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Development of viscometry of lubricants under very high pressure and elevated temperature by DAC and the evaluation and improvement of heavily loaded lubricants

Research Project

Project/Area Number 03555031
Research Category

Grant-in-Aid for Developmental Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field 機械要素
Research InstitutionMIE UNIVERSITY

Principal Investigator

FUJISHIRO Ikuya  Prof.MIE UNIVERSITY, Engineering, 工学部, 教授 (90023043)

Co-Investigator(Kenkyū-buntansha) SHIA Yoshiaki  Nippon Steel Co, 設備部, 係長
TAKEMOTO Masanori  Nippon Steel Co, 設備部, 部長代理
SAWA Masaaki  Nippon Steel Co, 設備部, 室長
NAKAMURA Yuichi  Assistant Prof., 工学部, 講師 (20164345)
Project Period (FY) 1991 – 1993
Project Status Completed (Fiscal Year 1993)
Budget Amount *help
¥13,200,000 (Direct Cost: ¥13,200,000)
Fiscal Year 1993: ¥900,000 (Direct Cost: ¥900,000)
Fiscal Year 1992: ¥4,100,000 (Direct Cost: ¥4,100,000)
Fiscal Year 1991: ¥8,200,000 (Direct Cost: ¥8,200,000)
KeywordsHigh pressure / Maintenance tribology / Lubricant / Elevated pemperature / Viscosity / Friction / Diamond-anvil cell / Wear / メインテナンストライボロジ-
Research Abstract

Abstracts of this research results are outlined as follows considering research schedule :
1). A fast pressure measuring system employing spectrometric multichannel analyzer and a falling viscometry system using a diamond-anvil cell (DAC) were developed. The measurement of a reference lubricant, DOS, resulted to agree with the data of ASME, and the possibility of Raman light scattering measurement by this system was confirmed
2). The pressure increment due to the restriction of thermal expansion of the liquid in DAC was measured up to an elevated temperature (200。C) by means of the viscosity measurements for the reference lubricant. And the temperature coefficient of ruby R_1 was also found to be 0.00641 nm/。C up to 120。C at 850 MPa. By using this, the viscosity of polyalphaolefine, PAO68, was obtained at elevated temperature under high pressure.
3). In laboratry test, the friction and wear characteristics were investigated employing a four-roller traction machine and ferrography with synthetic lubricants, PAO68, tar naphthene (TN68) and their blends. Friction coefficient was resulted to increase with the blend ratio of TN68. Viscosity measurement concluded that the friction coefficient was found to raise with the viscosity-pressure coefficient of lubricant. The blend oil of about 30% TN68 showed the maximum glass transition pressure which was similar to the results of 4-ball experiment. In steelworks, Contaminant controls such as an amorphous oil cleaner resulted to prevent machine troubles.
4). Viscosity measurement technique of tallow oils for metal sheet cold rolling was established, which show gel-like property so thus it is impossible to measure viscosity at room temperature. Viscosity of the tallow oils was measured up to 1 GPa and 180。C and phase transition was observed. Using these properties and elastohydrodynamics for rolling control, Improvement of troubles for rolling assemblies was examined.

Report

(4 results)
  • 1993 Annual Research Report   Final Research Report Summary
  • 1992 Annual Research Report
  • 1991 Annual Research Report
  • Research Products

    (38 results)

All Other

All Publications (38 results)

