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Superplastic Forming of Ceramics

Research Project

Project/Area Number 01850154
Research Category

Grant-in-Aid for Developmental Scientific Research

Allocation TypeSingle-year Grants
Research Field 金属加工(含鋳造)
Research InstitutionThe university of Tokyo

Principal Investigator

SAKUMA Taketo  Professor, University of Tokyo, 工学部, 教授 (50005500)

Co-Investigator(Kenkyū-buntansha) KIKUCHI Norihumi  Mitsubishi Material Co. Ltd., 中央研究所, 室長
YOSHIZAWA Yu-ichi  Research Assistant, University of Tokyo, 工学部, 助手 (00200973)
菊地 則文  三菱金属(株), 中央研究所, 室長
Project Period (FY) 1989 – 1991
Project Status Completed (Fiscal Year 1991)
Budget Amount *help
¥10,400,000 (Direct Cost: ¥10,400,000)
Fiscal Year 1991: ¥1,300,000 (Direct Cost: ¥1,300,000)
Fiscal Year 1990: ¥1,500,000 (Direct Cost: ¥1,500,000)
Fiscal Year 1989: ¥7,600,000 (Direct Cost: ¥7,600,000)
Keywordsalumina / zirconia / Al_2O_3-ZrO_2 / superplasticity / grain growth / Al_2O_3-ZrO_2 / Al_2O_3ーZrO_2(アルミナ-ジルコニア)
Research Abstract

The results obtained are summarized as follows,
(1) The high-temperature deformability in TZP is improved by an addition of small amount of grain boundary glass phase. The addition of 5 wt% lithium-aluminosilicate glass results in about 200゚C decrease of superplastically deformed temperature. TZP containing this glass deforms superplastically at 1100゚C.
(2) The marked grain growth and cavitation during high-temperature deformation retards the tensile ductility of high-purity Al_2O_3. The MgO addition effectively suppresses the grain growth of Al_2O_3 and consequently improves the ductility. The maximum elongation obtained is 70% at 1400゚C.
(3) The high-temperature flow stress in Al_2O_3-ZrO_2 depends markedly on zirconia content. A sharp peak value is obtained in Al_2O_3-2wt%ZrO_2. The composition dependence of flow stress can qualitatively be explained by assuming that the grain boundary sliding is much difficult along Al_2O_3/ZrO_2 boundary than other boundaries.

Report

(4 results)
  • 1991 Annual Research Report   Final Research Report Summary
  • 1990 Annual Research Report
  • 1989 Annual Research Report
  • Research Products

    (33 results)

All Other

All Publications (33 results)

