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High-Quality Single Crystal Growth of Rare Earth Inter metallic compounds under Ultra-high vacuum

Research Project

Project/Area Number 03554006
Research Category

Grant-in-Aid for Developmental Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field 固体物性
Research InstitutionUniversity of Tsukuba

Principal Investigator

ONUKI Yoshichika  Univ. of Tsukuba Institute of Materials Science A. Prof., 物質工学系, 助教授 (40118659)

Co-Investigator(Kenkyū-buntansha) SATOH Kazuhiko  Univ. of Tsukuba Institute of Materials Science R. Associate, 物質工学系, 助手 (60225927)
Project Period (FY) 1991 – 1992
Project Status Completed (Fiscal Year 1992)
Budget Amount *help
¥4,100,000 (Direct Cost: ¥4,100,000)
Fiscal Year 1992: ¥1,000,000 (Direct Cost: ¥1,000,000)
Fiscal Year 1991: ¥3,100,000 (Direct Cost: ¥3,100,000)
KeywordsUltra-high vacuum / zone melting / Crystal Growth / Heavy Electrons / Rare Earth Compounds / CeRu_2Si_2 / LaRh_2
Research Abstract

We have constructed the zone-melting rf furnace under a ultra-high vacuum condition. An ingot of the rare earth compound is set on the boat-like Cu-hearth which is cooled by water. When this ingot passes through the rf working coil, it melts partially and grows as an single crystal.
(1)The single crystals of CeRu_2Si_2 were first grown by the tri-arc Chochralski pulling method in an argon gas atmosphere and were annealed at 1500゚C under a high vacuum of 1x10^<-8>torr for five hours. The residual resistivity ratio of the obtained sample was 250, indicating good quality of the crystal. By using this high-quality sample we have observed a super-heavy carrier with the large cyclotron mass 120m_0.
(2)We have also succeeded in growing a single crystal of LaRh_2 by a zone-melting method in the present furnace. The sweep-speed for zone-melting was 5mm/hr. An obtained single crystal ingot was about 5mm in diameter and 30mm in length. The Fermi surface of LaRh_2 was determined by the dHvA effect.

Report

(3 results)
  • 1992 Annual Research Report   Final Research Report Summary
  • 1991 Annual Research Report
  • Research Products

    (14 results)

All Other

All Publications (14 results)

  • [Publications] H.AOKI,S.UJI,A.Albessard and Y.ONUKI: "Observation of Heavy Electrons in CeRu_2Si_2 via the dHVA EHect" J.Phys.Soc.Jpn.61. 3457-3461 (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] K.SATOH et al.: "de Haas-san Alphen Effect in UGe_2" J.Phys.Soc.Jpn.61. 1827-1828 (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] Y.ONUKI: "Quantum Oscillatory Magnetization" Jpn.J.Apl.Phys. 8. 149-156 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] H.AOKI et al.: "dHVA Effect Study of Metamagnetic Transition in CeRu_2Si_2" J.Phys.Soc.Jpn.

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] H, Aoki, S. Uji A. K. Albessard and Y. Onuki: "Observation of Heavy Electrons in CeRu_2Si_2 via the dHVA Effect" J. Phys. Soc. Jpn.61. 3457-3461 (1992)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] K. Satoh, S. W. Yun, I. Umehara, Y. Onuki, S. Uji, T. Shimizu, H. Aoki: "de Haas-van Alphen Effect in UGe_2" J. Phys. Soc. Jpn.61. 1827-1828 (1992)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] Y. Onuki: "Quantum Oscillatory Magnetization" Jpn. J. Apl. Phys.8. 149-156 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] H. Aoki, S. Uji, A. K. Albessard and Y. Onuki: "dHVA Effect Study of Metamagnetic Transition in CeRu_2Si_2" J. Phys. Soc. Jpn.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1992 Final Research Report Summary
  • [Publications] H.Aoki et al.: "Observation of Heavy Electrons in CeRu_2Si_2 via the dHVA Effect" J.Phys.Soc.Jpn.61. 3457-3461 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] K.Satoh et al.: "de Haas-san Alphen Effect in UGe_2" J.Phys.Soc.Jpn.61. 1827-1828 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] Y.Onuki: "Quantum Oscillatory Magnetization" Jpn.J.Apl.Phys. 8. 149-156 (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] H.Aoki et al.: "dHVA Effect Study of Meta magnehc Transition in CeRu Si_2" J.Phys.Soc.Jpn.

    • Related Report
      1992 Annual Research Report
  • [Publications] Y.Onuki et al.: "Fermi Surface Properties of CeRu_2Si_2 and LaRu_2Si_2" to be published in J.Phys.Soc.Jpn.

    • Related Report
      1991 Annual Research Report
  • [Publications] 大貫 惇睦: "結晶成長ハンドブック" 共立出版, (1992)

    • Related Report
      1991 Annual Research Report

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Published: 1991-04-01   Modified: 2016-04-21  

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