  • [Publications] 藤城郁哉、中村裕一、谷口和雅: "HYSTERESIS OF RUBY FLUORESCENT LINE BY PRESSURE AND ANNEALING EFFECT" High Pressure Research(Gordon and Breach Science Publishers). 6-5. 301-307 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 四阿佳昭、小野総: "製鉄所におけるコンタミナントコントロール" 潤滑経済(潤滑通信社). 317. 24-28 (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 竹本雅謙ほか: "新しい合成系作動油" 油空圧技術(日本工業出版). 31-2. 34-38 (1992)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 中村裕一、藤城郁哉、近藤英二、倉橋基文、竹本雅謙、四阿佳昭: "Traction Experiments and Lubricants' Properties at High Pressure in Maintenance Tribology" Proceedings of INTERNATIONAL SEMINAR ON MICROSTRUCTURES AND MECHANICAL PROPERTIES OF NEW ENGINEERING MATERIALS. 265-272 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 藤城 郁哉、中村 裕一: "ルビー蛍光法による圧力測定" 高圧力の科学と技術. 3-1. 87-88 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 藤城郁哉、中村裕一、山之口秀則: "Evaluation of Temperature Dependency on Ruby Fluorescence at High Pressure by Viscosity Measurement of Lubricants" Proceedings of Joint AIRAPT/APS Conference on High Pressure Science and Technology. (掲載予定).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 内山雄二、竹本雅謙、四阿佳昭、土井宏幸、大石直樹: "実践保全技術シリーズ(3)「潤滑技術」" 日本プラントメインテナンス協会, 263 (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 藤城郁哉、中村裕一ほか: "Current Japanese Materials Research,Vol.13" Elsevier(日本材料学会)(発行予定), 195 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Ikuya Fujishiro, Yuichi Nakamura and Kazumasa Taniguchi: "Hysteresis of Rudy Fluorescent Line by Pressure and Annealing Effect" High Pressure Research. 6. 301-307 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Yoshiaki Shia and Satoru Ono: "Contaminant Control at Steelworks" Junkatsu Keizai [in Japanese]. 317. 24-28 (1992)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Masanori Takemoto, Onoyama Masuhiro and Seiji Matsushita: "New Synthetic Hydraulic Oils" Yukuuatsu-Gijutsu [in Japanese]. 31-2. 34-38 (1992)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Y.Nakamura, I.Fujishiro, F.Ishibe, E.Kondoh, M.Kurahashi, M.Takemoto, and Y.Shia: "Traction Experiments and Lubricants' Properties at High Pressure in Maintenance Tribology" Proceedings of IMMM'93. 265-272 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Ikuya Fujishiro and Yuichi Nakamura: "Pressure Measurement by Ruby Fluorescence Method" The Review of High Pressure and Tech.[in Japanese]. 3-1. 87-89 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Ikuya Fujishiro, Yuichi Nakamura and Hidenori Yamanokuchi: "Evaluation of Temperature Dependence on Ruby Fluorescence at High Pressure by Viscosity Measurement of Lubricants" Proc.of Joint AIRAPT/APS Conf.(to be published).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Y.Uchiyama, M.Takemoto, Y.Shia, H.Doi and N.Ohichi: Lubrication Technology. Association of Jpn.Plant Maintenance, [in Japanese], 32-41(263) (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Ikuya Fujishiro and Yuichi Nakamura: Measurement of Viscoelastic Properties of Lubricants under High Pressure by DAC, Current Japanese Materials Research. Elsevier Vol.13 (to be published), 144-162(195) (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 四阿佳昭: "製鉄設備における油圧作動油の清浄度管理事例" 油空圧技術(日本工業出版). 31-2. 43-48 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] 近藤英二,中村裕一,藤城郁哉: "高温高圧力下における牛脂系圧延潤滑油の粘度測定" 第33回高圧討論会講演要旨集. 33. 438-439 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] 藤城郁哉,中村裕一,角田正幸: "Raman Scattering Measurements of Lubricants over Glass Transition Pressure" Proceedings of INTERNATIONAL SEMINAR ON MICROSTRUCTURES and MECHANICAL PROPERTIES OF NEW ENGINEERING MATERIALS. 257-264 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] 中村裕一、藤城郁哉、近藤英二、倉橋基文、竹本雅謙、四阿佳昭: "Traction Experiments and Lubricants′ Properties at High Pressure in Maintenance Tribology" Proceedings of INTERNATIONAL SEMINAR ON MICROSTRUCTURES and MECHANICAL PROPERTIES OF NEW ENGINEERING MATERIALS. 265-272 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] 藤城郁哉、中村裕一: "ルビー蛍光法による圧力測定" 高圧力の科学と技術. 3-1. 87-88 (1994)

    • Related Report
      1993 Annual Research Report
  • [Publications] 藤城郁哉、中村裕一、山之口秀則: "Evaluation of Temperature Dependency on Ruby Fluorescence at High Pressure by Viscosity Measurement of Lubricants" Proceedings of Joint AIRAPT/APS Conference on High Pressure Science and Technology(掲載予定). (1994)

