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Ion Beam Microsectioning Apparatus for Precision Measurement of Neutron Radiation-Enhanced Diffusion

Research Project

Project/Area Number 02555134
Research Category

Grant-in-Aid for Developmental Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field Physical properties of metals
Research InstitutionTohoku University

Principal Investigator

NAKAJIMA Hideo  Institute for Materials Research, Tohoku University, Associate Professor, 金属材料研究所, 助教授 (30134042)

Co-Investigator(Kenkyū-buntansha) MATSUI Hideki  Institute for Materials Research, Tohoku University, Professor, 金属材料研究所, 教授 (50005980)
Project Period (FY) 1990 – 1991
Project Status Completed (Fiscal Year 1991)
Budget Amount *help
¥10,200,000 (Direct Cost: ¥10,200,000)
Fiscal Year 1991: ¥2,400,000 (Direct Cost: ¥2,400,000)
Fiscal Year 1990: ¥7,800,000 (Direct Cost: ¥7,800,000)
Keywordsdiffusion / neutron radiation effect / radiation-enhanced diffusion / ion beam / microsectioning apparatus / セクショニング装置 / 中性子照射 / 照射損傷 / 拡散機構
Research Abstract

The present research was undertaken to manufacture an ion beam microsectioning apparatus for precise measurements of neutron radiation-enhanced diffusion in metals and alloys. The neutronirradiated diffusion sample is sectioned by the ion-beam microsectioning apparatus and deposited onto Kapton films. After the deposition, the activity from the deposited Kapton films is measured by a scintillation counter to know the diffusion-penetration profiles. The apparatus was manufactured successfully and fully operated to measure the diffusion penetration profiles up to a depth of 200 nm.
Several irradiation experiments were performed at the JMTR. The aluminum sample on which iron film of 10 nm was deposited was capsuled into aluminum can under a vacuum to prevent oxidation in irradiation. Radiation diffusion runs were carried out for 533 hr. at 400C and for 168 hr. at 200C. After irradiation the samples were sectioned by the ion-beam microsectioning apparatus and diffusion penetration profiles were determined with high precision.

Report

(3 results)
  • 1991 Annual Research Report   Final Research Report Summary
  • 1990 Annual Research Report
  • Research Products

    (19 results)

All Other

All Publications (19 results)

  • [Publications] 山口 久: "拡散測定のためのナノセクショニング装置の試作" 東北大学金属材料研究所研究技術報告. (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] H.Nakajima: "Diffusion of Oxygen in Vanadium and its Alloys" Phil.Mag.,.

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] H.Matsui: "Swelling of a V-5Fe Alloy after Irradiation in JOYO" the Science Reports of the Research Institutes,Tohoku University. A35. 196-207 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] H.Nakajima: "Effect of Solute Addition on Swelling of Vanadium After FFTF Irradiation," Annual Progress Report for Fusion Year 1990. 71-77 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] H.Nakajima: "Effect of Solute Addition on Swelling of Vanadium After FFTF Irradiation," J.Nucl.Mater.,. (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] H.Matsui: "Microstructural Evolution in V-5%Fe Alloy by Fast Neutron Irradiation," J.Nucl.Mater.,. (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] H. Yamaguchi, H. Nakajima, H. Kawamura, S. Hayasaka, T. Shouji, K. Fuda, E. Koike, K. Irumagawa, T. Hongo and H. Igari: "Manufacture of Ion-Beam Microsectioning Apparatus for Precise Measurement of Diffusion" Technical Reports of Institute for Materials Research, Tohoku University. (1992)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] H. Nakajima, S. Nagata, H. Matsui and S. Yamaguchi: "Diffusion of Oxygen in Vanadium and its Alloys" Phil. Mag.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] H. Matsui and H. Nakajima: "Swelling of a V-5Fe Alloy After Irradiation in JOYO the Science Reports of the Research Institutes, Tohoku University" A35. 196 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] H. Nakajima, S. Yoshida, Y. Kohno and H. Matsui: "Effect of Solute Addition on Swelling of Vanadium After FFTF Irradiation" Annual Progress Report for Fusion Year 1990. 71 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] H. Nakajima, S. Yoshida, Y. Kohno and H. Matsui: "Effect of Solute Addition on Swelling of Vanadium After FFTF Irradiation" J. Nucl. Mater.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] H. Matsui and H. Nakajima: "Microstructural Evolution in V-5%Fe Alloy by Fast Neutron Irradiation" J. Nucl. Mater.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] H. Nakajima and M. Koiwa: "Diffusion in Titanium" ISIJ International. 31. 757 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] 山口 久: "拡散測定のためのナノセクショニング装置の試作" 東北大学金属材料研究所研究技術報告. (1992)

    • Related Report
      1991 Annual Research Report
  • [Publications] H.Nakajima: "Diffusion of Oxygen in Vanadium and its Alloys" Phil.Mag.,.

    • Related Report
      1991 Annual Research Report
  • [Publications] H.Matsui: "Swelling of a V-5Fe Alloy after Irradiation in JOYO" the Science Reports of the Research Institutes,Tohoku University. A35. 196-207 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] H.Nakajima: "Effect of Solute Addition on Swelling of Vanadium After FFTF Irradiation," Annual Progress Report for Fusion Year 1990. 71-77 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] H.Nakajima: "Effect of Solute Addition on Swelling of Vanadium After FFTF Irradiation," J.Nucl.Mater.,. (1992)

    • Related Report
      1991 Annual Research Report
  • [Publications] H.Matsui: "Microstructural Evolution in V-5%Fe Alloy by Fast Neutron Irradiation," J.Nucl.Mater.,. (1992)

    • Related Report
      1991 Annual Research Report

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Published: 1990-04-01   Modified: 2016-04-21  

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