  • [Publications] Y.Yoshizawa and T.Sakuma: "Role of grain boundary glass phase on the superplastic detormation of tetragonal airconia poly cry stal" J.A.Ceram.Soc.,. 73. 3069-3073 (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Y.Yoshizawa and T.Sakuma: "High-temperature deformation and grain growth in fine-grained zirconia" Eng.Fract.Mech.,. 40. 847-854 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] K.Okada,Y.Yoshizawa and T.Sakuma: "High-temperature deformation and microstructure in alumina-rich Al_2O_3-Z_rO_2" Proc.1st Int.Symp.on the Science of Engineering Ceramics. 251-256 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] K.Okada,Y.Yoshizawa and T.Sakuma: "Grain-size distribution in Al_2O_3-Z_rO_2 generated by annealing at high temperatures" J.Am.Ceram.Soc.,. 74. 2820-2823 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Y.Yoshizawa and T.Sakuma: "Straln-enhanced grain grouth in tetragonal zirconia polycry stal during superplastic deformation" Super plasticity in Advanced Materials,Ed.by S.Hori et al.,. 251-256 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Y.Yoshizawa and T.Sakuma: "Grain grouth acceleration during high-temperature deformation in high-purity alumina" Mater.Sci.Eng.,. A149. 59-64 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] 佐久間 健人: "セラミック材料学" 海文堂, 240 (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Y. Yoshizawa and T. Sakuma: "Evolution of microstructure and grain growth in ZrO_2-Y_2O_3 alloys" ISIJ International. 29. 746-752 (1989)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Y. Yoshizawa and T. Sakuma: "Effect of grain boundary glassy phase on superplastic deformation in ZrO_2-2.5 mol% Y_2O_3 alloy" Proc. 1st Jpn. Int. SAMPE Symp., Ed. by N. Igata et al.272-277 (1989)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] T. Sakuma, Y. Yoshizawa and Y. Zhou: "Intercritical annealing in the system ZrO_2-Y_2O_3" Proc. 1st Jpn. Int. SAMPE Symp., Ed. by N. Igata et al.815-820 (1989)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Y. Yoshizawa and T. Sakuma: "The role of grain boundary glass phase on the superplastic deformation of tetragonal zirconia polycrystals" J. Am. Ceram. Soc.73. 3069-3073 (1990)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Y. Yoshizawa and T. Sakuma: "High-Temperature Deformation and Grain Growth in Fine-Grained Zirconia" Eng. Fract. Mech.40. 847-854 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] K. Okada, Y. Yoshizawa and T. Sakuma: "High-Temperature Deformation in Alumina-Rich Al_2O_3-ZrO_2" Proc. 1st Int. Symp. on the Science of Engineering Ceramics, Ed. by S. Kimura and K. Niihara, The Ceramics Soc. Jpn. 251-256 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] K. Okada, Y. Yoshizawa and T. Sakuma: "Grain Size Distribution in Al_2O_3-ZrO_2 Generated by High-Temperature Annealing" J. Am. Ceram. Soc.74. 2820-2823 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] K. Okada, Y. Yoshizawa and T. Sakuma: "High-Temperature Deformation in Al_2O_3-ZrO_2" Superplasticity in Advanced Materials, ed. by S. Hori et al., The Jpn. Soc. for Res. on Superplasticity. 227-232 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Y. Yoshizawa and t. Sakuma: "The Strain Enhanced Grain Growth in Tetragonal Zirconia Polycrystal During Superplastic Deformation" Superplasticity in Advanced Materials, ed. by S. Hori et al., The Jpn. Soc. for Res. on Superplasticity. 251-256 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Y. Yoshizawa and T. Sakuma: "The Grain Growth Acceleration During High-Temperature Deformation in High-Purity Alumina" Mater. Sci. Eng.A149. 59-64 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] Y.Yoshizawa and T.Sakuma: "High-Temperature Deformation and Grain Growth in Fine-Grained Zirconia" Eng.Fract.Mech.,. 40. 847-854 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] K.Okada,Y.Yoshizawa and T.Sakuma: "High-Temperature Deformation and Microstmcture in Alumina-Rich Al_2O_3-ZrO_2" Proc.1st Int.Symp.on the Science of Engineering Ceramics. 251-256 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] K.Okada,Y.Yoshizawa and T.Sakuma: "Grain-Size Distribution in Al_2O_3-ZrO_2 Generated by Annealing at High Temperatures" J.Am.Ceram.Soc.,. 74. 2820-2823 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] Y.Yoshizawa and T.Sakuma: "Strain-Enhanced Grain Growth in Tetragoual Zirconia Polycrystal during Superplastic Deformatiom" Superplasticity in Advanced Materials,Ed.by S.Hori et al.,. 251-256 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] K.Okada,Y.Yoshizawa and T.Sakuma: "High-Temperature Detormation in Al_2O_3-ZrO_2" Superplaticity in Advanced Materials,Ed.by S.Hori et al.,. 227-232 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] Y.Yoshizawa and T.Sakuma: "Grain Growth Accelenation duriug High-Temperature Deformation in High-Purity Alumina" Mater.Sci.Eug.,. A149. 59-64 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] Y.Yoshizawa,T.Sakuma: "Role of grainーboundary glass Phase on the superplastic deformation of tetragonal zirconia polycrystal" J.Am.Ceram.Soc.,. 73. 3069-3073 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] 佐久間 健人,吉澤 友一: "正方晶ジルコニア多結晶の超塑性変形と粒界ガラス相" 東京大学工学部紀要. A28. 36-37 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] Y.Yoshizawa,T.Sakuma: "Highーtemperature deformation and grain growth in fineーgrained zirconia"

    • Related Report
      1990 Annual Research Report
  • [Publications] K.Okada,Y.Yoshizawa T.Sakuma: "Grainーsize distribution in Al_2O_3ーZrO_2 generated by annealing at high temperatures"

    • Related Report
      1990 Annual Research Report
  • [Publications] 佐久間 健人: "セラミック材科学" 海文堂, 240 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] 佐久間健人,吉澤友一: "ZrO_2-Y_2O_3の微細組織と結晶粒成長" ジルコニアセラミックス. 10. 95-108 (1989)

    • Related Report
      1989 Annual Research Report
  • [Publications] Y.Yoshizawa,T.Sakuma: "Evolution of microstructure and grain growth in ZrO_2-Y_2O_3 alloys" ISIJ International. 29. 746-752 (1989)

    • Related Report
      1989 Annual Research Report
  • [Publications] T.Sakuma,Y.Yoshizawa,Y.Zhou: "Intercritical annealing in the system ZrO_2-Y_2O_3" Proc.1st SAMPE Symposium ed.by Igata et al.815-820 (1989)

    • Related Report
      1989 Annual Research Report
  • [Publications] H.Harada,T.Sakuma: "Final-stage densification and grain growth in ZrO_2-Y_2O_3 alloys" Proc.1st SAMPE Symposium ed.by I gata et al.324-329 (1989)

    • Related Report
      1989 Annual Research Report
  • [Publications] Y.Yoshizawa,T.Sakuma: "Effect of grain boundary glassy phase on superplastic deformation in ZrO_2-2.5mol% Y_2O_3 alloy" Proc.1st SAMPE Symposium ed.by Igata et al.272-277 (1989)

    • Related Report
      1989 Annual Research Report

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Published: 1989-04-01   Modified: 2019-02-15  

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