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TOUGHENING OF BRITTLE MATERIALS BY GRAIN BOUNDARY DESIGN AND CONTROL

Research Project

Project/Area Number 02452241
Research Category

Grant-in-Aid for General Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field 金属材料(含表面処理・腐食防食)
Research InstitutionTOHOKU UNIVERSITY

Principal Investigator

WATANABE Tadao  TOHOKU UNIVERSITY, FACULTY OF ENGINEERING, RESEARCH FELLOW, 工学部, 助手 (40005327)

Co-Investigator(Kenkyū-buntansha) OIKAWA Hiroshi  TOHOKU UNIVERSITY, FACULTY OF ENGINEERING, PROFESSOR, 工学部, 教授 (30005243)
Project Period (FY) 1990 – 1992
Project Status Completed (Fiscal Year 1992)
Budget Amount *help
¥5,100,000 (Direct Cost: ¥5,100,000)
Fiscal Year 1992: ¥800,000 (Direct Cost: ¥800,000)
Fiscal Year 1991: ¥1,000,000 (Direct Cost: ¥1,000,000)
Fiscal Year 1990: ¥3,300,000 (Direct Cost: ¥3,300,000)
KeywordsGrain Boundary Design and Control / Grain Boundary Character Distribution / Intergranular Brittleness Control / Brittle Materials / Refractory Metal / Intermetallics / Ni_3Al / Brittle Magnets / 強磁性脆性合金 / N_<i3>Al / 粒界設計制御工学 / 脆性材料の強靭化 / 先端高温材料Ni_3Al / 磁場中焼鈍効果 / 高性能磁性材料Feー50%Co合金 / 規則合金・金属間化合物 / 多結晶体の強靭化 / 粒界性格分布制御 / 高融点金属材料
Research Abstract

The grain boundary character distribution (GBCD) was investigated on three different types of brittle polycrystalline materials produced by different processing methods: refractory metal molybdenum, directionally solidified Ni_3Al and rapidly solidified Fe-50%Co alloy ribbon.
It has been found that the grain boundary character distribution (GBCD) condition of processing and subsequent heat treatments. It has been reveal ed that intergranular brittleness can be controlled by enhancement of the frequency of low-energy boundaries which are resistant to intergranular fracture, or conversely by reduction of the frequency of high-energy random boundaries which are prone to intergranular fracture.
Other microstructural factors associated intergranular brittleness have been investigated: The grain boundary correlation number and the grain boundary triple junction character have been proposed and experimentally studied for real polycrystalline materials.
The modelling of fracture processes and characteristics in polycrystals has made clear that the fracture toughness and brittle-ductile transition strongly depend on the grain boundary character distribution (GBCD) and geometrical arrangements of grain boundaries. This finding has provided a strong support to the basic concept of toughening of brittle materials by grain boundary design and control achieved in this investigation. The result obtained from this work may be applied to ceramics.

Report

(4 results)
  • 1992 Annual Research Report   Final Research Report Summary
  • 1991 Annual Research Report
  • 1990 Annual Research Report
  • Research Products

    (25 results)

All Other

All Publications (25 results)

