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Study on deformation and fracture behavior of tuicrystals and its application to design of grain boundaries in polycrystals

Research Project

Project/Area Number 03402045
Research Category

Grant-in-Aid for General Scientific Research (A)

Allocation TypeSingle-year Grants
Research Field Physical properties of metals
Research InstitutionKyoto University

Principal Investigator

MIURA Sei  Kyoto Univ., Faculty of Eng., Professor, 工学部, 教授 (00066169)

Co-Investigator(Kenkyū-buntansha) KATO Hiroyuki  Kyoto Univ., Fac. of Eng., Ass. Instructor, 工学部, 助手 (80224533)
ONAKA Susumu  Kyoto Univ., Fac. of Eng., Ass. Instructor, 工学部, 助手 (40194576)
HASHIMOTO Satoshi  Kyoto Univ., Fac. of Eng., Ass. Professor, 工学部, 助教授 (50127122)
Project Period (FY) 1991 – 1993
Project Status Completed (Fiscal Year 1993)
Budget Amount *help
¥16,500,000 (Direct Cost: ¥16,500,000)
Fiscal Year 1993: ¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 1992: ¥1,000,000 (Direct Cost: ¥1,000,000)
Fiscal Year 1991: ¥14,900,000 (Direct Cost: ¥14,900,000)
KeywordsTriple Line / Bicrystal / Tricrystal / Grain Boundary / Interphase Boundary / Creep / Fatigue / Intergranular Fracture / 二相ステンレス鋼 / 異相界面 / 界面すべり / 粒界疲労 / 粒界構造 / 粒界会合部 / 対応格子 / 粒界すべり / 中間温度ぜひ性 / 高温変形 / 粒界三重線 / 三重線fold / すべり帯 / 変形帯 / 応力伝達係数 / 不均一変形
Research Abstract

The purpose of this project is to understand the structures of grain boundaries and boundary nodes (triple lines) necessary for strengthening of polycrystals. To achieve the purpose, we have studied roles of a grain boundary and a triple line in deformation and fracture from experiments employing tricrystals. Mains results obtained are summarized as follows.
1. We have grown single, bi-and tri-crystals of metals and alloys, and studied deformation and fracture behavior of the crystals by tensile, creep and fatigue tests. Localized deformation and formation and propagation of cracks at and around the grain boundaries and triple lines have been quantitatively and systematically studied including the effects of orientations of the grain boundaries and triple lines. We have revealed contribution of the triple lines to deformation and fracture and its temperature dependence, and presented the structures of grain boundaries and triple lines necessary for the strengthening of materials.
2. We have adopted tricrystals consisting of so called special boundaries as main specimens. The same triple lines with the triple lines in the tricrystals have been found in recrystallized copper bicrystals. We have shown the application of the results obtained using the tricrystals to the discussion of mechanical properties of polycrystals.
3. Considering the importance of multi-phase materials as practical structural materials, effects of intrphase boundaries on mechanical properties have been studied. We have (gamma/alpha) stainess bicrystals by diffusion bonding and investigated the constraint of grain deformation and the superplastic flow at the interphase boundaries.

Report

(4 results)
  • 1993 Annual Research Report   Final Research Report Summary
  • 1992 Annual Research Report
  • 1991 Annual Research Report
  • Research Products

    (35 results)

All Other

All Publications (35 results)

