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The study on the adhesive durability of dental restorative composite resins by new testing mthod

Research Project

Project/Area Number 04671154
Research Category

Grant-in-Aid for General Scientific Research (C)

Allocation TypeSingle-year Grants
Research Field Conservative dentistry
Research InstitutionTokyo Medical and Dental University

Principal Investigator

HUKUDA Hideaki  Tokyo Med.Dent.Univ., Inst.Med.Dent.Enging., Researcher, 医用器材研究所, 助手 (50014163)

Co-Investigator(Kenkyū-buntansha) NAGAI Masahiro  Tokyo Med.Dent.Univ., Inst.Med.Dent.Enging., Researcher, 医用器材研究所, 助手 (10013971)
TAKAKUDA Kazuo  Tokyo Med.Dent.Univ., Inst.Med.Dent.Enging., Asso.Prof., 医用器材研究所, 助教授 (70108223)
MIYAIRI Hiroo  Tokyo Med.Dent.Univ., Inst.Med.Dent.Enging., Professor, 医用器材研究所, 教授 (50013892)
Project Period (FY) 1992 – 1994
Project Status Completed (Fiscal Year 1994)
Budget Amount *help
¥2,100,000 (Direct Cost: ¥2,100,000)
Fiscal Year 1994: ¥500,000 (Direct Cost: ¥500,000)
Fiscal Year 1993: ¥900,000 (Direct Cost: ¥900,000)
Fiscal Year 1992: ¥700,000 (Direct Cost: ¥700,000)
Keywordscomposite resin / bovine tooth / adhesive shear strength / push-out shear test / adhesive durability / pulsating fatigue / measuring for marginal leakage / adhesive interface / 接着耐久性試験 / せん断強さ / 疲れ強さ / 辺縁封鎖性 / 光重合レジン / 化学重合レジン / 接着強さ / 疲労試験 / 打ち抜き試験 / はく離 / 臼歯用コンポジットレジン / クリープ試験 / 一定荷重 / 耐久試験
Research Abstract

The adhesive shear strength and the adhesive durability of chemically cured type (CCT) and light cured type (LCT) of dental restorative composite resins were comparatively investigated. The test specimen cut from different locations on bovine tooth, cylindrical cavities 5mm in diameter were prepared and then filled with each composite resin. The test for adhesive shear strength was done using the push-out shear test method developed by the authors. The adhesive durability test of which the test specimen was the cavity with bottom was done by pulsating fatigue test in the conditions of load amplitudes of 50N and 100N,frequency of 1Hz and cycles of one handred thousand times, and then the adhesive durability was evaluated by measuring a marginal leakage. The following are major results :
1. Push-out shear test In test specimens of all types, adhesive strengths of LCT resin were higher than those of CCT resin. Adhesive strength of Types I and II (dentin) were similar, consequently, it is difficult to positively confirm the anchoring effect of dentinal tubules by resin tags. And their strengths were much lower than those Type IV (enamel). Type III (enamel/dentin) showed an intermediate value between the strength of Type I and IV.In the test specimen of Type III,debonding was observed on the adhesive interface of the dentin layr by SEM photo.
2. Adhesive durability test In test specimen for enamel/dentin after pulsating test the marginal leakage was verified, threfore, the repeated loading seemed to cause the debonding at a margin part. In adhesive interface of the composite resin/enamel the debonding was also observed from SEM photo.
Such the shear test methods appear to be useful in evaluting the adhesive properties of composite resin for dental use.

Report

(4 results)
  • 1994 Annual Research Report   Final Research Report Summary
  • 1993 Annual Research Report
  • 1992 Annual Research Report
  • Research Products

    (9 results)

All Other

All Publications (9 results)

  • [Publications] 福田秀昭: "修復用コンポジットレジンの特性と評価-打ち抜きせん断試験による強度特性-" 歯科材料・器械. 12-SI,22. 178-179 (1993)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] 福田秀昭: "修復用コンポジットレジンの接着特性-疲労試験による評価-" 歯科材料・器械. 13-SI,23. 120-121 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] Miyairi,Hiroo: "ABSTRACT BOOK-Inter.Adhesion Symposium in Japan" 103-104 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] Hukuda, H.: "Adhesive Properties of restorative composite resins-Evaluation by push-out shear test" J.J.Dent.Mater.12-SI.22. 178-179 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] Hukuda, H.: "Adhesive Properties of restorative composite resins-Evaluation by fatigue test" J.J.Dent.Mater.13-SI.23. 120-121 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] Miyairi, H.: "Adhesive Properties of dental restorative composite resins by push-out shear test" ABSTRACT BOOK-Inter.Adhesion Symposium in Japan. 103-104 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] 福田秀昭: "修復用コンポジットレジンの接着特性-疲労試験による評価-" 歯科材料・器械. 13. 120-121 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] 福田秀昭: "修復用コンポジットレジンの特性と評価" 歯科材料・器械. 12. 178-179 (1993)

    • Related Report
      1993 Annual Research Report
  • [Publications] 福田秀昭: "歯科用コンポジットレジンの接着耐久性に関する研究" 日本接着学会. 123-124 (1993)

    • Related Report
      1993 Annual Research Report

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Published: 1992-04-01   Modified: 2016-04-21  

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