  • [Publications] L.C.Lim: "Floctune Toughness and Brittle-Duclile Transition Controlled by Grain Boundary Chanacten Distribution(GBCD)in Polycngstale" Acta Metallusgica et Materialia. 38. 2507-2516 (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] T.Satanage: "Grain Boundary Design and Groni Boundary Chanacten Distribution(GBCD)in Textuved Polycngstallive Materials" Textuves and Microstrucheves. 14-18. 739-744 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] T.Watanabe: "Grain Boundary Strengthening Associated With Σ9 Near-Coincidence Boundary in<10TO>Turist Zinc Bicrystals at High Temponature" Philosophical Magazine A. 63. 1013-1022 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] T.Watanabe: "Grain Boundary Chanacten Distribution(GBCD)Analysis of Gram Growth-Related Phenomena in Polycrystallive Materials" Materials Science Forum. 94-96. 209-220 (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] T.Watanabe: "The Importance of Grain Boundary Chanacten Distribution(GBCD)to Recnystallization,Grain Grouth and Textune" Scripta Metallungico et Materialia. 27. 1497-1502 (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] T.Watanabe: "Toughening of Brittle Materials by Grain Boundary Design and Contral" Materials Science Forum. (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] L.C.LIM and T.WATANABE: "Fracture Toughness and Brittle-Ductile Transition controlled by Grain Boundary Character Distribution (GBCD) in Polycrystals." Acta Metallurgica et Materialia. 38. 2507-2516 (1990)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] T.WATANABE: "Grain Boundary Design and Grain Boundary Character Distribution (GBCD) in Textured Polycrystalline Materials." Textures and Micro-structures. 14-18. 739-744 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] T.WATANABE, M.YAMADA, S.KARASHIMA: "Grain Boundary Strengthening Associated with SIGMA9 Near-Coincidence Boundary in <1010> Twist Zinc Bicrystals at High Temperatures." Philosophical Magazine. A,63. 1013-1022 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] T.WATANABE: "Grain Boundary Character Distribution (GBCD) Analysis of Grain Growth-Related Phenomena in Polycrystalline Materials." Materials Science Forum. 94-96. 209-220 (1992)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] T.WATANABE: "The Importance of Grain Boundary Character Distribution (GBCD) to Recrystallization, Grain Growth and Texture." Scripta Metallurgica et Materialia. 27. 1497-1502 (1992)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] T.WATANABE: "Toughening of Brittle Materials by Grain Boundary Design and Control." Materials Science Forum. (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] T.WATANABE: "Grain Boundary Character Distribution (GBCD) Analysis of Graiin Growth Related Phenomena in polycristallive Materials" Materials Science Forum. 94-96. 209-220 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] T.WATANABE: "The Importance of Grain Boundary Charactor Distribution (GBCD) to Recngstallization Groin Growth and Texture" Scripta Metallurgica et Materialia. 27. 1497-1502 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] 渡辺 忠雄: "結晶界面の性格・構造と性質の相関の材料設計への応用" 日本金属学会会報. 31. 138-145 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] 渡辺 忠雄: "結晶粒成長に係わる諸問題と粒界" 材料科学. 29. 263-270 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] T.WATANABE: "Grain Boundary Design for Adianced Materials on the Basis of the Relationship between Texture and Grain BoundaryCharacter Distribution (GBCD)." Textures and Microstructures. (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] T.WATANABE: "Toughening of Brittle Materials by Grain Boundary Design and Control" Materials Science Forum. (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] Tadao WATANABE: "Grain Boundary Design and Grain Boundary Character Distribution(GBCD)in Textured Polycrystalline Materials" Textures and Microstructures. 14〜18. 739-744 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] 渡辺 忠雄: "結晶界面の性格・構造と性質の相関の材料設計への応用" 日本金属学会会報,特集号. 31. 138-145 (1992)

    • Related Report
      1991 Annual Research Report
  • [Publications] Tadao WATANABE: "Grain Boundary Design for Advanced Materials on the Basis of the Relationship between Texture and Grain Boundary Character Distribution(GBCD)" 米国金属学会シンポジウム会議録 Textures and Microstructures. 特集号. (1992)

    • Related Report
      1991 Annual Research Report
  • [Publications] 渡辺 忠雄: "粒界設計制御にもとづく先端材料開発への道.…マイクロマシン材料から超電導材料まで…" 日本材料学会誌「材料」. 41. (1992)

    • Related Report
      1991 Annual Research Report
  • [Publications] Tadao WATANABE: "Toughening of Brittle Materials by Grain Boundary Design and Control." 第6回粒界・異相界面に関する国際会議(基調講演,1992年6月,ギリシヤ)会議録,予定. (1993)

    • Related Report
      1991 Annual Research Report
  • [Publications] L.C.LIM Tadao WATANABE: "Fracture Toughness and BrittleーDuctile Transition Controlled by Grain Boundary Character Distribution (GBCD) in Polycrystals." ACTA METALLURGICA et MATERIALIA. 38. 2507-2516 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] Tadao WATANABE: "Grain Boundary Design and Grain Boundary Character Distribution (GBCD) in Textured Polycrystalline Materials." Proceedings of the 9th International Conference on Textures of Materials,Societe Francaise de Metallurgie. (1991)

    • Related Report
      1990 Annual Research Report

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Published: 1990-04-01   Modified: 2016-04-21  

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