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Construction of a Positron Lifetime Spectrometer with beta^+-gamma coincidence for in-situ studies of lattice Defect

Research Project

Project/Area Number 05555167
Research Category

Grant-in-Aid for Developmental Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field Physical properties of metals
Research InstitutionKYOTO UNIVERSITY

Principal Investigator

SHIRAI Yasuharu  Kyoto University Dept.of Materials Science and Technology, Associate Professor, 工学部, 助教授 (20154354)

Co-Investigator(Kenkyū-buntansha) NISHITANI Shigeto  Kyoto University Department of Materials Science and Technology, Instructor, 工学部, 助手 (50192688)
Project Period (FY) 1993 – 1994
Project Status Completed (Fiscal Year 1994)
Budget Amount *help
¥3,700,000 (Direct Cost: ¥3,700,000)
Fiscal Year 1994: ¥700,000 (Direct Cost: ¥700,000)
Fiscal Year 1993: ¥3,000,000 (Direct Cost: ¥3,000,000)
KeywordsPositron Annihilation / Lattice Defects / Metals / Intermetallics / 金属間化合物 / 高温熱平衡測定
Research Abstract

Positron lifetime spectrometry has been successfully applied to the studies of atomicscale defects in solids. The conventional positron source in the lifetime measurements is ^<22>Na. The positron emission is accompanied by a suitable start signal, the 1.28MeV photon from de-excitation of the resulting ^<22>Ne nucleus. The positron source is usually prepared by evaporating a few microcuries of aqueous ^<22>NaCl onto a thin metal or plastic foil (typically 1 mg cm^<-2>) and covering it with the same foil. The source is then sandwiched by two identical pieces of sample material.
However, it is quite difficult or almost impossible to carry ont lifetime measurements at high temperatures or under high pressures with the sandwich configulation. We, therefore, constructed a new positron lifetime spectrometer adopting the beta^+-gamma coincidence technique which uses positrons themselves for supplying the start signal. Positrons give a start signal to the coincidence circuit when they pass a positron detector, which consists of a thin plastic scintillator connected with a light guide to a fast photomultiplier. The positrons passed through the start detector are guided and implanted into a sample marterial. The whole apparatus is desk-top. The time resolution of the whole system is about 300ps (FWHM) as yet, which is worse than that of the conventional gamma-gamma coincidence method but is better than any former beta^+-gamma coincidence lifetime spectrometers in the world.

Report

(3 results)
  • 1994 Annual Research Report   Final Research Report Summary
  • 1993 Annual Research Report
  • Research Products

    (11 results)

All Other

All Publications (11 results)

  • [Publications] 白井 泰治 他: "格子欠陥その場測定のためのエネルギー選別型β^+-γ同時計測陽電子寿命測定装置の試作" 日本金属学会誌. 59. 679-680 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] 白井 泰治: "陽電子ビームによる材料+'構造欠陥非破壊分析装置の開発" 生産技術誌. 48. 50-52 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] Y.Shirai, M.Sakamura, I.Shishido and M.Yamaguchi: J.Japan lnst.Metals. Vol.59. 679-80 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] Y.Shirai: The Production and Technique. Vol.48. 50-52 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1994 Final Research Report Summary
  • [Publications] Y.Shirai: "Vacancies and their properties in L1_2Al_<67>Mn_8Ti_<25> studied by positron lifetime spectroscopy" Intermetallics. 2. 221-224 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] Y.Shirai: "Construction and performance of a slow positron beam guided by a increasing magnetic field" Applied Surfase Science. 85. 138-142 (1995)

    • Related Report
      1994 Annual Research Report
  • [Publications] Y.Shirai: "Positron lifetime study of vacancies in CoSi_2" Materials Science Forum. (in press). (1995)

    • Related Report
      1994 Annual Research Report
  • [Publications] Y.Shirai: "Vacancies and their clusters in Ti_3Al studied by positron lifetime spectroscopy" Intermetallics. (in press). (1995)

    • Related Report
      1994 Annual Research Report
  • [Publications] Y.Shirai: "Radiation damage and the recovery of neutron-irradiated TiAl" Intermetallics. (in press). (1995)

    • Related Report
      1994 Annual Research Report
  • [Publications] 白井泰治: "陽電子計測の科学" 丸善,東京, 175 (1993)

    • Related Report
      1994 Annual Research Report
  • [Publications] Y.Shirai: "Physical Metallurgy and Processing of Intermetallic Compounds,ed.N.S.Stoloff" Chapmann and Hall,New York, 656 (1995)

    • Related Report
      1994 Annual Research Report

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Published: 1993-04-01   Modified: 2016-04-21  

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