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Development of scanning tunneling microscope for materials growth front observations on an atomic scale

Research Project

Project/Area Number 01850001
Research Category

Grant-in-Aid for Developmental Scientific Research

Allocation TypeSingle-year Grants
Research Field Applied materials
Research InstitutionThe University of Tokyo

Principal Investigator

SHIRAKI Yasuhiro  The University of Tokyo, Research Center for Advanced Science and Technology Professor, 先端科学技術研究センター, 教授 (00206286)

Co-Investigator(Kenkyū-buntansha) KATAYAMA Yoshifumi  Optoelectronic Research Laboratory R&D director, つくば研究所, 研究開発部長
FUKATSU Susumu  The University of Tokyo Research Center for Advanced Science and Technology Assi, 先端科学技術研究センター, 助手 (60199164)
UOZUMI Kiyohiko  Aoyama-gakuin University Department of Science and Technology Professor, 理工学部, 教授 (20011124)
Project Period (FY) 1989 – 1991
Project Status Completed (Fiscal Year 1991)
Budget Amount *help
¥11,200,000 (Direct Cost: ¥11,200,000)
Fiscal Year 1991: ¥1,100,000 (Direct Cost: ¥1,100,000)
Fiscal Year 1990: ¥2,300,000 (Direct Cost: ¥2,300,000)
Fiscal Year 1989: ¥7,800,000 (Direct Cost: ¥7,800,000)
Keywordsepitaxial growth / surface structure / scanning tunneling microscopy (STM) / kinetic phase / Ge islanding / mechanism of interfacial mixing / Si / Ge heterostructure / atomic details on solid surfaces / エピタキシャル成長 / 5×5構造 / 選択的吸着 / 超高真空 / モリブデンブル-ブロンズ / Si(111)、Si(100) / アンチモン(Sb) / 原子層ド-ピング / 半導体清浄表面 / 高速トンネル分光 / 慣性式移動方式
Research Abstract

A new class of scanning tunneling microscopy (STM) was developed, which has a potential of probing atomic details on solid surfaces during the epitaxial growth. Two types of STM were constructed. The first is truly compact and the coarse positioning system consists of a novel inertia "walker" driven by shear mode piezoelectric elements. The second system was even rigid but truly compact and the coarse positioning was basically mechanically driven. Mechanical stability and thermal drift were appreciably improved and the vibronic immunity was further improved by introducing a spring suspension along with eddy current dampers. Both systems were shown to be readily fitted onto a conventional material growth facility.
Initial check of the system was satisfactory with respect to the ability of the new STM to probe the atomic detail to a subnanometer resolution. Atomic structures of graphite, Au deposited on mica, and cleaved K_<0.3>MoO_3 were observed. Subsequently, the STM was introduced int … More o UHV environment with a newly developed sample transfer system and materials deposition facilities. Unexpectedly, It was found that the sample quench mechanism was not necessary. Rather a mere contact with the sample transfer fork was sufficient to quench a kinetic phase of the smample.
Finally, we investigated the initial stage of epitaxial growth of Ge on Si (111) since Si/Ge/Si growth are of primary importance while little is studied by STM. Major objective is to find out the mechanism of interfacial mixing in the context of surface structure change upon deposition which is pronounced in Si/Ge heterostructural systems when grown by deposition. We found that the solid Ge islanding on terrace regions dictates the local topography leading a rugged Si/Ge interface. We also found that a kinetic phase of 5x5 reconstruction as observed in electron diffraction is scattered and manifest itself on higher terraces of Ge islands.
It is expected that the present results would be extended to be Put into practice in the near future. Less

Report

(4 results)
  • 1991 Annual Research Report   Final Research Report Summary
  • 1990 Annual Research Report
  • 1989 Annual Research Report
  • Research Products

    (24 results)

All Other

All Publications (24 results)

  • [Publications] S.Fukatsu: "Self-limitation in the surface segregation of Ge atoms during Si molecular beam epitaxial growth" Applied Physics Letters. 59. 2103-2105 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] K.Fujita: "Involvement of the topmost Ge layer in the Ge surface segregation during Si/Ge heterostructure formation" Applied Physics Letters. 59. 2240-2241 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] S.Fukatsu: "One-dimensional adsorption of Ge atoms at step-edges of Si(111)" Applied Physics Letters.

