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Development of Microstructure-controlled L1_2-type High Temperature Intermetallics

Research Project

Project/Area Number 01850166
Research Category

Grant-in-Aid for Developmental Scientific Research (B).

Allocation TypeSingle-year Grants
Research Field 金属材料(含表面処理・腐食防食)
Research InstitutionKyushu University

Principal Investigator

NEMOTO Minoru  Kyushu Univ., Fac. Eng., Professor, 工学部, 教授 (90005265)

Co-Investigator(Kenkyū-buntansha) SANO Takeshi  Kyushu Univ., Fac Eng., Research Associate, 工学部, 助手 (70037810)
HORITA Zenji  Kyushu Univ., Fac. Eng., Associate Professor, 工学部, 助教授 (20173643)
MIURA Yasuhiro  Kyushu Univ., Fac. Eng., Professor, 工学部, 教授 (80037879)
Project Period (FY) 1989 – 1990
Project Status Completed (Fiscal Year 1990)
Budget Amount *help
¥10,000,000 (Direct Cost: ¥10,000,000)
Fiscal Year 1990: ¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 1989: ¥9,400,000 (Direct Cost: ¥9,400,000)
KeywordsIntermetallic compound / Nickl aluminide / Precipitation strengthening / High temperature strength / Single crystal / Transmission electron microscopy / Super dislocation / Carbide / ニッケルーアルミニウムーチタン合金 / 金属間化合物単結晶 / 組織制御 / 超耐熱材料 / 温度依存性 / 方位依存性 / 炭素添加化合物 / 析出炭化物 / ニッケル-アルミニウム-チタン合金 / 時効析出硬化 / APBエネルギ- / 析出硬化モデル
Research Abstract

Experimental studies were made on the microstructure control of gamma'-Ni_3A1 based intermetallics mainly by means of transmission electron microscopy. Results are as follows.
1. Precipitation of disordered gamma phase in an Ll_2 ordered gamma'-Ni_3 (Al, Ti) phase. A uniform solid solution of gamma'-Ll_2 ordered phase supersaturated with Ni can be obtained annealing in a suitable temperature range.
2. Deformation induced microstructure of Ll_2 ordered gamma'-Ni_3 (Al, Ti) single crystals containing fine dispersion of disordered gamma precipitates. Superlattice dislocations dissociate into fourfold Schockley partial dislocations in a uniform supersaturatred solid solution of the gma' phase.
3. Hardening mechanisms in a gamma'-Ll_2 ordered phase containing disordered gamma precipitates. Extra work necessary to pull out the dislocations from the precipitate is dependent on the difference in antiphase boundary energy between the matrix and the precipitates.
4. Temperature dependence of the yie … More ld stress in gamma'-Ll_2 ordered Ni_3 (Al, Ti) single crystals containing disordered gamma precipitates. The strength of gamma'-Ni_3 (Al, Ti) increases over the temperature range of experiment by the precipitation of fine gamma particles.
5. Orientation dependence of the yield stress in gamma'-Ll_2 ordered Ni_3 (Al, Ti) single crystals containing disordered gamma precipitates. The critical resolved shear stress for (111) [101] slip decreases with increasing temperature in the temperature range where (111) slip operates.
6. Dislocation structures in high temperature deformed Ni_3 (Al, Ti) single crystals containing disordered gamma precipitates. The super dislovations are strongly attracted to the disordered particles and dissociate on the (111) plane in the matrix.
7. Precipitation in Ll_2-Ordered Ni-Al-Cr alloys. By aging at temperatures around 1073 K after solution treatment at 1423 K, fine polyhedral precipitates appear firstly on the dislocations and then in the matrix. The selected area electron diffraction studies revealed that these particles are a M_<23>C_6 type carbide. Less

Report

(3 results)
  • 1990 Annual Research Report   Final Research Report Summary
  • 1989 Annual Research Report
  • Research Products

    (27 results)

All Other

All Publications (27 results)

  • [Publications] 田 文懐: "γ'Ni_3(Al,Ti)L1_2型規則相中への不規則γ相の析出" 日本金属学会誌. 53. 1013-1021 (1989)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] 田 文懐: "微細に分散した不規則γ相を含むγ'ーNi_3(Al,Ti)L1_2型規則相単結晶の変形組織" 日本金属学会誌. 53. 1022-1028 (1989)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] 田 文懐: "不規則γ相の析出によるγ'ーL1_2の強化機構" 日本金属学会誌. 53. 1029-1034 (1989)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] 田 文懐: "不規則γ析出相を含むγ'ーNi_3(Al,Ti)L1_2型規則相単結晶の強度の温度依存性" 日本金属学会誌. 54. 276-284 (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] 田 文懐: "不則規γ析出相を含むγ'ーNi_3(Al,Ti)L1_2型規則相単結晶の強度の方位依存性" 日本金属学会誌. 54. 285-291 (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] NEMOTO,Minoru: "Coherent Precipitation Strengthening by/in L1_2ーOrdered Phases" La Revue de Physique Applique^^´e.

