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Experimental Studies on Micro-fracture Mechanics of High-Temperature Polymer Matrix Composites

Research Project

Project/Area Number 04452111
Research Category

Grant-in-Aid for General Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field Aerospace engineering
Research InstitutionThe University of Tokyo

Principal Investigator

TAKEDA Nobuo  Associate Professor Research Center for Advanced Science and Technology The University of Tokyo, 先端科学技術研究センター, 助教授 (10171646)

Project Period (FY) 1992 – 1994
Project Status Completed (Fiscal Year 1994)
Budget Amount *help
¥6,700,000 (Direct Cost: ¥6,700,000)
Fiscal Year 1994: ¥1,200,000 (Direct Cost: ¥1,200,000)
Fiscal Year 1993: ¥2,600,000 (Direct Cost: ¥2,600,000)
Fiscal Year 1992: ¥2,900,000 (Direct Cost: ¥2,900,000)
KeywordsHigh-temperature Polymer / Composite Materialss / Laminates / Transverse Crack / Delamination / In-situ Microscopic Observation / Damage Modeling / Damage Mechanism / モデリング / クロスプライ
Research Abstract

The pupose of the present investigation is to study experimentally the micro-fracture process and mechanism of high-temperarture polymer matrix composite laminates under quasi-static monotonic and repeated fatigue loadings. Three diffirent types of microscopes with displacement-rate-controlled loading devices were used for in-situ microscopic observations of damage initiation and growth. Cross-ply laminates were chosen as basic laminate configurations for high-performance carbon fiber reinforced high-temperature epoxy composites. The damage evolution includes the following three stages : (1)Transverse crack initiation in transverse layrs, (2)Multiple transverse crack formation, and (3)Initiation and growth of delamination from tips of transverse cracks. Based on the above quantitative experimental results, some new theoretical models were proposed to predict the damage evolution.
1. The tested CFRP materials include (1)a conventional 180゚C-cured TGDDM/DDS system (T300/3601), (2)an impro … More ved toughened system(T800H/3631), (3)an interlaminar-toughened system with interlaminar resin film layrs(T800H/3631-FM300), and(4)a new interlaminar-toughened system with nylon-particle-dispersed interlaminar layrs(T800H/3900-2). The laminate configurations were[0/90_n/0](n=4,8,12).
2. In-situ microscopic observations were successfully conducted by a combination of an optical microscope(OM), a scanning electron microscope (SEM), and a scanning acoustic microscope (SAM) with each loading stage. The microscopic deformation and failure processes such as, (1)transverse crack initiation in transverse layrs, (2)multiple transverse crack formation, and(3)initiation and growth of delamination from tips of transverse cracks, were observed at 20゚C and 80゚C to study the temperatue effects.
3. A new evolution law for transverse crack development was proposed based on the statistical strength distribution of 90゚layrs. A new evolution law for delamination from tips of transverse cracks was also proposed based on the energy balance concept. Both theoretical preditions were found to be sufficiently valid to explain the quantitative experimental results. An interaction between transverse cracks and delaminations was also considered for better prediction. These theories were also extended for fatigue-loaded specimens. Less

Report

(4 results)
  • 1994 Annual Research Report   Final Research Report Summary
  • 1993 Annual Research Report
  • 1992 Annual Research Report
  • Research Products

    (23 results)

All Other

All Publications (23 results)

  • [Publications] N.Takeda,S.Ogihara: "In Situ Observation and Probabilistic Prediction of Microscopic Failure Processes in CFRP Cross-Ply Laminates" Composites Science and Technology22GD01:52(2). 183-195 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] N.Takeda,S.Ogihara: "Initiation and Growth of Delamination from the Tips of Transverse Cracks in CFRP Cross-Ply Laminates" Composites Science and Technology.52(3). 309-318 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] 荻原慎二,武田展雄,島田卓也,小林昭: "CFRPクロスプラト積層板の疲労損傷進展特性" 強化プラスチックス. 40(1). 14-18 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] 志波光晴,武田展雄,岸輝雄: "CFRP積層板を伝播する疑似AE波の伝播特性" 日本複合材料学会誌. 20(3). 108-115 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] 志波光晴,武田展雄,岸輝雄: "CFRP積層板を伝播する類似AE波の圧電AE変換検出特性" 日本複合材料学会誌. 20(4). 137-143 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] N.Takeda,S.Ogihara,A.Kobayashi: "Experimental Micromechanical Approach to Failure Process in CFRP Cross-Ply Laminates" Proc.9th Tech.Conf.Am.Soc.Compos.23GE06:1994. 89-96

