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Mechanism of fluxing action for brazing titanium

Research Project

Project/Area Number 05671615
Research Category

Grant-in-Aid for General Scientific Research (C)

Allocation TypeSingle-year Grants
Research Field 補綴理工系歯学
Research InstitutionHokkaido University

Principal Investigator

OHKAWA Shoji  Hokkaido Univ. Dent. Instructor, 歯学部, 助手 (40001945)

Project Period (FY) 1993 – 1994
Project Status Completed (Fiscal Year 1994)
Budget Amount *help
¥2,100,000 (Direct Cost: ¥2,100,000)
Fiscal Year 1994: ¥400,000 (Direct Cost: ¥400,000)
Fiscal Year 1993: ¥1,700,000 (Direct Cost: ¥1,700,000)
KeywordsFlux / Brazing / Soldering / Spreading / Fluxing / チタン / ろう付
Research Abstract

The cumulative weigt loss of titanium in melt fluxes was measured at 900゚C using (1) 100%LiF,(2) 100%KHF_2, (3) 70%KHF_2-30%LiF,(4) 50%KHF_2-50%LiF-, (5) 56%KHF_2-14%LiF30%NaCl・KCl, (6) 100%NaCl・KCl. The component of NaCl・KCl contained 50%NaCl and 50%KCl by weight. The element distribution in spreading of Ag solder on titanium with 50%KHF_2-50%LiF was analyzed by EPMA,after heating for 25,35,45, and 75sec at 800゚C.
The results were as folows.
1. The cumulative weigt loss of titanium increased with pssing times.
2. The reactivity of fluxes increased in order of (6), (5), (4), (3), (2), (1).
3. The degree of spreading of Ag solder did not always coincide with the reactivity of fluxes.
4. The front of edge of spreading was rich in Cu and poor in Ag for all heating times.
5. Solder near interface with Ti was rich in Cu and Ti for 25 and 35 sec heating.
6. The upper part of solder inside the front of edge of spreading was rich in Ag and the lower part poor in Ag for 45 and 75sec heating, whereas the upper was poor in Ti and the lower part was rich in Ti.

Report

(3 results)
  • 1994 Annual Research Report   Final Research Report Summary
  • 1993 Annual Research Report

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Published: 1993-04-01   Modified: 2016-04-21  

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