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DEVELOPMENT OF A HIGH-PRECISION ELECTRON DENSITY MEASUREMENT TECHNIQUE FOR MULTILAYER FILMS

Research Project

Project/Area Number 06555092
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section試験
Research Field Electronic materials/Electric materials
Research InstitutionTOKYO INSTITUTE OF TECHNOLOGY

Principal Investigator

HASHIZUME Hiroo  TOKYO INSTITUTE OF TECHNOLOGY,MATERIALS AND STRUCTURE LABORATORY PROFESSOR, 応用セラミックス研究所, 教授 (10011123)

Co-Investigator(Kenkyū-buntansha) SAKATA Osami  TOKYO INSTITUTE OF TECHNOLOGY,MATERIALS AND STRUCTURE LABORATORY RESEARCH ASSOCI, 応用セラミックス研究所, 助手 (40215629)
熊谷 一夫  理学電機株式会社, 設計部, 課長
小林 勇二  理学電機株式会社, 設計部・開発課, 主任技師(研究職)
Project Period (FY) 1994 – 1996
Project Status Completed (Fiscal Year 1996)
Budget Amount *help
¥6,500,000 (Direct Cost: ¥6,500,000)
Fiscal Year 1996: ¥200,000 (Direct Cost: ¥200,000)
Fiscal Year 1995: ¥500,000 (Direct Cost: ¥500,000)
Fiscal Year 1994: ¥5,800,000 (Direct Cost: ¥5,800,000)
KeywordsX-RAY FRESNEL REFLECTION / ELECTRON DENSITY PROFILE THROUGH THIN FILMS / INTEFACE ROUGINESS / CORRELATED ROUGHNESS STRUCTURE / SURFACE STEP / SURFACE PROFILE REPLICATION / MAGNETIC MULTILAYER / X線鏡面反射 / 散漫散乱 / SiGe人工超格子 / 共鳴X線磁気散乱 / 電子密度分布決定 / 積層薄膜 / 電子密度分布 / 界面構造 / 非鏡面反射 / X線反射 / 表面・界面ラフネス / フレネル反射
Research Abstract

An X-ray reflectometer with a crystal monochromator and analyzer has been designed for high-precision determination of electron of density profiles in multilayr films. Use of an asymmetric channel-cut silicon monochromator resulted in an X-ray beam intensity one order of magnetitue greater than in the conventional design. For data analysis a package of computer codes has been prepared using the scattering theory based on the distorted-wave Born approximation, which allows us to determine the interface roughness and its correlations in the in-plane and out-of-plane directions from specular and non-specular diffuse scattering data collected over a large range of scattering angle including the total-external reflection region. The system has bee applied to the determination of layr thicknesses and their variation, interface roughness in semiconductor SiGe/Si superlattices and magnetic multilayrs including Gd Co and Gd layrs, an Al/C nanolayrs. It was found that the replication of surfacestep structure on a vicinal siicon substrate strongly depends on the alloy composition of Ge in the SiGe layr. The system was proved useful in the structure characterization of magnetic multilayrs for X-ray resonant magnetic scattering experiments at synchrotron sources. It was also applied to a model-independent determination of electron density profiles in Al/C films from anomalous dispertion X-ray reflectometry data.

Report

(4 results)
  • 1996 Annual Research Report   Final Research Report Summary
  • 1995 Annual Research Report
  • 1994 Annual Research Report
  • Research Products

    (21 results)

All Other

All Publications (21 results)

  • [Publications] A.Nikulin他: "High-resolution triple-crystal X-ray diffraction expcricnents performed at the Anstralian beamline facilitry on a silicon sainpec" J.Applied Crystallopaply. 28. 57-60 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] A.Nikulin他: "High-resolution mapping of two-dicnensirial lattice distortions in ion-implanted crystals from X-ray diffraction data" J.Applied Crystallopaply. 28. 803-811 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T.Ohkawa他: "Anomalous disprsim X-ray reflectometry for Aelc multilayas" Plysica. B221. 416-419 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] N.Ishimatsu他: "X-ray reflectivity at the L edges of Gd" J. Synch. Radiation. 4. (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] P.M.Reimer他: "Interfacial ronyhness of Si_<1-x>Ge_x/Si multilayu Structures" J. Phys. Cond. Matt.(1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] H.Hashizume他: "X-ray ciraular dichroic Bragg reflections from GdCo multilayas" Jpn. J. Appl. Phys.(1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] A.Nikulin et al.: "High-resolution triple crystal diffraction experiments performed at the Australian beamline facility on a silicon crystal" J.Appl.Crystallogr. 28. 57-60 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] A.Nikulin et al.: "High-resolution mapping of two-dimensional lattice distortions in ion-implanted crystals from X-ray diffraction data" J.Appl.Crystallogr.28. 803-811 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T.Ohkawa et al.: "Anomalous disperison X-ray reflectometry for Al/C multilayrs" Physica. B221. 416-419 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] N.Ishimatsu et al.: "X-ray reflectivity at the L edges of Gd" J.Synch.Rad.4. (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] P.M.Reimer et al.: "Interfacial roughness of Si_<1-x>Ge_x/Si multilayr structures" J.Phys.Cond.Matt.(1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] H.Hashizume et al.: "X-ray circular dichroic Bragg reflections from GdCo multilayrs" Jpn.J.Appl.Phys.(1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] N.Ishimatsu 他: "X-ray Reflectivity at the L edges of Gd" J.Synch,Red.4. (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] P.M.Reimer 他: "Interfacial roughness of Si_<1-x>Gex/Si multilayer structures" J.Phys.Cond.Matt.(1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] H.Hashizume 他: "X-ray circular dichroic Bragg reflections from GdCo multilayus" Jpn.J.Appl.Phys.(1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] T.Ohkawa 他: "Anomalous dispersion X-ray reflectometry for Al/C multilayers" Physica. B221. 416-419 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] A, Yu, Nikulin 他: "Mapping of Two-Dimensional Lattice Distortions in Silicon Crystals at Shbmiuomelen Resulution from X-ray Rocking-Curve Data." J. Applied Crystorllography. 27. 338-344 (1994)

    • Related Report
      1995 Annual Research Report
  • [Publications] O. Sakata & H. Hashizume: "Vltahigh Vacuum diffraetoweter for gtazing-angle X-ray Standing-wave experiuents at a vertical wigglen source" Reviem of Scientific Iustruaents. 66. 1364-1366 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] A, Yu, Nikulin 他: "High-resolution tiple-uystal X-ray diffraction experiunents perforwed at the Anstraliam National beamline facility on a silicon sample" J. Applied Crystorllography. 28. 57-60 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] O. Sakata & H. Hashizume: "Propenties of-qrazuing X-ray standing waves and their apbication to an ansenic-deposited si(III)(X)smface" Acta Crystallographica. A51. 375-384 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] A, Yu, Nikulin 他: "High-resolution auapping of two-dimensional lattiu distortions in ion-implanted uystals from X-ray aiffractowetry data" J. Applied Crystorllography. 28. 803-811 (1995)

    • Related Report
      1995 Annual Research Report

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Published: 1994-04-01   Modified: 2016-04-21  

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