    • Related Report
      1993 Annual Research Report
  • [Publications] 倉橋基文、四阿佳昭: "日本トライボロジー学会、第38回トライボロジー先端講座" 機械設備の寿命予測とトライボロジー, 91 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] 藤城郁哉、中村裕一ほか: "Current Japanese Materials Research,Vol.13" Elsevier(日本材料学会)(発行予定), 195 (1994)

    • Related Report
      1993 Annual Research Report
  • [Publications] 藤城 郁哉,中村 裕一: "MEASUREMENT OF VISCOELASTIC PROPERTIES OF LUBRICANTS UNDER HIGH PRESSURE BY DAC" Current Japanese Matereals Research. 13. (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] 藤城 郁哉,中村 裕一,山之口 秀則: "Evaluation Temperature Dependency on Ruby Fluoresccnce at High Pressure Viscosity Measurement of Lubricants" Proceedings of Joint AIRAPT/APS Conference on High Pressure Science and Technology. (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] 藤城 郁哉,中村 裕一,近藤 英二,矢崎 寿恵,倉橋 基文,竹本 雅謙,四阿 佳昭: "トラクション試験および潤滑油高圧物性とメインテナンストライボロジー" 日本機械学会東海支部三重地方講哀会講演論文集. 923-2. 161-164 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] 中村 裕一,藤城 郁哉,近藤 英二,倉橋 基文,竹本 雅謙,四阿 佳昭: "Traction Experiments and Lubricants′Ppoperties at High Pressure in Maintenance Tribology" Proceeding of INTERNATIONAL SEMINAR ON MICROSTRUCTURES AND MECHANICAL PROPERTIES OF NEW ENGINEERING MATERIALS. (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] 中村 裕一,藤城 郁哉,山之口 秀則: "潤滑油の粘度測定による高圧力下のルビー蛍光線の温戸依存性評価" 第33会高圧討論会講演要旨集. 14-15 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] 四文 佳昭,小野 総: "製鉄所におけるコンタミナントコントロール" 潤滑経済(潤滑通信社). 317. 24-28 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] 倉橋 基文,四阿 佳昭ほか: "第38回トライボロジー先端講座「機械設備の寿命予測とトライボロジー」" (社)日本トライポロジー学会, 82 (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] 石部 文和、後城 郁哉、中村 裕一: "ルビ-蛍光法による潤滑油の高圧力下での力学特性の評価とメインテナンストライボロジ-" 第32会高圧討論会講演要旨集. 228-229 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] 山之口 秀則、藤城 郁哉、中村 裕一: "高温のDAC中の圧力決定法と潤滑油の粘度測定" 第32会高圧討論会講演要旨集. 230-231 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] 藤城 郁哉、中村 裕一,谷口 和雅: "HYSTERESIS OF RUBY FLUORESCENT LINE BY PRESSURE AND ITS ANNEALING EFFECT" High Pressure Research(Gordon and Breach Science Publishers). 6-5. 301-307 (1991)

    • Related Report
      1991 Annual Research Report
  • [Publications] 竹本 雅謙 ほか: "新しい合成系作動油" 油空圧技術(日本工業出版). 31-2. 34-38 (1992)

    • Related Report
      1991 Annual Research Report
  • [Publications] 四阿 佳昭、土井 宏幸: "Development of Lubrication Control Technique for Improvement of Equipment Reliability" Proceedings of South East Asia Iron & Steel Institute in Manila Phillipines.

    • Related Report
      1991 Annual Research Report
  • [Publications] 藤城 郁哉、中村 裕一、近藤 英二、知崎 寿恵、倉橋 基文 竹本 雅謙、四阿 佳昭: "トラクション試験および潤滑油高圧物性とメインテナンストライボロジ-" 日本機械学会三重地方講演会講演論文集.

    • Related Report
      1991 Annual Research Report
  • [Publications] 内山 雄二、竹本 雅謙、四阿 佳昭, 土井 宏幸、大石 直樹: "実践保全技術シリ-ズ(3)「潤滑技術」" 日本プラントメインテナンス協会, 263 (1991)

    • Related Report
      1991 Annual Research Report

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Published: 1991-04-01   Modified: 2016-04-21  

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