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A study on the microstructure of resin-dentin interface

Research Project

Project/Area Number 02404074
Research Category

Grant-in-Aid for General Scientific Research (A)

Allocation TypeSingle-year Grants
Research Field Conservative dentistry
Research InstitutionTokyo Medical and Dental University

Principal Investigator

TAGAMI Junji  Tokyo Medical and Dental University, Faculty of dentistry, Instructor, 歯学部, 助手 (50171567)

Co-Investigator(Kenkyū-buntansha) INOKOSHI Shigehisa  Lecturer, 歯学部, 講師 (60143583)
FUJITANI Morioki  Instructor, 歯学部, 助手 (60190055)
YAMADA Toshimoto  Lecturer, 歯学部, 講師 (40134712)
SANO Hidehiko  Instructor, 歯学部, 助手 (90205998)
Project Period (FY) 1990 – 1992
Project Status Completed (Fiscal Year 1992)
Budget Amount *help
¥13,600,000 (Direct Cost: ¥13,600,000)
Fiscal Year 1992: ¥1,000,000 (Direct Cost: ¥1,000,000)
Fiscal Year 1991: ¥2,000,000 (Direct Cost: ¥2,000,000)
Fiscal Year 1990: ¥10,600,000 (Direct Cost: ¥10,600,000)
KeywordsADHESIVE RESIN / RESIN-DENTIN INTERFACE / ARGON ION ETCHING / AGING / CARIES / RESIN IMPREGNATED LAYER / COLLAGEN / in vivo / 象牙質 / プライマ-
Research Abstract

Micro structure at the interface between adhesive resin materials and dentin was studied using the argon ion etching technique, which enabled the clear observation of resin impregnated layer under SEM, relating with TEM study and the bond strength.
Resin impregnated layer at resin-dentin interface was confirmed to vary when the dentin bonding system, dentin(i.e. aging, caries, abrasion, and type of tooth) were different. The resin impregnated layer was also different between in vivo and in vitro study.
Type of pretreatment solution for dentin, time of application and primer application were the significant factors which affected the depth of decalcification and the property of the collagen fibers exposed on dentinal surface. Penetration of the bonding resin into dentin may be controlled by these factors. The property of dentin to be bonded was also very important factor in creating resin impregnated layer. That is, type of tooth, site of dentin, distance from the pulp, phisiological or pathological changes in dentin caused by aging,caries and abrasion, and direction of the dentinal tubules at the surface were the factors affecting dentin bonding. Also, the dentinal fluid coming up from the tubules was considered to induce the decrease in the mechanical strength of a layer of bonding resin, resin impregnated layer and resin tags.
The existence of a layer in which bonding resin did not penetrated, was observed, and the layer may act as a micro channel for microleakage.
It was clarified that the width of the resin impregnated layer is not important for creating good bonding, but the bonding resin should be reached to dentin which is not affected with the acidic pretreatment solution, through the decalcified layer.

Report

(4 results)
  • 1992 Annual Research Report   Final Research Report Summary
  • 1991 Annual Research Report
  • 1990 Annual Research Report
  • Research Products

    (27 results)

All Other

All Publications (27 results)

