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Temperature measurement on submicron-area of thin films by using electron beam

Research Project

Project/Area Number 02650030
Research Category

Grant-in-Aid for General Scientific Research (C)

Allocation TypeSingle-year Grants
Research Field 物理計測・光学
Research InstitutionOsaka University

Principal Investigator

TAKAOKA Akio  Faculty of Engineering Associate Professor, 工学部, 助教授 (80029272)

Project Period (FY) 1990 – 1991
Project Status Completed (Fiscal Year 1991)
Budget Amount *help
¥1,900,000 (Direct Cost: ¥1,900,000)
Fiscal Year 1991: ¥400,000 (Direct Cost: ¥400,000)
Fiscal Year 1990: ¥1,500,000 (Direct Cost: ¥1,500,000)
KeywordsTemperature Measurement / Local Temperature / Thin Film / Thermal Conductivity / Electron Beam / Transmission Electron Microscope / Thermal Diffusivity / Thermal Diffuse Scattering / 電子ビ-ム / 薄膜温度
Research Abstract

The local temperature on submicron-area and the thermal-conductivity of thin films are measured by using transmission electron microscopes (TEM) whose spatial resolution is excellent. This measurement is based on the thermal diffuse scatterino, effect in the specimen and on the change of electron beam transmission by the temperature if an aperture is inserted. This high spatial resolution can not be attained for the measurement with light.
In 1990, we tried to measure the local temperature on Al lines in LSI as an expansion of measurement for polycrystalline films. The grain size of AI lines is about 1 mum, so the measuring area consists of almost single crystal. In the case of a single crystal, a slight tilt of the specimen by heating degrade the accuracy due to the change of Bragg diffraction and other interferences. Then, the transmission measured at many points automatically with a personal computer and the transmission independent of such interferences is obtained. The accuracy is about <plus-minus>50K in the range of 300-550 K at presen
In 1991, we investigated the measurement method of thermal conductivity of thin films by combining the local heating with a laser. The laser output is modulated by sine wave and the phase difference between the laser and the local temperature is measured by a lockin-amplifier. This method has some advantages that the absolute measurerdent of temperature does not need and it is no need to know the physical constant of films. For a polycrystalline Al film of 200nm in thickness, the measured conductivity varies in the range of 30-100 W/mK. This results from the error in the conversion form the phase difference to the conductivity as well as the error in the measurement of phase. The precise determination of laser irradiation condition needs for the specimen of TEIL. We improved the measurement system to determine this condition precisely and also found the condition in which the error is little.

Report

(3 results)
  • 1991 Annual Research Report   Final Research Report Summary
  • 1990 Annual Research Report
  • Research Products

    (7 results)

All Other

All Publications (7 results)

  • [Publications] Akio Takaoka and Kastumi Ura: "Temperature measarement on micro-area of specimen in TEM by using thermal diffuse scattering effect" J.Electron Microsc.39. 69-70 (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] A.Takaoka,H.Taoka and K.Ura: "Temperature measurement on micro-area of polycrys talline film with TEM" Electron Microscopy 1990 〔Proc.12 Int.Cong.for EM,Seattle〕. 1. 128-129 (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] 鷹岡 昭夫,裏 克己: "薄膜熱伝導率の電子顕微鏡を用いた計測法" 日本電子顕微鏡学会第48回学徴講演会予稿集. (1992)

    • Related Report
      1991 Annual Research Report
  • [Publications] 鷹岡 昭夫,裏 克己: "サブミクロン領域の試料温度計測システムの開発と応用" 日本電子顕微鏡学会、電子顕微鏡周辺機器の活用、開発とその応用に関する研究部会講演概要集. 1 (1992)

    • Related Report
      1991 Annual Research Report
  • [Publications] A.Takaoka,H.Taoka and K.Ura: "Temperature measurement on microーarea of polycrystalline film with TEM" Electron Microscopy 1990[Proc,12 Int,Cong,for EM,Seattle]. 1. 128-129 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] 鷹岡 昭夫,田岡 洋,裏 克己: "透過電子顕微鏡を用いた局所温度計測法(II)" 日本電子顕微鏡学会第46回学術講演会 予稿集. 233 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] 西 竜治,鷹岡 昭夫,裏 克己: "LSIアルミ配線の局所温度計測ー結晶粒子の温度計測法についてー" 日本電子顕微鏡学会第47回学術講演会 予稿集. (1991)

    • Related Report
      1990 Annual Research Report

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Published: 1990-04-01   Modified: 2016-04-21  

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