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Reliable High Pressure Technique for Material Synthesis.

Research Project

Project/Area Number 04044033
Research Category

Grant-in-Aid for international Scientific Research

Allocation TypeSingle-year Grants
SectionJoint Research
Research InstitutionInstitute of Materials Science, University of Tsukuba

Principal Investigator

WAKATSUKI Masao  Instutute of Materials Science, University of Tsukuba, Professor, 物質工学系, 教授 (50114153)

Co-Investigator(Kenkyū-buntansha) 洪 時明  成都科技大, 高温高圧物理研究所, 助教授
羅 湘捷  成都科技大, 高温高圧物理研究所, 助教授
丁 立業  成都科技大, 高温高圧物理研究所, 教授
〓 清泉  成都科技大, 高温高圧物理研究所, 教授
TOKUSHIGE Keinosuke  Technology Administration Division, Ishikawajima-Harima Heavy Industries, Ltd.,, 技術本部, 課長
KAGI Hiroyuki  Instutute of Materials Science, University of Tsukuba, Research Associate, 物質工学系, 助手 (70233666)
TAKANO Kaoru  Instutute of Materials Science, University of Tsukuba, Associate Professor, 物質工学系, 助教授 (60133005)
OHSUKA Kazuhiro  Instutute of Materials Science, University of Tsukuba, Professor, 物質工学系, 教授 (50029881)
SUENO Shigeho  Instutute of Earth Science, University of Tsukuba, Professor, 地球科学系, 教授 (30110513)
HONG Shiming  Instutute of High Temperature-High Pressure Physics, Chengdu University of Scien
LUO Xiaoxiao  Instutute of High Temperature-High Pressure Physics, Chengdu University of Scien
DING Liye  Instutute of High Temperature-High Pressure Physics, Chengdu University of Scien
GOU Qingquan  Instutute of High Temperature-High Pressure Physics, Chengdu University of Scien
こう 清泉  成都科技大, 高温高圧物理研究所, 教授
奥田 重雄  筑波大学, 物質工学系, 教授 (50111365)
Project Period (FY) 1992 – 1993
Project Status Completed (Fiscal Year 1993)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,900,000)
Fiscal Year 1993: ¥1,900,000 (Direct Cost: ¥1,900,000)
Fiscal Year 1992: ¥2,000,000 (Direct Cost: ¥2,000,000)
KeywordsHigh pressure apparatus / Anvils / Pressure medium / Hydraulic pressure control / Heating power control / Pressure evaluation / Temperature evaluation / Diamond synthesis
Research Abstract

Researches in this subject were performed for two years, 1992 and 1993. Cubic anvils designed in Chengdu University of Science and Technology (CUST) were applied successfully to the cubic anvil-type high pressure-high temperature apparatus designed and installed in University of Tsukuba (TU). The CUST-type anvils are effective in the mechanical stability of confining pressure (avoiding the "blowout" accident), though with a need for improvement of the design to raise the pressure efficiency a little. The pressure medium designed and produced in CUST was better than that used in TU conventionally, in showing improved stability of pressure and temperature because of having less thermal transformation undesirable.
The apparatus of CUST, applied with pressure and heating power controlling units designed and supplied by TU, showed a very improved stability and reproducibility in pressures and temperatures. The CUST apparatus was manifested to be used successfully in experiments of growing seed crystals of diamond from a carbon source of graphite at a small excess pressure. This growth process requires a very stable pressure for a long growth term.
Those results show improvement in experimental ability of the both universities and make one expect further development of finer experiments based on the co-operative characters of the both-type apparatuses.

Report

(2 results)
  • 1993 Final Research Report Summary
  • 1992 Annual Research Report
  • Research Products

    (48 results)

All Other

All Publications (48 results)

