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Application of N-hydroalkylacrylamide monomers for dentin primers

Research Project

Project/Area Number 05671651
Research Category

Grant-in-Aid for General Scientific Research (C)

Allocation TypeSingle-year Grants
Research Field 補綴理工系歯学
Research InstitutionFukuoka Dental College

Principal Investigator

FUKUSHUMA Tadao  Fukuoka Dental College, Associate professor, 歯学部, 助教授 (80084250)

Co-Investigator(Kenkyū-buntansha) KAWAGUCHI Minoru  Fukuoka Dental College, Research associate, 歯学部, 助手 (10122780)
Project Period (FY) 1993 – 1995
Project Status Completed (Fiscal Year 1995)
Budget Amount *help
¥2,100,000 (Direct Cost: ¥2,100,000)
Fiscal Year 1995: ¥400,000 (Direct Cost: ¥400,000)
Fiscal Year 1994: ¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 1993: ¥1,100,000 (Direct Cost: ¥1,100,000)
KeywordsDentinprimer / Bond strength / Dentin / Etchingagent / Composite resin
Research Abstract

The dentin primers containing N-hydroalkylacrylamide (N-HA) monomers { (N-methlolacryamide (MEAA), N-methylolmethacrylamide (MEMA), N- (2-hydroxyethyl) acrylamide (EAA), N- (2-hydroxyethyl) methacrylamide (EMA), N- (2,3-dihydroxypropyl) acrylamide (DAA), N- (2,3-dihydroxypropyl) methacrylamide (DMA) } were prepared in order to improve the bond strength of composite resin to etched dentin. The bond strength of composite resins with dentin primers to dentin etched with 10% citric acid-3% ferric chloride and EDTA solutions, and 10% maleic acid and 10% phosphoric acid gels was measured after 1-day, 1-year and 2-year immersion in 37゚C water or after thermal stress (4゚C*60゚C,20 * 10^3 and 50 * 10^3 cycles). The relationship between the chemical structures of N-HA monomers and dentin primer treatment capability was investigated. The dentin primers containing about 50% N-HA monomers showed better dentin primer treatment capability and improved the bond strength. N-HA monomers with acrylic group and short methylene chains showed better dentin primer treatment capability than the others, including HEMA and Glycery methacrylate. The highest bond strengths after 1-year and 2-year immersion in water and thermal stress were obtained with 50% MEAA followed by 30% MEMA and 35% HEMA dentin primers.

Report

(4 results)
  • 1995 Annual Research Report   Final Research Report Summary
  • 1994 Annual Research Report
  • 1993 Annual Research Report
  • Research Products

    (5 results)

All Other

All Publications (5 results)

  • [Publications] 福島忠男: "N-ハイドロアルキルメタクリルアミドのデンチンプライマーへの応用" 歯科材料・器械. 13. 397-402 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Tadao Fukushima: "Effect of dentin primers containing N-methylolacrylamide or N-methylolmethacrylamide on dentin treatment" Dental Materials.

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Tadao Fukushima: "Application of N- (Hydroxyalkyl) Methacrylamides for Dentin Primer" J J Dent Mater. Vol 13. 397-402 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Tadao Fukushima: "Effectof dentin primers containing N-methaylolacrylamide or N-methylolmethacrylamide on dentin treatment" Dental Materials.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 福島忠男,井口勇介,川口稔,宮崎光治: "N-ハイドロアルキルメタクリルアミドのデンチンプライマーへの応用" 歯科材料・器械. 13. 398-402 (1994)

    • Related Report
      1994 Annual Research Report

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Published: 1993-04-01   Modified: 2016-04-21  

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