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The development of the system for analyzing thin-film structure by using grazing incidence diffraction technique

Research Project

Project/Area Number 03452293
Research Category

Grant-in-Aid for General Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field 結晶学
Research InstitutionNagoya Institute of Technology

Principal Investigator

TORAYA Hideo  Nagoya Institute of Technology, Associate Professor, 工学部, 助教授 (20143662)

Co-Investigator(Kenkyū-buntansha) TORAYA Hideo  Nagoya Institute of Technology, Associate Professor (20143662)
Project Period (FY) 1991 – 1993
Project Status Completed (Fiscal Year 1993)
Budget Amount *help
¥7,600,000 (Direct Cost: ¥7,600,000)
Fiscal Year 1993: ¥300,000 (Direct Cost: ¥300,000)
Fiscal Year 1992: ¥200,000 (Direct Cost: ¥200,000)
Fiscal Year 1991: ¥7,100,000 (Direct Cost: ¥7,100,000)
KeywordsGrazing Incidence Diffraction / Thin-Film / Asymmetric Diffraction / Surface Structure / Parallel-Beam Optics / Computer Software for Analysis / スレスレ入射回析 / スレスレ入射回折法 / 計算機用ソフトウェア- / 解析システム開発
Research Abstract

The diffractometer for grazing incidence diffraction (GID) has been developed, which can be used for thin-film structure analysis by using specular reflection technique. High quality of the data was obtained by using this instrument. A new diffractometer for asymmetric diffraction experiment has also been developed by modifying the instrument for GID.
For quantitative analysis of thin-film structures, the use of parallel-beam geometry is essntially important, because the focusing (divergent-beam) geometry induces the degradation of diffraction profiles. Profiles in asymmetric diffraction were examined in both theory and experiment using synchrotron radiation parallel-beam geometry and pseudo-parallel-beam geometry in a laboratory system developed in the present project. It has been demonstrated that the present laboratory system is very useful for the quantitative study of thin-film structure analysis.
A computer software for analyzing grazing incidence diffraction patterns has been developed.

Report

(4 results)
  • 1993 Annual Research Report   Final Research Report Summary
  • 1992 Annual Research Report
  • 1991 Annual Research Report
  • Research Products

    (23 results)

All Other

All Publications (23 results)

  • [Publications] W.Parrish,C.Erikson,T.C.Huang,虎谷 秀穂: "X-ray Reflectometry of Single- and Multi-layer Thin Films" Proceedings Mat.Res.Soc.Symp.208. 327-337 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] N.Masciocchi,虎谷 秀穂,W.Parrish: "A Theta-Dependent Error Present in Powder Data of Highly Absorbing Materials:A Surface Roughness Effect?" Materials Science Forum. 79-82. 245-250 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] T.C.Huang,虎谷 秀穂,T.N.Blanton,Y.Wu: "X-ray Powder Diffraction Analysis of Silver Behenate,A Possible Low-Angle Diffraction Standard" J.Appl.Cryst.26. 180-184 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 虎谷 秀穂,T.C.Huang,Y.Wu: "Asymmetric Diffraction with Parallel-Beam Synchrotron Radiation" Advances in X-ray Analysis. 36. 609-616 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 虎谷 秀穂,T.C.Huang,Y.Wu: "Intensity Enhancement in Asymmetric Diffraction with Parallel-Beam Synchrotron Radiation" J.Appl.Cryst.26. 774-777 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 虎谷 秀穂: "種々の方法を用いた粉末回折図形のバックグラウンドの決定について" セラミックス研究施設年報. 3. 13-22 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] H.Toraya: ""The Determination of Background Level of Powder Diffraction Pattern Using Various Techniques"" Annual Rep.Ceramics Res.Lab.3. 13-22 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] H.Toraya, T.C.Huang, and Y.Wu: ""Intensity Enhancement in Asymmetric Diffraction with Parallel-Beam Synchrtron Radiation"" J.Appl.Cryst.26. 774-777 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] H.Toraya, T.C.Huang, and Y.Wu: ""Asymmetric Diffraction with Parallel-Beam Synchrotron Radiation"" Adv.X-ray Anal.36. 609-616 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] T.C.Huang, H.Toraya, T.N.Blanton, and Y.Wu: ""X-ray Powder Diffraction Analysis of Silver Behenate, a Possible Low-Angle Diffraction Standard"" J.Appl.Cryst.26. 180-184 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] N.Masciocchi, H.Toraya, and W.Parrish: ""A Theta-Dependent Error Present in Powder Data of Highly Absorbing Materials : A surface Roughness Effect ? " ed.by R.Delhez and E.J.Mittemeijer" Mat.Sci.Forum Trans Tech Publications, Zurich. 79-82. 245-250 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] W.Parrish, C.Erickson, T.C.Huang, M.Hart, B.Gilles, and H.Toraya: ""X-ray Reflectometry of Single-and Multi-Layr Thin Films"" Symp.Proc.Adv.Suface Thin Film Diffraction, Mat.Res.Soc.Pittsburgh. 208. 327-337 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] W.Parrish,虎谷 秀穂 etc.: "X-ray Reflectometry of Single-and Multi-layer Thin Films" Proceedings Mat.Res.Soc.Symp.208. 327-337 (1991)

    • Related Report
      1993 Annual Research Report
  • [Publications] Masciocchi,虎谷 秀穂 他1名: "A Theta-Dependent Error Present in Powder Data of Highly Absorbing Materials:A Surface Rousness Effect?" Materials Science Forum.79-82. 245-250 (1991)

    • Related Report
      1993 Annual Research Report
  • [Publications] T.C.Huang,虎谷 秀穂 他2名: "X-ray Powder Diffraction Analysis of Silver Behenate,A Possible Law Angle Diffraction Standard" J.Appl.Cryst.26. 180-184 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] 虎谷 秀穂、T.C.Huang 他1名: "Asymmetric Diffraction with Parallel-Beam Synchrotron Radiation" Advances in X-ray Analysis. 36. 609-616 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] 虎谷 秀穂、T.C.Huang 他1名: "Intensity Enhancement in Asymmetric Diffraction with Parallel-Beam" J.Appl.Cryst.26. 774-777 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] 虎谷 秀穂: "種々の方法を用いた粉末回折図形のバックグラウンドの決定について" セラミックス研究施設年報. 3. 13-22 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] H.Toraya.: "Asymmetvic Diffraction with Parallel-Beam Synchrotron Radiation" Adv.X-ray Anal.36. (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] 虎谷 秀穂: "擬似平行ビーム系を用いた非対称反射に関する研究"

    • Related Report
      1992 Annual Research Report
  • [Publications] W,Parrish.,C,Erikson.,T.C.Huang.,M.Hant.,B,Gills.,H,Toraya: "Xーray Reflectometry of Singleーand Multiーlayer thin Films" Mat.Res.Soc.Symp.Proc.208. 327-337 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] N,Masciocchi.,H.Toraya.,W,Pnrrish: "A・θーDependent Error Present in Powder Data of Highly Absorbing Materials" Mat.Sci.Forum. 79ー82. 245-250 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] H.Toraya.,W,Parrish: "A ccurate Defermination of UnitーCell Parameters using Conventional Xーray Powder Diffrattometing" Proc.Pacific.Int.Cong.Xーray,Anal.Meth. (1992)

    • Related Report
      1991 Annual Research Report

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Published: 1991-04-01   Modified: 2016-04-21  

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