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] 根本 実: "γ'ーNi_3Al系金属間化合物の析出強化" 日本金属学会会報. 30. 19-23 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] TIAN,Wen Huai: "Dislocation Structures in High Temperature Deformed Ni_3(Al,Ti) Single Crystals Containing Disordered γ Precipitates" Sixth JIM Int.Symp.on Intermetallic Compounds,.

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] HAN,ChangーSuck: "Precipitation in L1_2ーOrdered NiーAlーCr Alloys" Sixth JIM Int.Symp.on intermetallic Compound,.

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] TIAN, Wen Huai: "Precipitation of Disordered gamma Phase in an Ll_2 Ordered gamma '-Ni_3(Al, Ti) Phase" J. Japan Inst. Metals. Vol. 53, No. 10. 1013-1021 (1989)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] TIAN, Wen Huai: "Deformation Induced Microstructure of Ll_2 Ordered gamma '-Ni_3(Al, Ti) Single Crystals Containing Fine Dispersion of Disordered gamma Precipitates" J. Japan Inst. Metals. Vol. 53, No. 10. 1022-1028 (1989)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] TIAN, Wen Huai: "Hardening Mechanisms in a gamma '- Ll_2 Ordered Phase Containing Disordered gamma Precipitates" J. Japan Inst. Metals. Vol. 53, No. 10. 1029-1034 (1989)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] TIAN, Wen Huai: "Temperature Dependence of the Yield Stress in gamma '- Ll_2 Ordered Ni_3(Al, Ti) Single Crystals Containing Disordered gamma Precipitates" J. Japan Inst. Metals. Vol. 54, No. 3. 276-284 (1990)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] TIAN, Wen Huai: "Orientation Dependence of the Yield Stress in gamma '- Ll_2 Ordered Nl_3(Al, Ti) Single Crystals Containing Disordered gamma Precipitates" J. Japan Inst. Metals. Vol. 54, No. 3. 285-291 (1990)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] NEMOTO, Minoru: "Coherent Precipitation Strengthening by/in Ll_2-Ordered Phases" La Revue de Physique Appliquee.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] NEMOTO, Minoru: "Precipitation Strengthening of gamma '-Ni_3Al Based Intermetallics" Bull. Japan Inst. Metals. Vol. 30, No. 1. 19-23 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] TIAN, Wen Huai: "Dislocation Structures in High Temperature Deformed Ni_3(Al, Ti) Single Crystals Containing Disordered gamma Precipitates" Sixth JIM Int. Symp. on Intermetallic Compounds.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] HAN, Chang-Suck: "Precipitation in Ll_2-Ordered Ni-Al-Cr Alloys" Sixth JIM Int. Symp. on Intermetallic Compounds.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] 田 文懐: "不規則γ析出相を含むγ'-Ni_3(Al,Ti)L1_2型規則相単結晶の強度の温度依存性" 日本金属学会誌. 54. 276-284 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] 田 文懐: "不規則γ析出相を含むγ'-Ni_3(Al,Ti)L1_2型規則相単結晶の強度の方位依存性" 日本金属学会誌. 54. 285-291 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] M.Nemoto: "Coherent Precipitation Strengthening by/in L1_2ーOrdered Phases" La Revue de Physique Applique^^´e,.

    • Related Report
      1990 Annual Research Report
  • [Publications] 根本 実: "γ'-Ni_3Al系金属間化合物の析出強化" 日本金属学会会報. 30. 19-23 (1991)

    • Related Report
      1990 Annual Research Report
  • [Publications] W.H.Tian: "Dislocation Structures in High Temperature Deformed Ni_3(Al,Ti)Single Crystals Containing Disordered γ Precipitates" Sixth JIM Int.Symp.on Intermetallic Compounds,.

    • Related Report
      1990 Annual Research Report
  • [Publications] C.S.Han: "Precipitation in L1_2ーOrdered NiーAlーCr Alloys." Sixth JIM Int.Symp.on Intermetallic Compounds,.

    • Related Report
      1990 Annual Research Report
  • [Publications] 田文懐: "γ-Ni_3(Al,Ti)L1_2型規則相中への不規則γ相の析出" 日本金属学会誌. 53. 1013-1021 (1989)

    • Related Report
      1989 Annual Research Report
  • [Publications] 田文懐: "微細に分散した不規則γ相を含むγ-Ni_3(Al,Ti)L1_2型規則相単結晶の変形組織" 日本金属学会誌. 53. 1022-1028 (1989)

    • Related Report
      1989 Annual Research Report
  • [Publications] 田文懐: "不規則γ相の析出によるγ-L1_2規則相の強化機構" 日本金属学会誌. 53. 1029-1034 (1989)

    • Related Report
      1989 Annual Research Report

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Published: 1989-04-01   Modified: 2016-04-21  

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