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Development of large-area Diamond Film Synthesis Apparatus by Chemical Vapor Deposition using Arc Discharge Plasma

Research Project

Project/Area Number 04555033
Research Category

Grant-in-Aid for Developmental Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field 機械工作
Research InstitutionTokyo Institute of Technology

Principal Investigator

HIRATA Atsushi (1993)  Tokyo Institute of Technology, Fuculty of Engineering Research Associate, 工学部, 助手 (50242277)

戸倉 和 (1992)  東京工業大学, 工学部, 助教授 (10016628)

Co-Investigator(Kenkyū-buntansha) YOSHIKAWA Masanori  Tokyo Institute of Technology, Fuculty of Engineering Professor, 工学部, 教授 (30016422)
大竹 尚登  東京工業大学, 工学部, 助手 (40213756)
Project Period (FY) 1992 – 1993
Project Status Completed (Fiscal Year 1993)
Budget Amount *help
¥12,000,000 (Direct Cost: ¥12,000,000)
Fiscal Year 1993: ¥1,500,000 (Direct Cost: ¥1,500,000)
Fiscal Year 1992: ¥10,500,000 (Direct Cost: ¥10,500,000)
KeywordsArc Discharge / Prasma / Diamond Film / Chemical Vapor Deposition / Deposition Area / Growth Rate / ダイヤモンド膜 / プラズマジェット / 高速合成 / 大面積
Research Abstract

In order to enlarge the diamond deposition area by arc discharge plasma jet chemical vapor deposition, a newly type of apparatus that has one cathode plasma torch and three anode plasma torches has been developed. These four plasma torch can be moved along their own axs, discharge area is changeable with changing the arrangement of the plasma torches. In this research, the possibility of the enlargement of the diamond deposition area by this appatatus has been discussed, and the growth rate, the film shape and properties of synthesized diamond films have been evaluated. Moreover, the mechanical properties of the diamond film has been characterized by applying the diamond film for cutting tool that was mode by YAG laser cutting technique and polishing technique by heat-chemical reaction with hot metal plate.
As a result, the diamond deposition area has been enharged at up to 40mm in diameter with increasing the discharge area when the pressure has been 200 Torr and methane concentration has been 4%. It is more effective for enlargement of the diamond deposition area to increase the discharge distance in the direction that is perpendicular to the axis of the plasma jet. The growth rate has been incerased with increasing the dischaege distance because the number of active species has increased. However, the film shape that central part is thicker has not changed when the discharge distance has been varied. Moreover, the crystallinity of the diamond film was characterized by Raman spectroscopy and it has been found that good crystallinity has been obtained independent of the arrangement of the plasma torches.
The diamond film has been shaped into a cutting edge and cutting of aluminum alloy was performed. The result of the experiments shows that the this CVD diamond film can be usued for ultraresicion cutting tool and has the same mechanical strength as natural diamond.

Report

(3 results)
  • 1993 Annual Research Report   Final Research Report Summary
  • 1992 Annual Research Report
  • Research Products

    (16 results)

All Other

All Publications (16 results)

  • [Publications] 平田敦,吉川昌範: "1陰極-3陽極アーク放電プラズマによる大面積ダイヤモンド膜合成装置の試作" 精密工学会誌. 59. 838-843 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 平田敦,吉川昌範: "生成ダイヤモンド膜に及ぼすアーク放電プラズマジェットCVD装置の電極位置の影響" 精密工学会誌. (印刷中).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] A.HIRATA,M.YOSHIKAWA: "Enlargement of The Diamond Deposition Area by one-cathode three-anode Arc Discharge Plasma Jet Chemical Vapor Deposition" Diamond and Related Materials. 2. 1402-1408 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] A.HIRATA,M.YOSHIKAWA: "Effects of Process Pressure on Diamond Growth by Arc Discharge Plasma Jet CVD Method" 2nd Int.Conf.on the Applications of Diamond Films and Related Materials. 469-474 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] M.YOSHIKAWA: "Application of CVD Diamond Chips for Ultraprecision Cutting Tools" 2nd Int.Conf.on the Applications of Diamond Films and Related Materials. 555-558 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Atsushi HIRATA and Masanori YOSHIKAWA: "Development of 1cathode-3anode Arc Discharge Plasma Apparatus for Enlargement of Diamond Deposition Area" Journal of the Japan Society for Precision Engineering. Vol.59-No.5. 838-843 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Atsushi HIRATA and Masanori YOSHIKAWA: "Effects of Electrodes Arrangement of Arc Discharge Plasma Jet CVD Apparatus on Diamond Films" Journal of the Japan Society for Precision Engineering. (in printing).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Atsushi HIRATA and Masanori YOSHIKAWA: "Enlargement of The Diaomond Deposition Area by one-cathode three-anode Arc Discharge Plasma Jet Chemical Vapor Deposition" Diamond and Related Materials. Vol.2. 1402-1408 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Atsushi HIRATA and Masanori YOSHIKAWA: "Effects of Process Pressure on Diamond Growth by Arc Discharge Plasma Jet CVD Method" 2nd International Conference on the Applications of Diamond Films and Related Materials. 469-474 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] Masanori YOSHIKAWA: "Application of CVD Diamond Chips for Ultraprecision Cutting Tools" 2nd International Conference on the Applications of Diamond Films and Related Materials. 555-558 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1993 Final Research Report Summary
  • [Publications] 平田敦,吉川昌範: "1陰極-3陽極アーク放電プラズマによる大面積ダイヤモンド膜合成装置の試作" 精密工学会誌. 59. 838-843 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] 平田敦,吉川昌範: "生成ダイヤモンド膜に及ぼすアーク放電プラズマジェットCVD装置の電極位置の影響" 精密工学会誌. (印刷中).

    • Related Report
      1993 Annual Research Report
  • [Publications] A.HIRATA and M.YOSHIKAWA: "Enlargement of The Diamond Deposition Area by one-cathode three-anode Arc Discharge Plasma Jet Chemical Vapor Deposition" Diamond and Related Materials. 2. 1402-1408 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] A.HIRATA and M.YOSHIKAWA: "Effects of Process Pressure on Diamond Growth by Arc Discharge Plasma Jet CVD Method" 2nd Int.Conf.on the Applications of Diamond films and Related Materials. 469-474 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] T.TATAMI,T.YASUHARA and M.YOSHIKAWA: "Application of CVD Diamond Chips for Ultraprecision Cutting Tools" 2nd Int.Conf.on the Applications of Diamond films and Related Materials. 555-558 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] 吉川 昌範: "1陰極-3陽極アーク放電プラズマジェットCVD装置によるダイヤモンドの合成" 第6回ダイヤモンドシンポジウム講演要旨集. 104-105 (1992)

    • Related Report
      1992 Annual Research Report

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Published: 1992-04-01   Modified: 2016-04-21  

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