal MgO" Mater.Sci.Eng.B (in press). (1992)

    • Related Report
      1991 Annual Research Report
  • [Publications] 藤井 保彦: "Systematics in the modulated phases of 〔N(CH_3)_4〕_2MnCl_4" J.Phys.:Condens.Matter. 3. 3387-3391 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] 大嶋 建一: "Xーray diffraction study of Fe/MgO multilayered films with an enhanced magnetization" J.Phys.:Condens.Matter. 3. 5921-5927 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] Weidner,D.J.: "Phase transition and thermal expansion of MgSiO_3 perovskite: Implications for the compositon of the Earth's lower mantle" Science. 251. 410-413 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] Vaughan,M.T.: "Large volume high pressure research using the wiggler port an NSLS" High Pressure Research. (1992)

    • Related Report
      1991 Annual Research Report
  • [Publications] Masao Wakatsuki: "Detection of impurities in diamond grown in the metallic solvent by xーray fluorescence method using SR." Proc.2nd International Conf.on New Diamond Science and Technology,Washington,1990(Special issue of J.Materials Research). (1991)

    • Related Report
      1990 Annual Research Report
  • [Publications] Kaoru J.Takano: "An optical high pressure cell with spherical sapphire anvils." Rev.Sci.Instrum.62. (1991)

    • Related Report
      1990 Annual Research Report
  • [Publications] Kaoru J.Takano: "New high pressure phases of carbon." Japan.J.Appl.Phys.30. (1991)

    • Related Report
      1990 Annual Research Report
  • [Publications] H.Yurimoto: "Quantitative SIMS analysis of GSJ rock reference samples." Geochem.Cosmochem.J.23. 215-235 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] C.K.Shearer: "Ion microprobe studies of trace elements in Apollo 14 volcanic glass beads:Comparison to Apoll 14 mare basalts and petrogenesis of picritic magas." Geochimica et Cosmochimica Acta. 54. 851-867 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] S.Sueno: "A SIMS study on lattice and dislocation diffusion in MgO." Proc.2nd Eurasia Conf.on on Chemistry,Seoul.171-172 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] H.Yurimoto: "Quantitative nickel analysis in GSJ standard rock using ionmass spectrometry." Geostandards Newsletter. (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] 末野 重穂: "SIMSによるセラミックスの微量分析ー最近の進歩ー" 工業と製品. 72. 147-152 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] N.Metoki: "Timeーresolved xーray diffraction study of oneーdimensional nucleation and growth in the firstーorder transition." Phys.Rev.Letters. 64. 657-660 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] Y.Ohishi: "Structural instability of PbSe/SnSe superlattices under pressure." High Pressure Research. 4. 300-302 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] H.Fujihisa: "Pressureーinduced molecular dissociation in iodine at low temperatures." High Pressure Research. 4. 330-332 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] S.Hayakawa: "Xーray microanalysis with energy tunable synchrotron xーrays." Nuclear Instruments and Methods in Physics Research. B49. 555-560 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] K.Ninomiya: "Xーray photoelectron spectroscopy using a focused 300μmーdiameter xーray beam." Jpn.J.Appl.Phys.29. 974-979 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] K.Ninomiya: "Xーray photoelectron spectroscopy of micrometerーsize surface area using synchrotron radiation." Jpn.J.Appl.Phys.29. L1026-L1028 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] Y.Kuroiwa: "Xーrayーdiffraction study of inーplane and interlayer correlations in layered compounds Ag_xTiS_2." Phys.Rev.B. B42. 11591-11597 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] 黒岩 芳弘: "層間化合物Ag_xTis_2の次元間相転移" 日本結晶学会誌. 33. 1-6 (1991)

    • Related Report
      1990 Annual Research Report
  • [Publications] N.Toyoshima: "A simple device for mounting a vacuum chamber on a fourーcircle diffractometer with central chiーcircle." to be published in J.Appl.Cryst.

    • Related Report
      1990 Annual Research Report
  • [Publications] K.Yagi: "Angle resolved photoemission study of Pd(110)surface." Surf.Sci.231. 397-403 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] H.Fukutani: "Reflection and photoemission study of neutron irradiated graphite." J.Phys.Soc.Jpn.59. 3089-3093 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] T.Koide: "Optical study of stoichiometry dependent electronic structure of TiC_x,VC_x,and NbC_x." Phys.Rev.B42. 4979-4995 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] Izumi Nakai: "Synchrotron xーray Rietvert analysis of αーhafnium phosphate." Analytical Sci.6. 689-693 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] Izumi Nakai: "Singleーcrystal xーray structure analysis of new oxideーsuperconductor Bi_2(Sr_<1ーx>Ln_x)_2(Gd_<1ーy>Ce_y)_2Cu_2O_<10> _<+z>." Jpn.J.Appl.Phys.29. L572-L575 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] R.Miyawaki: "Crystal structure of rare earth minerals.3rd Supplement." 希土類. 17. 1-10 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] J.B.Parise: "Crystal structure and thermal expansion of(Mg,Fe)SiO_3 perovskite." Geophys.Res.Letters.17. (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] N.Hamaya: "High Pressure Research" Search for polytypic structures of gadolinium., 375-377 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] 丁 立業: "成都科学技術大学学報" 金鋼石合成用介質的伝圧効果研究, 41-46 (1990)

    • Related Report
      1990 Annual Research Report

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Published: 1989-04-01   Modified: 2016-04-21  

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