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Development of aluminum-alloy extrahigh-vacuum (XHV) systems featured by new surface treatments

Research Project

Project/Area Number 02555008
Research Category

Grant-in-Aid for Developmental Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field 物理計測・光学
Research InstitutionTohoku University

Principal Investigator

MIYAMOTO Nobuo  Tohoku University, Research Institute of Electrical Communication, Professor, 電気通信研究所, 教授 (00006222)

Co-Investigator(Kenkyū-buntansha) WATANABE Fumio  Sukegawa Electric Co., Ltd. Tsukuba Labo. Senior Researcher, 主管技師
MIYAMOTO Kazuo  Musashino Engineering Co., Ltd. Technical Director, 技術部長
SUEMITSU Maki  Tohoku University Research Institute of Electrical Communication, Associate Prof, 電気通信研究所, 助教授 (00134057)
Project Period (FY) 1990 – 1991
Project Status Completed (Fiscal Year 1991)
Budget Amount *help
¥15,800,000 (Direct Cost: ¥15,800,000)
Fiscal Year 1991: ¥2,300,000 (Direct Cost: ¥2,300,000)
Fiscal Year 1990: ¥13,500,000 (Direct Cost: ¥13,500,000)
KeywordsExtrahigh Vacuum / Aluminum-Alloy Vacuum System / Titan Sublimation Pump / mirror-polished surface / 超高真空 / ガス放出率 / 光電子分光
Research Abstract

1) A new mirror-surface polishing technique for aluminum-alloys, OMCP (Organo-Mechanochemical Polishing) method, has been developed and has been applied to a construction of aluminum-alloy extrahigh vacuum (XHV) system. The OMCP method is the first surface polishing technique for aluminum-alloys that can produce a surface oxide layer as thin as a few nm. In addition to chamber walls, mirror-polished valves and a liquid N_2 shroud have also been constructed using this method.
2) A new Ti sublimation pump (TSP) has been constructed based on an idea that the performance of conventional TSPs are limited by (1) the outgassing from the heated sublimator and (2) the desorption of the gettered molecules from the evaporated Ti surface. The new TSP is equipped with an electron-gun type Ti evaporator and an mounted heater in the liquid N_2 shroud, in order to overcome the limitations (1) and (2), respectively.
3) A new method to evaluate the x-ray limit of an extractor gauge has been developed, which allows precise pressure measurements in the XHV range.
Furthermore, a new total pressure gauge, ion spectroscopy gauge (ISG), has been developed to elliminate errors due to both the ions by the electron stimulated desorption (ESD) from the grid and the x-ray limit.
4) Finally, all these equipments have been combined to form a system. It has been evacuated and an XHV of 10^<-12> mbar order has been realized after only 29 h of evacuation from the air-purged state.

Report

(3 results)
  • 1991 Annual Research Report   Final Research Report Summary
  • 1990 Annual Research Report
  • Research Products

    (18 results)

All Other

All Publications (18 results)

  • [Publications] 渡辺 文夫: "新しいX線光電子エミッション打ち消し法とXHVゲ-ジへの応用" 真空. 34. 25-28 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] 渡辺 文夫: "ポイントコレクタ-ゲ-ジによる10^<ー11>Pa領域での圧力測定の誤差の評価" 真空. 34. 17-24 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] M.Suemitsu,H.Shimoyamada,N.Matsuzaki,N.Miyamoto and J.Ishibe: "Photoemission studies and outgassing-rate measurements on aluminum-alloy surfaces lathed with various alcohols" J.Vac.Sci.Technol. A10. 188-192 (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] M.Suemitsu,H.Shimoyamada,N.Muyamoto,T.Tokai,Y.Moriya,H.Ikeda,and H.Yokoyama: "An ultrahigh-vacuum compatible mirror-polished aluminum-alloy surface:observation of surface-roughness-correlated outgassing tates" J.Vac.Sci.Technol. A10. (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] 渡辺 文夫: "ESDイオン誤差を除去したX線限界10^<ー12>Paのイオン分光ゲ-ジ" 真空. 35. (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] 末光 眞希,采女 豊,石辺 二朗,宮本 信雄: "変調加熱昇温脱離法によるガス放出特性評価" 真空. 35. (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] F. Watanabe: "New x-ray limit measurements for extractor gauges" J. Vac. Sci. Technol.A9. 2744-2746 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] M. Suemitsu, H. Shimoyamada, N. Matsuzaki, N. Miyamoto, and J. Ishibe: "Photoemission studies and outgassing-rate measurements on aluminum-alloy surfaces lathed with various alcohols" J. Vac. Sci. Technol.A10. 188-192 (1992)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] M. Suemitsu, H. Shimoyamada, N. Miyamoto, T. Tokai, Y. Moriya, H. Ikeda, and H. Yokoyama: "An ultrahigh-vacuum compatible mirror-polished aluminum-alloy surface : observation of surface-roughness-correlated outgassing rates" J. Vac. Sci. Technol.A10. (1992)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] M. Suemitsu, Y. Uneme, J. Ishibe, and N. Miyamoto: "TDS evaluation of outgassing characteristics of surfaces by modulated heating method" J. Vac. Soc. Jpn.35. (1992)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] F. Watanabe: "Ion spectroscopy gauge for the XHV pressure measurements down to 10^<-12> Pa without errors due to ESD" J. Vac. Soc. Jpn.35. (1992)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] 渡辺 文夫: "新してX線光電子エミッション打ち消し法とXHVゲ-ジへの応用" 真空. 34. 25-28 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] 渡辺 文夫: "ポイントコレクタ-ゲ-ジによる10^<-11>Pa領域での圧力測定の誤差の評価" 真空. 34. 17-24 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] M.Suemitsu,H.Shimoyamada,N.Matsuzaki,N.Miyamoto,and J.Ishibe: "Photoemission studies and Outgassing-rate measurements on aluminum-alloy,surfaces lathed with various alcohols" J.Vac.Sci.Technol.A10. 188-192 (1992)

    • Related Report
      1991 Annual Research Report
  • [Publications] M.Suemitsu,H.Shimoyamada,N.Miyamoto,T.Tokai,Y.Moriya,H.Ikeda,and H.Yokoyama: "An ultrahigh-vacuum compatible mirror-polished aluminum-alloy surface:observation of surface-roughness-correlated outgassing rates" J.Vac.SCi.Technol.A10. (1992)

    • Related Report
      1991 Annual Research Report
  • [Publications] 渡辺 文夫: "ESDイオン誤差を誤差を除去したX線限界10^<-12>Paのイオン分光ゲ-ジ" 真空. 35. (1992)

    • Related Report
      1991 Annual Research Report
  • [Publications] 門光 眞希,采女 豊,石辺 二朗,宮本 信雄: "変調加熱昇温脱離法によるガス放出特性評価" 真空. 35. (1992)

    • Related Report
      1991 Annual Research Report
  • [Publications] M.Suemitsu,H.Shimoyamada,N.Matsuzaki,N.Miyamoto,J.Ishibe: "Photoemission studies and outgassingーrate measurements on aluminumーalloy surfaces lathed with various alcohols" J.Vac.Sci.Technol.

    • Related Report
      1990 Annual Research Report

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Published: 1990-04-01   Modified: 2016-04-21  

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