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Developement of in situ structural analyzes of bonding between different materials

Research Project

Project/Area Number 06555209
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section試験
Research Field Material processing/treatments
Research InstitutionNagoya University

Principal Investigator

KIZUKA Tokushi  Nagoya University School of Engineering, Research Associate, 工学部, 助手 (10234303)

Co-Investigator(Kenkyū-buntansha) ISHIDA Yoichi  Tokyo University Faculty of Engineering, Professor, 工学部, 教授 (60013108)
TANAKA Nobuo  Nagoya University School of Engineering, Associate Professor, 工学部, 助教授 (40126876)
Project Period (FY) 1994 – 1996
Project Status Completed (Fiscal Year 1996)
Budget Amount *help
¥3,500,000 (Direct Cost: ¥3,500,000)
Fiscal Year 1996: ¥300,000 (Direct Cost: ¥300,000)
Fiscal Year 1995: ¥400,000 (Direct Cost: ¥400,000)
Fiscal Year 1994: ¥2,800,000 (Direct Cost: ¥2,800,000)
Keywordsbonding / Transmission electron microscopy / hetero bonding / in situ analysis / atomic resolution / 高分解能透過電子顕微鏡 / 電子線加工
Research Abstract

Atomic scale solid state direct bonding in time-resolved high-resolution transmission electron microscopy was realized by using the piezodriven specimen holder. The structural variations of atomic arrangements in approach, contact, bonding and separation processes between two gold tips were observed at atomic scale. It was found that the nanometer-sized gold tips contact spontaneously when the tips approach at the critical distance corresponding to a few atomic distance underi intense electron irradiation. The crystallographic boundary forms after the contact. A few layrs near the surfaces and bonding-boundaries are responsible for the bonding and separation processes. New kinds of atomic scale mechanical tests such as the friction test, the compressing, tensile and shear deformation tests were proposed.

Report

(4 results)
  • 1996 Annual Research Report   Final Research Report Summary
  • 1995 Annual Research Report
  • 1994 Annual Research Report
  • Research Products

    (31 results)

All Other

All Publications (31 results)

  • [Publications] T. Kizuka et al.: "Cross-sectional high-resolution transmission electron microscopy of atomic scale contact and noncontact-type scannings on Sold surfaces" Phys. Rev.B55 (in print). (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T. Kizuka et al.: "Time-resolved HREM of solid state direct bonding of gold and zinc oxide nanocrystallites" Appl. Phys. Lett.(in print). (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T. Kizuka et al.: "Time-resolved HREM of atomic scale solid state direct bonding of Sold tips" J. Electron Microscopy. 46 (in print). (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T. Kizuka et al.: "Time-resolved atomic observation of fragmentation of gold clusters by HREM" Surf. Rev. Lett.,. 3. 1187-1190 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T. Kizuka et al.: "Critical grainsize for structural transformation in vacuum-deposited molybdenum films" Surf. Rev. Lett.,. 3. 1181-1185 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T. Kizuka et al.: "Structure and hardness of narocry stalline silver" J. Mat. Sci.(in print). (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T.Kizuka: "Nanometer scale electron beam processing and in-situ atomic observation of vacuum-deposited MgO films in high-resolution electron microscopy" Phil.Mag.A. 71. 631-639 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T.Kizuka: "Time-resolved atomic observation of fragmentation of gold clusters by high-resolution electron microscopy" Surf.Rev.Lett.3. 1187-1190 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T.Kizuka: "Critical grain size for structural transformation in vacuum-deposited molybdenum films" Surf.Rev.Lett.3. 1181-1185 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T.Kizuka: "Dynamic high-resolution electron microscopy of grain boundary migration and structural transformation in nanocrystalline ZnO" Trans.JIM. (in print). (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T.Kizuka: "Structure and hardness of nanocrystalline silver" J.Mat.Sci.(in print). (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T.Kizuka: "Cross sectional high-resolution transmission electron microscopy of atomic scale contact and non-contact type scanning on gold surfaces" Phys.Rev.B. (in print). (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T.Kizuka: "Time-resolved high-resolution electron microscopy of solid state direct bonding of gold and zinc oxide nanocrystallites" Appl.Phys.Lett.(in print). (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] T.Kizuka et al.: "Cross-sectional high-resolution transmission electron microscopy of atomic scale contact and noncontact-type scannings on sold surfaces" Rhys.Rev.B55(in print). (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] T.Kizuka et al.: "Time-resolved HREM of solid state direct bonding of gold and zincoxide nanocrystallites" Appl.Phys.Lett.(in print). (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] T.Kizuka et al.: "Time-resolved HREM of atomic scale solid state direct bonding of sold tips" J.Electron Microscopy. 46(in print). (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] T.Kizuka et al.: "Time-resolved atomic observation of fragmentation of gold clusters by HREM" Surf.Rev.Lett.,. 3. 1187-1190 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] T.Kizuka et al.: "Critical grain size for structural transformation in vacuum-deposited molybdenum films" Surf.Rev.Lett.,. 3. 1181-1185 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] T.Kizuka et al.: "Structure and hardness of nanocrystalline silver" J.Mat.Sci.(in print). (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] T.Kizuka et al.: "Nanometer-scale election beam processing and in-sifu atomic observation of vacuum-deposited MgOf:lms in HREM" Philosophical magazine. 71. 631-639 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] T.Kizuka et al.: "Time-resolved atomic observation of fragmentation in gold clusters studied by HRTEM" Surface Review and Letters. (in print). (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] T.Kizuka et al.: "Critical site for structural transformatin in Vacccum-dwposited molybdenum films" Surface Review and Letlers. (in print). (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] T.Kizuka et al.: "Structure and hardness of nanocrystalline silver" Journal of Materials Science. (in print). (1996)

    • Related Report
      1995 Annual Research Report
  • [Publications] 木塚徳志 他: "超微細電子線加工の動的原子直視観察" 日本金属学会報. 34. 547 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] 木塚徳志 他: "金属クラスターの分裂" 日本金属学会報. 34. 548 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] T.Kizuka,他: "Structure and thermal Stability of nanocrystalline silver Stadied by HREM′ and PAS." Philosophical magazine. A69. 551-563 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] T.Kizuka,他: "Nanometer-scale electron beam processing and in-situ atomic observation of vacuum-deposited MgO films in HREM" Philosophical magazine. A69(in print). (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] T.Kizuka,他: "Dynamic HREM of diflusion bonding between ZnO nanocry stallites at ambient temperature" Philosophical magazine Letter. 69. 135-139 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] T.Kizuka,他: "HREM of nanocrystalline Ni-Al alloys:instability of ordered ctracture and dynamic behavior of grain bondalies" Journal Material Science. 29. 5599-5606 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] T.Kizuka,他: "Structure and Mechanical properties of nanocrystalline AglMgO composites" Journal Material Science. 29. 3107-3112 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] T.Kizuka,他: "Time-resolved atomic observation of fragmertation in gold clusters stadied by HRTEM" Surface Revier and Letter. (in print). (1995)

    • Related Report
      1994 Annual Research Report

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Published: 1994-04-01   Modified: 2016-04-21  

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