  • [Publications] M.Wakatsuki,K.J.Takano,H.Kagi and S.Kumagai: "Real-time evaluation of pressure using the pressure effect on emf of thermocouples." Proc.14th AIRAPT International Conf.on High Pressure Science and Technology,Colorado,1993. (in press). (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] W.Li,H.Kagi and M.Wakatsuki: "Growth of single crystals of diamond by a two-stage method." Proc.3rd IUMRS International Conference on Advanced Materials,Tokyo,1993. (in press). (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 若槻雅男: "金属溶媒によるダイヤモンド合成" New Diamond. 9. 4-13 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] K.J.Takano,K.Shino,A.Izawa,M.Miyahara and M.Wakatsuki: "Detection of pressure-induced phase transition in a diamond anvil cell." Japan.J.Appl.Phys.31(3A). 1268-1274 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] H.Kagi,M.Wakatsuki,S.Hayakawa,F.Nakamura,Y.Gohshi,H.Kanda and J.Isoya: "Characterization of trace nickel in Synthetic diamond and its relation ship to the abundance of substitutional nitrogen." Proc 14th AIRAPT International Conference on High Pressure Science and Technology,Colorado,1993. (in press). (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] H.Kagi,M.Wakatsuki,S.Hayakawa,Y.Gohshi,H.Kanda and J.Isoya.: "Trace amount of nickel in synthetic diamond and its implication to substitutional nitrogen." Proc.3rd IUMRS International Conference on Advanced Materials,Tokyo,1993. (in press). (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] K.Matsumoto,H.Yurimoto,K.Kosaka,T.Nakamura and S.Sueno: "A novel ion imager for secondary ion mass spectroscopy." Electron Devices. 40. 82-85 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] O.Koike,H.Yurimoto,H.Nagasawa and S.Sueno: "Ion microprobe measurements of Mg isotopes in type B1 CAI of Allende meteorite." Proc.NIPR Symp.Antarct.Meteorites.6. 357-363 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] K.Otsuka,T.Ohba,M.Tokonami and C.Wayman: "New description of long period stacking order structures of martensites in β-phase alloys." Scripta Met.29. 1359-1364 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Min Piao,K.Otsuka,S.Miyazaki and H.Hirokawa: "Mechanism of the As temperature increase by predeformation in thermo-electric alloys." Matrials Trans.JIM. 34. 919-929 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 〓立,張茹,洪時明,〓清泉: "用SiC和Ni_<70>Mn_<25>Co_5合金合成金剛石的試験" 高圧物理学報. 1993増巻号. 27 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 曹国英,陳叔〓,李会士,〓清泉: "八面体硼皮金剛石的高圧合成研究" 原子与分子物理学報. 10. 2603-2608 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 羅湘捷,丁立業,蔡民東,呉細芽: "人造金剛石鉄磁性雑質的EPR譜特性分析" 成都科技大学学報. 1993(6). 62-68 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 丁立業,若槻雅男,羅湘捷: "金剛石生長時高圧融剤中石炭的伝輸及其影響" 高圧物理学報. 8(in press). (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] S-M.Hong and M.Wakatsuki: "Diamond formation from the SiC-Co system under high pressure and high temperature." J.Mater.Sci.12. 283-285 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] S-M.Hong,W.Li,X-P.Jia and M.Wakatsuki: "Diamond formation from a system of Sic and a metal." Diamond and Related Materials.2. 508-511 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] M.Wakatsuki,K.J.Takano and H.Kagi: "Formation process of materials at high pressure:in New Functionality Materials,Vol.C,ed.by T.Tsuruta,M.Doyama and M.Seno" Elsevier,Amsterdam, 91-98 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] M.Wakatsuki, K.J.Takano, H.Kagi and S.Kumagai: "Real-time evaluation of pressure using the pressure effect on EMF of thermocouples" Proc. 14th AIRAPT International Conf. on High Pressure Science and Technology, Colorado, 1993. in press. (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Wei Li, H.Kagi and M.Wakatsuki: "Growth of single crystals of diamond by a two-stage method" Proc. 3rd IUMRS International Conference on Advanced Materials Tokyo, 1993. in press.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] M.Wakatsuki: "Synthesis of diamond using metallic solvents (in Japanese)" New Diamond. 9(4). 4-13 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] K.J.Takano, K.Shino, A.Izawa, M.Miyahara and M.Wakatsuki: "Detection of a pressure-induced phase transition in a diamond anvil cell" Japan. J. Appl. Phys.31(A). 1268-1274 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] H.Kagi, M.Wakatsuki, S.Hayakawa, F.Nakamura, Y.Gohshi, H.Kanda and J.Iasoya: "Characterization of trace nickel in synthetic diamond and its relationship to the abundance of substitutive nitrogen" Proc. 14th AIRAPT International Conf. on High Pressure Science and Technology, Colorado, 1993. in press. (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] H.Kagi, M.Wakatsuki, S.Hayakawa, Y.Gohshi, H.Kanda and J.Isoya: "Trace amount of nickel in synthetic diamond and its implication to substitutive nitrogen" Proc. 3rd IUMRS International Conference on Advanced Materials Tokyo, 1993. in press. (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] K.Matumoto, H.Yurimoto, K.Kosaka, T.Nakamura and S.Sueno: "A novel ion imagery for secondary ion mass spectroscopy" Electron Devices. 40. 82-85 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] O.Koike, H.Yurimoto, H.Nagasawa and S.Sueno: "Ion microprobe measurements of Mg isotopes in type B1 CAI meteorites" Proc. NIPR Antarct. Meteorites. 