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Measarements of Mass Transfer Volumetric Coefficient and Droplet Diameter in Liquid-Liquid Mixing Vessel by Using Chemical Reaction Method

Research Project

Project/Area Number 02650684
Research Category

Grant-in-Aid for General Scientific Research (C)

Allocation TypeSingle-year Grants
Research Field 化学工学
Research InstitutionNagoya Institute of Technology

Principal Investigator

HIRAOKA Setsuro  Nagoya Institute of Technology, Faculty of Engineering ; Professor, 工学部, 教授 (80026070)

Project Period (FY) 1990 – 1991
Project Status Completed (Fiscal Year 1991)
Budget Amount *help
¥2,200,000 (Direct Cost: ¥2,200,000)
Fiscal Year 1991: ¥400,000 (Direct Cost: ¥400,000)
Fiscal Year 1990: ¥1,800,000 (Direct Cost: ¥1,800,000)
KeywordsLiquid Liquid Dispersion / Mass Transfer Coefficient / Droplet Diameter / Ester Hydrolysis / Wire Gauze Impeller / Double Stage Impeller / Tall Agitated Vessel / 物質移動係数 / 撹拌所要動力
Research Abstract

In a present work, the mass transfer volumetric coefficient, K_La, on droplet surface in liquid-lipuid dispersons was measured by using hydrolysis reaction of ester with alkali. The diameter, dp, was measured by using a videorecorder via a microscope during the reaction period, allowing the mass transfer coefficient, K_L, to be determined. The measurements of K_La and dp were conducted in various kinds of agitated vessels, and the following results were obtained.
(a) Standard paddle impeller : Various sizes of paddle impellers were used to measure the values of K_La and dp in liquid-liquid agitated vessels. The mass transfer coefficient obtained was well correlated with the power input per unit volume and the dropeet diameter. The resultant dimensionless correlation equation was confirmed to be close to that for the solid suspension system.
(b) Wire-gauze impeller : Wire-gauze impeller was designed to get higher value of K_La in liquid-liquid dispersions, then it is known that the impeller with larger diameter of wire-gauze blades than that of board blades was more effective to mass transfer at a specified power imput.
(c) Double-stage impeller : Double-stage impeller was used in a tall agitated vessel, then it was confirmed experimentally that the double-stage impeller was most effective in the vessel whose height was twice the vessel diameter.

Report

(3 results)
  • 1991 Annual Research Report   Final Research Report Summary
  • 1990 Annual Research Report
  • Research Products

    (9 results)

All Other

All Publications (9 results)

  • [Publications] 日比野 慎司: "近接異種2段翼を備えた液液撹拌槽における物質移動係数と液滴径の測定" 化学工学会岡山大学講演要旨集. 12-13 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] S.Hiraoka: "Mass Transfer Coefficient and Droplet Diameter in Liquid-Liquid Dispersons Stirred with Wire - Gauze Impeller" Proceedings China - Japan Chemical Engineering Conference. 828-835 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] 日比野 慎司: "2段翼を備えた液液撹拌槽における物質移動係数と液滴径の測定" 化学工学会第57年会講演要旨集. 70 (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] S. Hibino et al: "Measurements of Mass Transfer Coefficient and Droplet Diameter in a Loquid - Liquid Agitated Vessel with a Double - Stage Impeller" Proceedings of Chemical Engineering Okayama Meeting. 12-13 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] S. Hiraoka et al.: "Mass Transfer Coefficient and Droplet Diameter in Liquid - Liquid Dispersions Stirred with Wire - Gauze Impeller" Proceedings of China - Japan Chemical Engineering Confernce. 828-835 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] S. Hiraoka et al.: "Measurements of Mass Transfer Coefficient and Droplet Diameter in Liquid - Lquid Dispersions Stirred with Double - Stage Impeller" Proceedings of 57th Annual Meeting of the Society of Chemical Engineers Japan. 70 (1992)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1991 Final Research Report Summary
  • [Publications] S.Hiraoka: "Mass Transfer Coefficient and Droplet Diameter in LiquidーLiquid Dispersions Stirred with WireーGauze Impeller" Proceedings ChinaーJapan Chemical Engineering Conference. 828-835 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] 日比野 慎司: "2段翼を備えた液液撹拌槽における物質移動係数と液滴径の測定" 化学工学会第57年会講演要旨集. (1992)

    • Related Report
      1991 Annual Research Report
  • [Publications] 日比野 慎司: "近接異種2段翼を備えた液液撹拌槽における物質移動係数と液滴径の測定" 化学工学会岡山大会講演要旨集. (1991)

    • Related Report
      1990 Annual Research Report

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Published: 1990-04-01   Modified: 2016-04-21  

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