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Development of scanning micro-evaporator for the study of SiGeC

Research Project

Project/Area Number 06402024
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Applied materials science/Crystal engineering
Research InstitutionTokyo Institute of Technology

Principal Investigator

TAKAYANAGI Kunio  TIT,Graduate school, Dept.of materials & Engineering, Professor, 大学院・総合理工学研究科, 教授 (80016162)

Co-Investigator(Kenkyū-buntansha) OSHIMA Yoshifumi  TIT,Graduate school, Dept.of materials & Engineering, Assistant, 大学院・総合理工学研究科, 助手 (80272699)
HIRAYAMA Hiroyuki  TIT,Graduate school, Dept.of materials & Engineering, A.Professore, 大学院・総合理工学研究科, 助教授 (60271582)
Project Period (FY) 1994 – 1996
Project Status Completed (Fiscal Year 1996)
Budget Amount *help
¥36,300,000 (Direct Cost: ¥36,300,000)
Fiscal Year 1996: ¥2,300,000 (Direct Cost: ¥2,300,000)
Fiscal Year 1995: ¥5,800,000 (Direct Cost: ¥5,800,000)
Fiscal Year 1994: ¥28,200,000 (Direct Cost: ¥28,200,000)
Keywordsdensity-modulated super lattice / scanning tunneling microscopy / micro-evaporator / 不整合超格子 / STM / 電界蒸発 / 走査型マイクロ蒸発源 / 密度変調・歪整合型格子 / 超高真空電子顕微鏡
Research Abstract

In recent years deivice sizes hve been decreased to nano-meter scale dimensions, and mesoscopic properties of electrons have come to be important. In these devices, it is certainly important to controle the electron scattering at the interfaces. The defects at the interface interfare the phase of the electorons and afect the electron transport in the devices. In this research we have aimed to develop a miniaturized evaporator to make a well defined nano-stuructures on atomically flat surfaces, to see any effect of the electron transport from the nano-structures.
We designed a specific specimen holder for nano-structure fablication. The specimen holder has a miniaturized STM,on top of which an evaporant can be attached, and a specimen faced to the STM tip. The specimen holder is used for the ultra-high vacuum electron microscope (UHV-EM) to observe any nano-structures formed on the specimen surface.
We used a silicon crystal as a substrate and a tungsten tip as an evaporant. When the tip was approached to the sample surface so close as 1 nm, and field of a few eV was applied between the tip and the sample, we found that a tungsten droplet was desorped from the tip side to be deposited on the substarte. This field evaporation technique for a micro-area deposition to produce nano-wires on the silicon surface was found to be not enough to wires of uniform thickness, because of poor controle of the field strength on the tungsten tip.
Anyway, we have succeeded to approach the evaporant to a sumple surface as close as a few nm, the approaching process being observed directly by electron microscopy. The scanning capability of the evaporant by STM allow us to form nano-structures, which are also observable by reflection electron microscopy.
The present reseach showed a possibility of nano-scale fablication on an atomically flat and clean surface.

Report

(4 results)
  • 1996 Annual Research Report   Final Research Report Summary
  • 1995 Annual Research Report
  • 1994 Annual Research Report
  • Research Products

    (25 results)

All Other

All Publications (25 results)

