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Development of NMR imaging probe of measuring polymer materials

Research Project

Project/Area Number 06555288
Research Category

Grant-in-Aid for Developmental Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field 高分子構造・物性(含繊維)
Research InstitutionTOKYO INSTITUTE OF TECHNOLOGY

Principal Investigator

ANDO Isao  Tokyo Institute of Technology Fuculty of Engineering Professor, 工学部, 教授 (20016637)

Co-Investigator(Kenkyū-buntansha) HIGUCHI Keiichiro  Japan electronics Optics NMR Laboratories senior Research Fellow, NMR室, 主任研究員
KUROSU Hiromichi  Tokyo Institute of Technology Faculty of Engineering Research Associate, 工学部, 助手 (20221228)
Project Period (FY) 1995
Project Status Completed (Fiscal Year 1995)
Budget Amount *help
¥11,900,000 (Direct Cost: ¥11,900,000)
Fiscal Year 1995: ¥900,000 (Direct Cost: ¥900,000)
Fiscal Year 1994: ¥11,000,000 (Direct Cost: ¥11,000,000)
KeywordsNMR imaging / NMR probe / structure / dynamics / polymer / gel / 画像解析 / ゲル
Research Abstract

A high resolution NMR imaging probe and its power amplifier have been developed, in order to investigate macroscopic and microscopic structure and dynamics of polymer materials and its spatial distribution associated with physical properties. The NMR imaging experiments using our developed NMR probe have provided high resolution NMR imaging pattern of polymer gels as one of typical polymer materials and have elucidated spatial information on macroscopic and microscopic structures and dynamics of the gel. We have demonstrated that our developed NMR imaging probe system is a powerful means for spatial information on structures and dynamics of polymer materials associated with physical properties.

Report

(3 results)
  • 1995 Annual Research Report   Final Research Report Summary
  • 1994 Annual Research Report
  • Research Products

    (24 results)

All Other

All Publications (24 results)

  • [Publications] H.Kurosu,T.Shibuya,H.Yasunaga,I.Ando: "Spatial information on a polymer gel as studied by ^1H NMR imaging.III" Polymer Journal. 28. 80-85 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] T.Shibuya,H.Yasunaga,H.Kurosu, I.Ando: "Spatial information on a polymer gel as studied by ^1H NMR imaging.II" Macromolecules. 28. 4377-4382 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] D.Inoue,H.Kurosu,Q.Chen,I.Ande: "Structural and dynamical studies of ^<13>C-labeled polyethylene adsorbed on the surface of silica gel by NMR" Acta Polymerica. 46. 420-423 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] H.Kurosu,M.Kikuchi,I,Ando: "Structural characterization of polypyrrole in the solid state by high resolution ^<15>N NMR spectroscopy. II" J.Polymer Sci.,polymer Phys.33. 769-775 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] H.Kurosu,Y.Nakajima,I.Ando: "Structural characterization of polyacenic polymers in the solid state by high resolution NMR spectroscopy" J.Mol.Structure. 355. 27-32 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] H.Yasunaga,M.Kobayashi,S.Matsukawa,H.Kurosu,I.Ando: "Structures and dynamics of polymer gel systems viewed from NMR spectroscopy" Annual Reports on NMR Spectroscopy. 32 (in press). (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 安藤 勲編: "高分子の構造工,磁気共鳴(新高分子実験学)" 共立出版, 572 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] H.Kurosu, T.Shibuya, H.Yasunaga, I.Ando: "Spatial information on a polymer gel as studied by ^1H NMR imaging. III" Polymer Journal. 28. 80-85 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] T.Shibuya, H.Yasunaga, H.Kurosu, I.Ando: "Spatial information on a polymer gel as studied by ^1H NMR imaging. III" Macromolecules. 28. 4377-4382

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] M.Kobayashi, I.Ando, T.Ishii, S.Amiya: "Structural study of poly (vinyl alcohol) in the gel state by high-resolution solid-state ^<13>C NMR spectroscopy" Macromolecules. 28. 6677-6679 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] K.Tsuchiya, A.Takahashi, N.Takeda, N.Asakawa, S.Kuroki, I.Ando, A.Shoji, T.Ozaki: "Hydrogen-bonding effect on ^<13>C NMR chemical shifts of amino acid residue carbonyl carbons of some peptides in the crystalline state" J.Mol.Structure. 350. 233-240 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] H.Yasunaga, M.Kobayashi, S.Matsukawa, H.Kurosu, I.Ando: "Structures and dynamics of polymer gel systems viewed from NMR spectroscopy" Annual Reports on NMR Spectroscopy. 31(in press). (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] H. Kurosu, T. Shibuya, H. Yasunaga, I. Ando: "Spatial information on a polymer gel as studied by ^1H NMR imaging. III" Polymer Journal. 28. 80-85 (1996)

    • Related Report
      1995 Annual Research Report
  • [Publications] T. Shibuya. H. Yasunaga, H. Kurosu. I. Ando: "Spatial information on a polymer gel as studied by ^1H NMR imaging. II" Macromolecules. 28. 4377-4382 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] D. Inoue, H. Kurosu, Q. Chen, I. Ando: "Structural and dynamical studies of ^<13>C-labeled polyethylene adsorbed on the surface of silica gel by NMR" Acta Polymerica. 46. 420-423 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] H. Kurosu, M. Kikuchi, I. Ando: "Structral characterization of polypyrrole in the solid state by high resolution ^<15>N NMR spectroscopy. II" J. Polymer Sci., polymer Phys.33. 769-775 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] H. Kurosu. Y. Nakajima, I. Ando: "Structural characterization of polyacenic polymers in the solid state by high resolution NMR spectroscopy" J. Mol. Structure. 355. 27-32 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] H. Yasunga, M. Kobayashi, S. Matsukawa, H. Kurosu, I. Ando: "Structures and dynamics of polymer gel systems viewed from NMR spectroscopy" Annual Reports on NMR Spectroscopy. 31(in press). (1996)

    • Related Report
      1995 Annual Research Report
  • [Publications] 安藤 勲編: "高分子の構造工、磁気共鳴(新高分子実験学)" 共立出版, 572 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] I.Ando,H.Kurosu: "NMR studies of higher-order structures of solid polymers" Annual Reports on NMR Spectroscopy. 28. 189-275 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] I.Ando,H.Kurosu: "Hydrogen-bonding structural study of solid peptides and polypeptides as studied by ^<17>O NMR spectroscopy" Journal of Molecular Structure. 323. 197-208 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] I.Ando,H.Kurosu: "Spatial information on a polymer gel as studied by ^1H NMR imaging : 2.Shrinkage by the application of an electric field" Macromolecules. (1995)

    • Related Report
      1994 Annual Research Report
  • [Publications] I.Ando,H.Kurosu: "Spatial information on a polymer gel as studied by ^1H NMR imaging : II" 5th SPSJ International Polymer Conference. 305-305 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] 安藤勲: "高分子の固体NMR" 講談社サイエンティフィク社, 220 (1994)

    • Related Report
      1994 Annual Research Report

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Published: 1994-04-01   Modified: 2016-04-21  

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