6. 357-363 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] K.Otsuka, T.Ohba, M.Tokonami and C.Wayman: "New description of long period stacking order structures of martensites in beta-phasealloys" Scripta Met.29. 1359-1364 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Min Piao, K.Otsuka, S.Miyazaki and H.Hirokawa: "Mechanism of the As temperature increase by pre-deformation in thermoelectric alloys" Materials Trans. JIM. 34. 919-929 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] L.Gou, J.Chang, S-M.Hong and Q-Q.Gou: "A trial of synthesizing diamond using SiC and a Ni_<70>Mn_<25>Co_5 alloy (in Chinese)" Chinese Journal of High Pressure Physics. special lssue. 27 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] G-Y.Cao, X-Q.Chen, H-S.Li and Q-Q.Gou: "Study for high pressure synthesis of octahedral diamonds surface-doped with boron (in Chinese)" Chinese Journal of Atomic and Molecular Physics. 10. 2603-2608 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] X-J.Luo, L-Y.Ding, M-D.Chai and X-Y.Wu: "The study of EPR properties of ferromagnetic impurities in synthetic diamond (in Chinese)" Journal of Chengdu University of Science and Technology. 1993(6). 62-68 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] L-Y.Ding, M.Wakatsuki and X-J.Luo: "Transport of carbon in the solvent and its effect on the formation of diamond (in Chinese)" Chinese Journal of High Pressure Physics. 8 in press. (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] S-M.Hong and M.Wakatsuki: "Diamond formation from the SiC-Co system under high pressure and high temperature" J.Mater.Sci.12. 283-285 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] S-M.Hong, W.Li, X-P.Jia and M.Wakatsuki: "Diamond formation from a system of SiC and a metal" Diamond and Related Materials. 2. 508-511 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] M.Wakatsuki, K.J.Takano and H.Kagi: Elsevier, Amsterdam. "Formation process of materials at high pressure", in New Functionality Materials, Vol.C, ed. by T.Tsuruta, M.Doyama and M.Seno, 91-98 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] K.J.TAKANO,K.SHINO.A.IZAWA,M.MIYAHARA and M.WAKATSUKI: "Detection of a pressure-induced phase transition in a diamond anvil cell." Japan.J.Appl.Phys.31. 1268-1274 (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] M.WAKATSUKI: "Some features of the grwth process of diamond at high pressure." Recent Trends in High Pressure Research,ed by A.K.Singh, Oxford & IBH Publishing Co., New Delhi,1992(Proc. 13th AIRAPT INT. Conf. on High Pressure Science and Technolgy, Bangalore, India, Oct., 1991). 671-675 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] Shi-Ming Hong,and M.Wakatsuki: "Diamond formation from Sic-Co system under high pressure and high temperature" J.Materials Science Letters. (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] Shi-Ming Hong,Wei Li, Xiao-Peng Jia dnd M.WAKATSUKI: "Diamond formation from a system of SiC cnd a metal." DIAMOND 1992(Proc.3rd Int.Conf.on the New Diamond Science and Technology, Aug. 31 - Sept.4,1992,Heidelberg, Germany). (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] 若規 雅男: "超高圧" 日本機械学会誌. 95. 868-869 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] H,MIZUBAYASHI,M.MORITA,T.KAKIHARA and S.OKUDA: "Anelastic study of screw dislocation motion in high purity miobium" Acta Metall.Mater.40. 2651-2659 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] H.TANIMOTO,H.MIZUBAYASHI,R.MASUDA,S.OKUDA,T.IWATA,H.TAKESITA and H.NARAMOTO: "Internal friction measurement of Mo after low-temperature 2MeV electron irradiation" Phys,stat,Sol.(a). 132. 353-360 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] H.MIZUBAYASHI,T.NARUSE and S.OKUDA: "Hydrogen internal friction peak in amorphous Cu_<50>Zr_<50>." Phys.stat.Sol.(a). 132. 79-90 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] K.MATSUMOTO,H.YURIMOTO,K.KOSAKA,T.NAKAMURA and S.SUENO.: "A novel ion imager for secondary ion mass spectrometry." Electron DEvices. 40. 82-85 (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] M.KUROSAWA,H.YURIMOTO,K.MATSUMOTO and S.SUENO: "Hydrogen analysis of mantle olivine by secondary ion mass spectrometry." Hige-Pressure Research in Mineral Physics:Application to Earth and Planetary Sciences. 283-287 (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] H.KAGI,Y.DOHMOTO,S.TAKANO and A.MASUDA: "Tetrad effect in lanthanide partitioning between calcium sulfate crystal and its saturated solution" Chemical Geology. in press. (1993)

    • Related Report
      1992 Annual Research Report
  • [Publications] H.KAGI,S.S.Russell C.T.Pillinger,K.TAKAHASHI and A.MASUDA: "Optical and isotopic properties of diamond in Ureilites." Extended Abstract on 17th Symposium on Antarctic Meteorites. 17. 989-91 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] 若規 雅男: "熱・圧力(実験化学講座4.日本化学会編)11,4,1項「高圧下の物質合成」担当(pp,490-497)," 丸善, 534 (1992)

    • Related Report
      1992 Annual Research Report
  • [Publications] T.Murae,H.kagi and A.Masuda(Ed.H.Oya): "Primitive Solar Nebula and Origin of Planets.(分担執筆)" TERRA Scientific Publishing Co.,Tokyo, 22 (1993)

    • Related Report
      1992 Annual Research Report

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Published: 1992-04-01   Modified: 2016-04-21  

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