  • [Publications] Y.Naitoh, K.Takayanagi and M.Tomitori: "Visualization of Tip-Surface Geometry at Atomic distance by TEM-STM Holder" Surface Science. 357-358. 208-212 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] W-S.Cho, E.Hamada, Y.Kondo,and K.Takayanagi: "Synthesis of carbon nanotubes from bulk polymer" Applied Physics Letters. 69. 278-279 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Q.Ru, M.Okamoto, Y.Kondo,and K.Takayanagi: "Attraction and Orientation Phenomena of Bulcky Onions Formed in a Transmission Electron Microscope" Chemical Physics Letters. 259. 425-431 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] M.Okamoto, K.Hashimoto,and K.Takayanagi: "Cube-octahedral B12 clusters in silicon crystal" Applied Physics Letters. 70. 978-980 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] K.Takayanagi, Y.Naitoh, Y.Oshima and M.Mitome: "Surface Transmission Electron Microscopy on Structures with Truncation" Sruface Review and Letters. 4. 687-694 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] K.Takayanagi, Y.Okamoto, Q.Ru ,H.Onishi and M.Okamoto: "UHV-HRTEM of Reconstructed Nano-Structure Surface" Journal of Surface Analysis. 3. 228-232 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Y.Oshima and K.Takayanagi: "Variation of Surface Morphology of Tin Particles Observed by UHV High-resolution TEM" Surface Review and Letters. 3 (1). 1199-1203 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T.Onozawa and K.Takayanagi: "A-15 Type Structure of Ultra Fine Cr particles studied by UHV-HRTEM" Surface Science. 357-358. 228-232 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Y.Naitoh, K.Takayanagi and M.Tomitori: "Visualization of Tip-Surface Geometry at Atomic distance by TEM-STM Holder" Surface Science. 357-358. 208-212 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] M.Mitome and K.Takayanagi: "Optimum Condition of Convergent Beam Illumination for observation of local structure by high resolution transmission electyron microscopy" Ultramicroscopy. 62. 123-131 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Y.Oshima, K.Takayanagi and H.Hirayama: "Structural Anomaly of Fine Bismuth Particles observed by Ultra High-Vacuum TEM" Z.Phys D. 40. 534-538 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] W-S.Cho, E.Hamada, Y.Kondo, and K.Takayanagi: "Synthesis of carbon nanotubes from bulk polymer" Applied Physics Letters. 69. 278-279 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Q.Ru, M.Okamoto, Y.Kondo, and K.Takayanagi: "Attraction and Orientation Phenomena of Bulcky Onions Formed in a Transmission Electron Microscope" Chmical Physics Letters. 259. 425-431 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] M.Okamoto, K.Hashimoto, and K.Takayanagi: "Cube-octahedral B12 clusters in silicon crystal" Applied Physics Letters. 70. 978-980 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] W-S.Cho, E.Hamada, Y.Kondo, and K.Takayanagi: "Stacking faults in BaTiO3 particles synthesized from organic precursor" Journal of Applied Physics. 81. 3000-3002 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] K.Takayanagi, Y.Naitoh, Y.Oshima and M.Mitome: "Surface Transmission Electron Microscopy on Structures with Truncation" Sruface Review and Letters. 4. 687-694 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] K.Takayanagi, Y.Okamoto, Q.Ru, H.Onishi and M.Okamoto: "UHV-HRTEM of Reconstructed Nano-Structure Surface" Journal of Surface Analysis. 3. 228-232 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] 内藤賀公,高柳邦夫,富取正彦: "Visualization of Tip-surface geometry at atomic distance by TEM-STM holder" Surface Science. 357-358. 208-212 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] 溜正則,高柳邦夫: "Optimum Condifion of conrergent beam illumination for observation of local structure by high-resolution TEM" Ultramicroscopy. 62. 123-131 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] T. Onozawa: "A-15 Type Structure of Ultra Fine Cr particles studied by UHV-HRTEM" Surface Science. (in press). (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] Y. Naitoh: "Visualization of Tip-Surface Geometry at Atomic distance by TEM-STM Holder" Surface Science. (in press). (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] K. Takayanagi: "Surface Transmission Electron Micoescopy: Structures with Truncation" Surface Review and Letters. (in press). (1996)

    • Related Report
      1995 Annual Research Report
  • [Publications] M. Mitome: "Optimum Condition of Convergent Beam Illumination for Observation of Local Structure by High-Resolution Transmission Electron Microsopy" Ultramicroscopy. (in press). (1996)

    • Related Report
      1995 Annual Research Report
  • [Publications] Y.Ohshima,K.Takayanagi: "Solid-Liquid phase transition of tin particles observed by UHV high resolution electron microscopy" Z.Phys.D. 27. 287-294 (1993)

    • Related Report
      1994 Annual Research Report
  • [Publications] Y.Kimura,K.Takayanagi: "Incommensurate phase of Sn/si(100)studied by HR-REM" Surface Sci.283. 349-354 (1993)

    • Related Report
      1994 Annual Research Report

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Published: 1994-04-01   Modified: 2016-04-21  

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