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Preparation of soft magnetic Fe-Al thin plate by Al diffusion penetration into Fe specimen.

Research Project

Project/Area Number 06453088
Research Category

Grant-in-Aid for General Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field Material processing/treatments
Research InstitutionKYUSHU INSTITUTE OF TECHNOLOGY

Principal Investigator

ONISHI Masami  Kyushu Institute of Technology, Faculty of Engineering, Professor., 工学部, 教授 (90029041)

Co-Investigator(Kenkyū-buntansha) WAKAMATSU Yoshinori  Kyushu Institute Technology, Faculty of Engineering, Associate Professor., 工学部, 助教授 (50039111)
Project Period (FY) 1994 – 1995
Project Status Completed (Fiscal Year 1995)
Budget Amount *help
¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 1995: ¥600,000 (Direct Cost: ¥600,000)
KeywordsThin iron plate / Aluminum / Diffusion penetration / Soft magnetic property / Maximum permeability / 鉄薄板
Research Abstract

When evaporated ALCL_3 gas contacts with an iron specimen annealed at high temperature in the oxygen free atmosphere, aluminum does not penetrate into the specimen. If the sub-halide, AlCl, gas contacts with the specimen at higher temperatures than 1373 K,aluminum penetrates into the specimen.
The evaporated AlCl_3 gas is led on the surface of molten aluminum heated at 1573K and then the gas reacts with aluminum according to the following equation ;
AlCl_3 (gas) + 2Al (liquid) * 3AlCl (gas) .(1)
The AlCl gas decomposes at the surface of the iron specimen annealed at 1548 K,owing to the opposite reaction of Eq.1., then atomic aluminum penetrates into the specimen.
Interstitial free steel specimen with 0.7 mm in thickens and 30 mm in diameter, of which each disk side is separately treated for 14.4 ks at the condition mentioned above. Thus treated disc shows the average concentration of 13.4 mass % Al, 360 mu Hv for hardness and 8*10^<-7>OMEGA m for electric resistant ratio. For the measurement of soft magnetic property the treated specimen is machined from the disk to the ring with 25 and 15 mm in outer and inner diameters. The ring exhibits maximum permeability of 6500 H/m and coercive force of 30A/m. Water quenching from 973 kyields the increase of the maximum permeability from 6500 H/m to about 10^4H/m. Metals containing aluminum usually resist the attack of acids and oxygen at high temperature, so that the results of this experiment is also applicable to the surface treatment of metals

Report

(3 results)
  • 1995 Annual Research Report   Final Research Report Summary
  • 1994 Annual Research Report
  • Research Products

    (10 results)

All Other

All Publications (10 results)

  • [Publications] 大西 正己: "CVDによるアルミニウムのα鉄試料への拡散浸透" 材料とプロセス. 7. 578-581 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 三原 英一郎: "鉄に対するアルミニウムの拡散浸透による軟磁性の向上" 表面技術協会九州支部119回例会会報. 34. 25-26 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 大西 正己: "金属ハライドによる鉄鋼の表面処理" 表面技術協会九州支部121回例会会報. 35. 1-6 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] M.Onishi: "Diffusion Penetration of Aluminum into alpha iron specimens using CVD." Current Advances in Materials and Processes. Vol.7, No.2. 578-581 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] E.Mihara: "Advance of Soft Magnetic Property due to Diffusion Penetration of Aluminum into Steel Thin Plate." Reikai-kaiho, Kyushu Branch of Surface Finishing Soc.Japan. Vol.34, No.3. 25-26 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] M.Onishi: "Surface treatment of iron and steel using metal halide." Reikai-kaiho, Kyushu Branch of Surface Finishing Soc.Japan. Vol.35, No.2. 1-6 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 大西 正巳: "CVDによるアルミニウムのα鉄試料への拡散浸透" 材料とプロセス. 7. 578-581 (1994)

    • Related Report
      1995 Annual Research Report
  • [Publications] "鉄に対するアルミニウムの拡散浸透による軟磁性の向上" 表面技術協会九州支部119回例会会報. 34. 25-26 (1994)

    • Related Report
      1995 Annual Research Report
  • [Publications] 大西 正巳: "金属ハライドによる表面処理" 表面技術協会九州支部121回例会会報. 35. 1-6 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] 大西正巳: "CVDによるアルミニウムのα鉄試料中への拡散浸透" 材料とプロセス. 7巻. 578-581 (1994)

    • Related Report
      1994 Annual Research Report

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Published: 1995-04-01   Modified: 2016-04-21  

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