• Search Research Projects
  • Search Researchers
  • How to Use
  1. Back to previous page

Development of Refractory Composites Using Pulse CVI Process

Research Project

Project/Area Number 01850177
Research Category

Grant-in-Aid for Developmental Scientific Research (B).

Allocation TypeSingle-year Grants
Research Field 無機工業化学
Research InstitutionNagoya University

Principal Investigator

SUGIYAMA Kohzo  Nagoya University, Dept. Engin., Professor, 工学部, 教授 (50023023)

Co-Investigator(Kenkyū-buntansha) KUWABARA Katsumi  Nagoya University, Dept. Engin., Res. Assoc., 工学部, 助手 (40023262)
SUZUKI Yutaka  Nagoya University, Dept. Engin., Res. Assoc., 工学部, 助手 (60023214)
Project Period (FY) 1989 – 1990
Project Status Completed (Fiscal Year 1990)
Budget Amount *help
¥7,900,000 (Direct Cost: ¥7,900,000)
Fiscal Year 1990: ¥2,300,000 (Direct Cost: ¥2,300,000)
Fiscal Year 1989: ¥5,600,000 (Direct Cost: ¥5,600,000)
Keywordspulse CVI process / refractory composites / CVI process / CVI of sillicon carbide / パルスCVI法 / CVI / 複合材料 / SiC複合材料
Research Abstract

1. Preparation of the apparatus of pulse CVI process with outer furnace medium scale apparatus for pulse CVI was designed and constructed. In order to shorten the evacuating time to below 1 Torr within 0.8 sec, large pumping system was equipped.
2. Preparating process for preforms the preparating process of two dimensional and three dimensional carbon fiber preforms were studied. Twenty, 40and 60% ethanol solutions of Plyophen (Dainihon Ink., #5900) were compared each other, and the last one which makes the highest ratio of fine pores was selected.
3. The conditions of pulse CVI Mainly, twodimensional C/C preforms with and without 4mum silicon carbide powder were compared. From the results of preliminary experiments, following conditions were selected as standards ; temperature 870-900, concentration of methyltrichlorosilane 4.5-7%, hold time after introduction of gas 0.3-0.6 sec. The preforms with SiC filler were apt to generate microcracks which normally can be seen in C/C composites. Elevating filling ratio of SiC filler is necessary for improvement of the strength of the composites.
4. Three point flexural strength after 10 pulses, the specimens with and without SiC filler showed the strength of 160 and 70 MPa.
5. SEM and EPMA of the cross section T-300 has a considerable clearlance, therefore, infiltration can be done perfectly, on the contrary, M-40 is woven so tight that infiltration is only limited one. The curve of strength vs. number of pulses showed linear property, the refore, the more pulses are considered to improve the strength.

Report

(3 results)
  • 1990 Annual Research Report   Final Research Report Summary
  • 1989 Annual Research Report
  • Research Products

    (18 results)

All Other

All Publications (18 results)

  • [Publications] Kohzo SUGIYAMA: "Reinforcement and Antioxidizing of Porous Carbon by Pluse CVI OF SiC" Journal of Material Science. 24. 3756-3762 (1989)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] Kohzo SUGIYAMA: "Pluse CVI of SiC to Porous Carbon or SiC Particulate Preforms using RFーheating Systems" Journal of Material Science. 25. 4511-4517 (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] 杉山 幸三: "気相からマトリックスを埋める複合材料製造法" ニュ-セラミックス. 3. 87-93 (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] Kouji ITOH: "Pluse CVI of SiC to 2Dーand 3DーCarbonーFiber Preforms" Proceeings of the 11th International Conference on Chemical Vapor Deposition. 11. 553-559 (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] 杉山 幸三: "CVI法によるセラミックス複合体の作製" セラミックス. 26. (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] Kohzo SUGIYAMA: "Reinforcement and Antioxidizing of Porous Carbon by Pulse CVI of SiC" J. Materials Science. Vol. 24. 3756-3762 (1989)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] Kohzo SUGIYAMA: "Pluse CVI of SiC to Porous Carbon or SiC Particulate Preforms using RF-heating Systems" J. Materials Science. Vol. 25. 4511-4517 (1990)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] Kohzo SUGIYAMA: "Preparing Process of Composites Burning the Matrix from Vapor Phase" New Ceramics. Vol. 3. 87-93 (1990)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] Kouji ITO: "Pulse CVI of SiC to 2D-and 3D-carbon-Fiber Preforms" Proceedings of the 11th International Conference on Chemical Vapor Deposition. Vol. 11. 553-559 (1990)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] Kohzo SUGIYAMA: "Preparation of Ceramic Composites by CVI Process" Ceramics. Vol. 26. (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] Kohzo SUGIYAMA: "Reinforcement and Antioxidizing of Porous Carbon by Pluse CVI OF SiC" Journal of Material Science. 24. 3756-3762 (1989)

    • Related Report
      1990 Annual Research Report
  • [Publications] Kohzo SUGIYAMA: "Pluse CVI of SiC to Porous Carbon or SiC Particulate Preforms using RFーheating Systems" Journal of Material Science. 25. 4511-4517 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] 杉山 幸三: "気相からマトリックスを埋める複合材料製造法" ニュ-セラミックス. 3. 87-93 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] Kouji ITOH: "Pluse CVI of SiC to 2Dーand 3DーCarbonーFiber Preforms" Proceeings of the 11th International Conference on Chemical. 11. 553-559 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] Kouji ITOH: "CVI法によるセラミックス複合体の作製" セラミックス. 26. (1991)

    • Related Report
      1990 Annual Research Report
  • [Publications] Kohzo Sugiyama: "Reinforcement and antioxodizing of porous carbon by pulse CVI of SiC" Journal of Materials Science. 24. 3756-3762 (1989)

    • Related Report
      1989 Annual Research Report
  • [Publications] Kohzo Sugiyama: "Pulse CVI of SiC to Porous carbon or SiC particulate preform using RF-heating system" Journal of Materials Science. 25. No.4 (1990)

    • Related Report
      1989 Annual Research Report
  • [Publications] 杉山幸三: "気相からマトリックスを埋める複合材料製造法" ニュ-セラミックス. 3. No.3 (1990)

    • Related Report
      1989 Annual Research Report

URL: 

Published: 1989-04-01   Modified: 2016-04-21  

Information User Guide FAQ News Terms of Use Attribution of KAKENHI

Powered by NII kakenhi