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] S.Fukatsu: "Spectral blue-shift of photoluminescnece in strained-layer SiGe quantum well structures" Applied Physics Letters.

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] S.Fukatsu: "Novel micro-positioning device for tunneling microscopy" Review of Scientific Instruments.

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] S.Fukatsu: "Surface structure of cleaved K_<0.3>MoO_3" Surface Science.

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] S. Fukatsu, K. Fujita, H. Yaguchi, Y. Shiraki, and R. Ito: "Self-limitation in the surface segregation of Ge atoms during Si molecular beam epitaxial growth" Appl. Phys. Lett.59. 2103-2105 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] K. Fujita, S. Fukatsu, H. Yaguchi, Y. Shiraki, and R. Ito: "Involvment of the topmost Ge layer in the Ge surface segregation during Si/Ge heterostructure formation" Appl. Phys. Lett.59. 2240-2241 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] S. Fukatsu, H. Yoshida, A. Fujiwara, Y. Takahashi, Y. Shiraki, and R. Ito: "Spectral blue-shift of photoluminescnece in strained-layer SiGe quantum well structures" Appl. Phys. Lett.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] S. Fukatsu, and Y. Shiraki: "One-dimensional adsorption of Ge atoms at the step-edges of Si (111)" Appl. Phys. Lett.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] S. Fukatsu, and Y. Shiraki: "Novel micro-positioning device for tunneling microscopy" Rev. Sci. Instrum.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] S. Fukatsu, and Y. Shiraki: "Surface structure of cleaved K_<0.3>MoO_3" Surf. Sci.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] S.Fukatsu: "Self-limitation in the surface segregation of Ge atoms during Si molecular beam epitaxial growth" Applied Physics Letters. 59. 2103-2105 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] K.Fujita: "Involvement of the topmost Ge layer in the Ge surface segregation during Si/Ge heterostructure formation" Applied Physics Letters. 59. 2240-2241 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] S.Fukatsu: "One-dimensional adsorption of Ge atoms at step-edges of Si(111)" Applied Physics Letters.

    • Related Report
      1991 Annual Research Report
  • [Publications] S.Fukatsu: "Spectral blue-shift of photoluminescnece in strained-layer SiGe quantum well structures" Applied Physics Letters.

    • Related Report
      1991 Annual Research Report
  • [Publications] S.Fukatsu: "Novel micro-positioning device for tunneling microscopy" Review of Scientific Instruments.

    • Related Report
      1991 Annual Research Report
  • [Publications] S.Fukatsu: "Surface structure of cleaved K0.3MoO3" Surface Science.

    • Related Report
      1991 Annual Research Report
  • [Publications] S.Fukatsu,H.Nakagawa,Y.Shiraki,and R.Ito: "A Simple Micropositioning Device for UHVーSTM"

    • Related Report
      1990 Annual Research Report
  • [Publications] S.Fukatsu,H.Nakagawa,Y.Shiraki,and R.Ito: "Atomic Details on the Cleaued Ko,3McO_3 studied by STM"

    • Related Report
      1990 Annual Research Report
  • [Publications] S.Fukatsu,S.Kubo,Y.Shiraki,and R.Ito: "Redistribution of Sb in an AtomicーLagerーDoped Silicon" Appl.Phys.Lett.58. (1991)

    • Related Report
      1990 Annual Research Report
  • [Publications] S.Fukatsu,S.Kubo,Y.Shiraki,and R.Ito: "Redistribution of deltaーdoped Sb inSi" J.Crystal Growth. (1991)

    • Related Report
      1990 Annual Research Report
  • [Publications] K.Fujita,S.Fukatsu,T.Igarashi,H.Yaguchi ,Y.Shiraki,and R.Ito: "Redization of Abrupt Interfaces in SilC_<3e> Superlaffices by Suppressing Cx Surfuce Segregation with Submonolayer of Sb" Jpn.J.Appl.Phys.29. L1981-L1983 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] S.Fukatsu: "A reliable positioning device for UHV-Scanning tunneling microscopy"

    • Related Report
      1989 Annual Research Report

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Published: 1989-04-01   Modified: 2019-02-15  

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