| Project/Area Number |
03555147
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| Research Category |
Grant-in-Aid for Developmental Scientific Research (B)
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| Allocation Type | Single-year Grants |
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| Research Field |
金属加工(含鋳造)
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| Research Institution | Institute for Material Research |
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Principal Investigator |
INOUE Akihisa Institute for Materials Research, Tohoku University, Professor., 金属材料研究所, 教授 (10108566)
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| Co-Investigator(Kenkyū-buntansha) |
SAIDA Jyunji Nisshin Steel Co.Ltd., Researcher., 阪神研究所, 研究員
KATO Akira Toyota Motor Co., Researcher., 東富士研究所, 研究員
OGUCHI Masahiro Teikoku Piston Ring Co.Ltd., Assistant to Manager., 技術開発部, 主任研究員
KIMURA Hisamichi Institute for Materials Research, Tohoku University, Assistant., 金属材料研究所, 助手 (00161571)
TSAI An-Pang Institute for Materials Research, Tohoku University, Associate Professor., 金属材料研究所, 助教授 (90225681)
SHIMIZU Kouichi Furuawa Co.Ltd., Researcher
KONISHI Mikio Asahi Chemical Industry Co., Ltd., Researcher.
清水 宏一 古河機械金属株式会社, 電子材料本部, 研究員
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| Project Period (FY) |
1991 – 1993
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| Project Status |
Completed (Fiscal Year 1993)
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| Budget Amount *help |
¥16,600,000 (Direct Cost: ¥16,600,000)
Fiscal Year 1993: ¥1,600,000 (Direct Cost: ¥1,600,000)
Fiscal Year 1992: ¥1,700,000 (Direct Cost: ¥1,700,000)
Fiscal Year 1991: ¥13,300,000 (Direct Cost: ¥13,300,000)
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| Keywords | supercooled quenching method / supercooled liquid droplet / high pressure gas atomization method / two-stage quenching method / flaky powder / cobalt base alloy / titanium base alloy / zirconium base alloy / 過冷却液適 / 二段液体急冷法 / 冷却速度 / アモルファス粉末 / 超薄型高アスペクト比粉末 / 高圧ガス噴霧 / 過冷却微小液滴 / 末緩和構造 / 高速冷却能 / 高速回転体 |
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| Research Abstract |
In 1991, we constructed a two-stage rapid quenching equipment and determined appropriate conditions for the production of flaky amorphous powders with very thin thickness in Fe-, Co- and Ni-based alloys. Furthermore, we examined fundamental properties of thermal stability, corrosion resistance and magnetic properties for the flaky amorphous powders and clarified that the flaky amorphous powders have unique characteristics which were different from those for amorphous sheets and wires.
In 1992, we searched alloy systems and alloy compositions in which a large glass-forming ability leading to the formation of flaky amorphous powders is achieved in refractory Ti- and Zr-based alloy systems. Subsequetly, the production of flaky amorphous powders was tried for the above-described alloys and the most appropriate atomizing conditions were determined. We also examined the morphology, thermal stability and corrosion resistance of the flaky powders.and investigated the relation between the proper
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ties and the preparation process of the flaky amorphous powders in their refractory metal base alloys.
In 1993, the production of flaky amorphous powders was tried for Al-based alloys where the exfoliation of the powder from the rotating roter is difficult because of their low specfic weight and the production of the flaky amorphous powder is difficult. As a result, it was found that the modification of the surface state of the rotating roter enables a high production ratio of Al-based flaky amorphous powders. As similar for the Fe-, Co-, Ni-, Ti- and Zr-based amorphous powders with flaky morphology, the Al-based flaky powders also have the heat of structural relaxation which is about two times as large as those for the amorphous ribbons, indicating that the amorphous powders were produced at very large cooling rates.
In addition, we evaluated the characteristics of the Fe- and Co-based flaky amorphous powders as magnetic shielding materials as well as the Ti- and Al-based flaky amorphous powders as corrosion resistanct painting materials. As a result, it was confirmed that the flaky amorphous powders in Fe, Co, Ti and Al based systems produced by the two-stage quenching technique have the characteristics which are good enough to use practically as magnetic shielding and corrosion resistant painting materials because of their extremely thin form and their unique amorphous structure. Less
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