  • [Publications] S.Hashimoto: "Sliding along the interphase boundary in austenite/ferrite duplex stainless steel bicrystals" Proc.of Superplasticity in Advanced Materials. 23-32 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] S.Hashimoto: "Interphase boundary sliding in two-phase (γ/α)-FeCrNi alloy bicrystals produced by a solid-solid diffusion method" Proc.of Mechanical Behaviour of Materials-VI. 3. 655-660 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 橋本 敏: "相界面のバイクリスタル研究-二相(γ/α)ステンレス鋼双結晶の超塑性界面すべり-" 日本金属学会会報. 31. 116-122 (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] J.Rys: "Deformation behaviour of stainless steel (α/γ) two-phase bicrystals" Archives of Metallurgy. 38. 255-275 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] S.Hashimoto: "Role of interphase-boundary sliding in a superplastic flow of duplex materials consisting of a soft and a hard phases" Proc.of JIMIS-7 on Aspects of High Temperature Deformation and Fracture in Crystalline Materials. 115-122 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] T.Takahashi: "Grain-boundary triple junction fold in FCC metals and alloys" Proc.of JIMIS-7 on Aspects of High Temperature Deformation and Fracture in Crystalline Materials. 131-138 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 方 蘇春: "Σ3{111}およびΣ9{221}粒界を有する銅双結晶の再結晶において結晶粒界が果たす役割" 材料. 42. 784-790 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 方 蘇春: "再結晶した銅多結晶における結晶粒方位差の分布およびΣ3+Σ3+Σ9粒界会合部の安定性" 材料. 42. 791-797 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 橋本 敏: "Compact-Tension双結晶試験片における粒界疲労亀裂の挙動" 日本金属学会誌. 57. 972-973 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] T.Wada: "Plastic deformation of two-phase (γ/α) stainless steel bicrystals" Proc.of IUMRS-ICAM-93. (in press).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] S.Onaka: "The effect of a boundary node on intergranular fracture of an α-CuAl alloy at intermediate temperatures" Proc.of ICSMA-10. (in press).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] S.Hashimoto: "Sliding along the interphase boundary in austenite / ferrite duplex stainless steel bicrystals" Proc. of Superplasticity in Advanced Materials. 23-32 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] S.Hashimoto: "Interphase boundary sliding in two-phase (gamma / alpha) -FeCrNi alloy bicrystals produced by a solid-solid diffusion method" Proc. of Mechanical Behavior of Materials-VI. Vol.3. 655-660 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] S.Hashimoto: "bicrystal study on the interface - Superplastic interphase-boundary sliding in a two-phase (gamma / alpha) -stainless steel bicrystals -" Bulletin of the Japan Institute of Metals. Vol.31. 116-122 (1992)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] J.Rys: "Deformation behavior of stainless steel (gamma / alpha) two-phase bicrystals" Archives of Metallurgy. Vol.38. 255-275 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] S.Hashimoto: "Role of interphase-boundary sliding in a superplastic flow of duplex materials consisting of a soft and a hard phases" Proc. of JIMIS-7 on Aspects of High Temperature Deformation and Fracture in Crystalline Materials. 115-122 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] T.Takahashi: "Grain-boundary triple junction fold in FCC metals and alloys" Proc. of JIMIS-7 on Aspects of High Temperature Deformation and Fracture in Crystalline Materials. 131-138 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] S.Fang: "Roles of grain boundaries in recrystallization of copper bicrystals with sigma3{111} and sigma9{221} boundaries" J.Soc. Materials Sci. Japan. Vol.42. 784-790 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] S.Fang: "Distribution of disorientation and stability of sigma3+sigma3+sigma9 triple junctions in a copper polycrystalafter recrystallization" J.Soc. Materials Sci. Japan. Vol.42. 791-797 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] S.Hashimoto: "intergranular fatigue cracking in compact-tension bicrystal specimens" J.of the Japan Institute of Metals. Vol.57. 972-973 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] T.Wada: "Plastic deformation of two-phase (gamma / alpha) stainless steel bicrystals" Proc. of IUMRS-ICAM-93. (in press). (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] S.Onaka: "The effect of a boundary node on intergranular fracture of an alpha-CuAl alloy at intermediate temperatures" Proc. of ICSMA-10. (in press). (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] T.Wada: "Plastic deformation of two-phase(γ/α)stainless steel bicrystals" Proc.of IUMRS-ICAM-93. (印刷中). (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] J.Rys: "Deformation behaviour of stainless steel(α/γ)two-phase bicrystals" Archives of metallurgy. 38. 255-275 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] T.Takahashi: "Grain-boundary triple junction fold in FCC metals and alloys" Proc.of JIMIS-7. 1. 131-138 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] S.Hashimoto: "Role of interphase-boundary sliding in a superplastic flow of duplex materials" Proc.of JIMIS-7. 1. 115-122 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] 橋本敏: "Compact-Tension 双結晶試験片における粒界疲労亀裂の挙動" 日本金属学会誌. 57. 972-973 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] 方 蘇春: "再結晶した銅多結晶における粒界方位差の分布およびΣ3+Σ3+Σ9粒界会合部の安定性" 材料. 42. (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] 方 蘇春: "Σ3{111}およびΣ9{221}粒界を有する銅双結晶の再結晶において結晶粒界が果たす役割" 材料. 42. (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] S.Hashimoto: "Sliding Along the Interphase Boundary in Austenite/Ferrite Duplex Stainless Steel Bicrystals" Superplasticity. 23-32 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] S.Hashimoto: "Interphase Boundary Sliding in TwoーPhase(γーα)ーFeCrNi Alloy Bicrystals Produced by a SolidーSolid Diffusion Method" Mechanical Behaviour of MaterialsーVl. 3. 655-660 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] M.Yamashita: "Intergranular Corrosion of Copper and αーCuーAl Alloy Bicrystals" Philosophical Magazine A. 63. 695-705 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] M.Yamashita: "Stress Corrosion Cracking of〔110〕and〔100〕Tilt Boundaries of αーCuーAl Alloy" Philosophical Magazine A. 63. 707-726 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] M.Yamashita: "Bicrystal Study on Intergranular StressーCorrosionーCracking" Materials Transactions.JIM. 32. 885-897 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] 橋本 敏: "相界面のバイクリスタル研究 一二相(γ/α)ステンレス銅双結晶の超塑性界面すべりー" 日本金属学会会報. 31. 116-122 (1992)

    • Related Report
      1991 Annual Research Report

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Published: 1991-04-01   Modified: 2016-04-21  

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