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Development of Young's Modulus Measurement System for Anisotropic Thin Films

Research Project

Project/Area Number 06555031
Research Category

Grant-in-Aid for Developmental Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field Materials/Mechanics of materials
Research InstitutionRITSUMEIKAN UNIVERSITY

Principal Investigator

OHNAMI Masateru  Ritsumeikan University, Faculty of Sci, & Eng., professor, 理工学部, 教授 (60066587)

Co-Investigator(Kenkyū-buntansha) YOSHIDA Toshihiro  HItachi Ltd., Storage System Workes, Senior Engineer, ストレージシステム事業部, 副参事
SAKANE Masao  Ritsumeikan University, Faculty of Sci, & Eng., professor, 理工学部, 教授 (20111130)
Project Period (FY) 1994 – 1995
Project Status Completed (Fiscal Year 1995)
Budget Amount *help
¥8,600,000 (Direct Cost: ¥8,600,000)
Fiscal Year 1995: ¥1,400,000 (Direct Cost: ¥1,400,000)
Fiscal Year 1994: ¥7,200,000 (Direct Cost: ¥7,200,000)
KeywordsYoung's modulus / 3-points bending test / Vibrating reed test / Thin film / Electric device / Cr thin film / Permalloy thin film / 弾性定数 / 曲げ試験 / 固有振動数 / 異方性
Research Abstract

(1) Young's modulus of Cr thin films was measured by a three-points bending and vibrating reed method. The value of the Young's modulus of the film thicker than 5.1 mum was 248.8Gpa and which agrees well with that of Young's modulus of the bulk material. Young's modulus of the film thinner than 3.2 mum increased with decreasing the film thickness. Young's modulus of 0.248 mum was 568GPa.
(2) X ray diffraction and SEM observation revealed that amorphous-like structure was formed in the thickness less than 1-2 mum while columnar structure was formed in the thickness thicker then 1-2 mum. The thickness boundary of the two structures was agrees well with the thickness at which Young's modulus increased with decreasing the film thickness.
(3) Young's modulus of permalloy was 222.0GPa for the film thicker than 2.9 mum which agrees with that of the bulk material. Young's modulus of the film thinner than 1.1 mum increased with decreasing the film thickness. Young's modulus of 0.276 mum film was 296GPa which is 1.48 times larger than that of the bulk material.
(4) SEM observations indicated that the variation of Young's modulus with film thickness was resulted from the change of the film structure. Amorphous-like structure was made in the thickness range thinner than 1-2 mum while columnar structure in the range thinner than 1-2 mum.

Report

(3 results)
  • 1995 Annual Research Report   Final Research Report Summary
  • 1994 Annual Research Report
  • Research Products

    (11 results)

All Other

All Publications (11 results)

  • [Publications] 橋本清司: "電子デバイス用薄膜のヤング率測定用精密3点曲げ試験装置の開発と測定例" 材料. 43巻489号. 703-709 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Kiyoshi Hashimoto: "young's Modulus of Thin Films Measured by High Resolution Three-Points Bending Machine" ASME 1994 WAM Symposia on Materials & Mechanics in Electronic Packaging for the 21st Century. AMP Vol.187. 57-62 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 橋本清司: "振動リ-ド法による薄膜のヤング率測定装置の開発と測定例" 材料. 44巻507号. 1456-1463 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 高橋 慎: "パ-マロイ薄膜の3点曲げおよび振動リ-ド法によるヤング率測定" 日本材料学会第45期学術講演会. (発表予定).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Kiyoshi Hashimoto: "Development of three-points bending machine for measuring Young's modulus of thin films for electric devices and experiments." J.Soc.Mater.Sci.Japan. Vol.43 No489. 703-709 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Kiyoshi Hashimoto: "Young's modulus of thin films measured by high resolution three-points bending machine." ASME 1994 WAM Symposia on Materials & mechanics in Electric Packaging for 21st century. (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Kiyoshi Hashimoto: "Developmnet of Vibrating reed Machine for Measuring Young's Modulus of Thin Films." J.Soc.Mater.Sci.Japan. Vol.44 No507. 1456-1463 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Makoto Takahashi: "Young's Modulus Measurement of Permalloy by Three-points Bending and Vibrating Reed Method." Proc.45th Annual Meeting of Japan Society of Materials Science. (to appear).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 橋本清司: "振動リ-ド法による薄膜のヤング率測定装置の開発と測定例" 材料. 44. 1456-1463 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] 高橋 慎: "パ-マロイ薄膜の3点曲げおよび振動リ-ド法によるヤング率測定" 日本材料学会第45期学術講演会. (発表予定). (1996)

    • Related Report
      1995 Annual Research Report
  • [Publications] 橋本清司: "振動法によるCr薄膜のヤング率測定法の開発" 材料. (発表予定).

    • Related Report
      1994 Annual Research Report

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Published: 1994-04-01   Modified: 2016-04-21  

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