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] N.Takeda,S.Ogihara,A.Kobayashi: "Low-Cycle and High-Cycle Fatigue Failure Process Characterization of CFRP Cross-Ply Laminates" Proc.9th Tech.Conf.Am.Soc.Compos. 967-974 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] TAKEDA,Nobuo OGIHARA,Shinji: "Is Situ Observation and Probabilistic Prediction of Microscopic Failure Processes in CFRP Cross-ply Laminates" Composites Science and Tech. Vol.52, No.2. 183-195 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] TAKEDA,Nobuo OGIHARA,Shinji: "Initiation and Growth of Delamination from the Tips of Transverse Cracks in CFRP Cross-ply La" Composites Science and Techn. Vol.52, No.3. 309-318 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] OGIHARA,Shinji TAKEDA,Nobuo SHIMADA,Takuya KOBAYASHI,Akira: "Fatigue Damage Growth Properties of DFRP Cross-Ply Laminates (in Japanese)" Reinforced Plastics. Vol.40, No.1. 14-18 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] SHIWA,Mitsuharu TAKEDA,Nobuo KISHI,Teruo: "Acoustic Emission Wave Propagation Properties on CFRP Laminates by Using Simulated AE Source (in Japanese)" Journal of the Japan Society for Composite Materials. Vol.20, No.3. 108-115 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] SHIWA,Mitsuharu TAKEDA,Nobuo KISHI,Teruo: "Response Properties of Piezoelectric AE Sensor on CFRP Laminates by Using Simulated AE Source (in Japanese)" Journal of the Japan Society for Composite Materials. Vol.20, No.4. 137-143 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] TAKEDA,Nobuo OGIHARA,Shinji KOBAYASHI,Akira: "Experimental Micromechanical Approach to Failure Process in CFRP Cross-Ply Laminates" Proc.9th Tech.Conf.Am.Soc.Comp.89-96 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] TAKEDA,Nobuo.OGIHARA,Shinji.KOBAYASHI,Akira: "Low-Cycle and High-Cycle Fatigue Failure Process Characterization of CFRP Cross-Ply Laminates" Proc.9th Tech.Conf.Am.Soc.Comp.967-974 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] N.Takeda,S.Ogihara: "In Situ Observation and Probabilistic Prediction of Microscopic Failure Processes in CFRP Cross-Ply Laminates" Composites Science and Technology. 52(2). 183-195 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] N.Takeda,S.Ogihara: "Initiation and Growth of Delamination from the Tips of Transverse Cracks in CFRP Cross-Ply Laminates" Composites Science and Technology. 52(3). 309-318 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] 志波光晴,武田展雄,岸輝雄: "CFRP積層板を伝播する疑似AE波の伝播特性" 日本複合材料学会誌. 20(3). 108-115 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] 志波光晴,武田展雄,岸輝雄: "CFRP積層板を伝播する疑似AE波の圧電AE変換子検出特性" 日本複合材料学会誌. 20(4). 137-143 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] N.Takeda,S.Ogihara,A.Kobayashi: "Experimental Micromechanical Approach to Failure Process in CFRP Cross-Ply Laminates" Proc.9th Tech.Conf.Am.Soc.Compos.89-96 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] N.Takeda,S.Ogihara,A.Kobayashi: "Low-Cycle and High-Cycle Fatigue Failure Process Characterization of CFRP Cross-Ply Laminates" Proc.9th Tech.Conf.Am.Soc.Compos.967-974 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] 荻原慎二,武田展雄,島田卓也,小林昭: "CFRPクロスプライ積層板の疲労損傷進展特性" 強化プラスチックス. 40(1). 14-18 (1994)

    • Related Report
      1993 Annual Research Report
  • [Publications] N.Takeda,S.Ogiwara,A.Kobayashi: "In-situ Observation and Modelling of Micromechanical Failure Process in CFRP Cross-ply Laminates" Proc.9th Int.Comf.Comp.Mater.3. 351-358 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] N.Takeda,S.Ogiwara,T.Shimada,A.Kobayashi: "Microscopic Fatigue Damage Tolerance of CFRP Cross-ply Laminates" Proc.3rd Japan Int.SAMPE Symp.1. 433-438 (1993)

    • Related Report
      1993 Annual Research Report

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Published: 1992-04-01   Modified: 2016-04-21  

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