  • [Publications] 杉崎 順平: "コンポジットレジンの象牙質接着性に及ぼす各種プライマーの効果に関する研究ー特に樹脂含浸層のSEMおよびTEM観察とプライマーの扇着向上効果についてー" 日本歯科保存学雑誌. 34. 228-265 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] 中島 正俊: "歯種および歯面の異なる象牙質に対するレジンの接着性に関する研究" 日本歯科保存学雑誌. 34. 266-274 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] Choltacha Harnirattisai: "Interfacal morphology of an adhesive composite resin and etched caries-affected dentin" Opera tive Dentistry. 17. 222-228 (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] Shigehisa Inokoshi: "Interfacial structure between dentin and seven dentin bonding systems revealed usinh argon ionbeam etching" Opera tive Dentistry. (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] Choltacha Harnirattisai: "Ashesive interface besween resin and etched dentin of cervical erosion/abrasion lesions" Opera tive Dentistry. (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] Junji Tagami: "Effect of aging on dentin bonding" American Journal of Dentistry. (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] 猪越 重久: "齲蝕象牙質並びに歯頸部摩耗症硬化象牙質のレジンー象牙質接合界面について" 接着歯学. 11. (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] 田上 順次: "レジン接着性に及ぼす象牙質の加齢の影響について" 接着歯学. 11. (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] Junpei Sugizaki: "The effect of the various primerson the dentin adhesion of resin composites,SEM and TEM observations of the resin impregnated layer and adhesion prompting effect of the primers." Japanese Journal of Conservative Dentistry. 34-1. 228-265 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] Masatoshi Nakajima, Tsunehiko Takada, Junji Tagami and Hiroyasu Hosoda: "A study on Bonding to dentin in various teeth and sites." Japanese Journal of Conservative Dentistry. 34-1. 266-274 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] Choltacha Harnirttasai, Shigehisa Inokoshi, Yasushi Shimada and Hiroyasu Hosoda: "Interfacial morphology of an adhesive composite resin and etched caries-affected dentin." Operative Dentistry. 17-6. 222-228 (1992)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] Shigehisa Inokoshi, Choltacha Harnirttsai, Yasushi Shimada and Hiroyasu Hosoda: "Interfacial structure between dentin and seven dentin bonding systems revealed using argon ion beam etching." Operative Dentistry. 18. (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] Choltacha Harnirttsai, Shigehisa Inokoshi, Yasushi Shimada and Hiroyasu Hosoda: "Adhesive interface between resin and etched dentin of cervical erosion/abrasion lesions." Operative Dentistry. 18. (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] Junji Tagami, Masatoshi Nakajima, Tsunehiko Takada, Toshio Takatsu and Hiroyasu Hosoda: "Effect of aging on dentin bonding." American Journal of Dentistry. 7. (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] Shigehisa Inokoshi, Choltacha Harnirttsai, Yasushi Shimada and Hiroyasu Hosoda: "Adhesive resin-dentin interface of caries affected dentin and cervical erosion/abrasion lesions" Adhesive Dentistry. 11. (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] Junji Tagami, Masatoshi Nakajima, Tsunekazu Shono, Michael F.Burrow, Tsunehiko Takada, Toshio Takatsu and Hiroyasu Hosoda: "Effect of aging on dentin bonding." Adhesive Dentistry. 11. (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] Choltacha Harnirattisai: "Interfacial morphology of an adhesive composite vesin and caries-affected dentin" Operative Dentistry. 17. 222-228 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] Shigehisa Inokoshi: "Inteefacial stucture between dentin and seven deutin bonding systems revealed using argon ion beam etching" Ooerative Dentistry. (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] Choltacha Harnirattisai: "Adhesive interface vesin and etched dentin of cervical erosion/abrasion lesions" Operative Dentistry. (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] Junji Tagami: "Effect of aging on dentin bonding" American Journal of Deutistry. (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] 猪越 重久: "齲蝕象牙質並びに歯頸部磨耗症硬化象牙質のレジン-象牙質接合界面について" 接着歯学. 11. (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] 田上 順次: "レジンの接着性に及ぼす象牙質の加齢の影響について" 接着歯学. 11. (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] 高田 恒彦: "各種〓寒法を用したII級接着性コンポジットレジン修復における歯肉側窩緑の辺緑封鎖性" 日本歯科保存学会雑誌. 34. 828-839 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] 二階堂 徹: "口腔内環境下における4ーMETA/MMAーTBBレジンの象牙質接着性" 日本歯科保存学会雑誌. 34. 1430-1434 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] 佐藤 暢昭: "各種レジンの口腔内環境下における接着性能について" 接着歯学. 9. 158-162 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] 杉崎 順平: "コンポジットレジンの象牙質接着性に及ぼす各種プライマ-の効果に関する研究.特に樹脂含浸層のSEMおよびTEM観察とプライマ-の接着向上効果について" 日本歯科保存学会雑誌. 34. 228-264 (1991)

    • Related Report
      1990 Annual Research Report
  • [Publications] 中島 正俊,高田 恒彦,田上 順次,細田 裕康: "歯種および歯面の異なる象牙質に対するレジンの接着性に関する研究" 日本歯科保存学会雑誌. 34. 265-273 (1991)

    • Related Report
      1990 Annual Research Report

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Published: 1990-04-01   Modified: 2016-04-21  

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