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Improvement of scanning laser microscope type in situ observation system and microscopic observation of fracture process in intermetallic compounds

Research Project

Project/Area Number 06650121
Research Category

Grant-in-Aid for General Scientific Research (C)

Allocation TypeSingle-year Grants
Research Field Materials/Mechanics of materials
Research InstitutionToyota Technological Institute

Principal Investigator

UENO Akira  Toyota Technological Institute, Fac.of Eng.Associate Prof., 工学部, 助教授 (30160188)

Co-Investigator(Kenkyū-buntansha) KISHIMOTO Hidehiro  Toyota Technological Institute, Fac.of Eng.Prof., 工学部, 教授 (10148348)
Project Period (FY) 1994 – 1995
Project Status Completed (Fiscal Year 1995)
Budget Amount *help
¥300,000 (Direct Cost: ¥300,000)
Fiscal Year 1995: ¥300,000 (Direct Cost: ¥300,000)
KeywordsScanning laser microscope / In situ observation system / Microscopic fracture process / Intermetallic compounds / TiAl / Crack initiation / Crack propagation / Fracture mechanics / 微視破壊現象
Research Abstract

The compact horizontal type elctric-hydrauric fatigue testing machine which could apply axial load under the scanning laser microscope was newly developed, and in situ observation system was improved. Characteristic of the improved system are shown in the following.
(1) During axial load of up to (]SY.+-。[) 98kN is applied, the specimen surface can be observed in the ambient air with high magnification.
(2) Load controlled or position controlled fatigue test with frequency of 0.001-tens Hz can carreid out.
(3) As the testing machine is placed on a computer-controlled X-Y automatic stage, the observation point can be moved of 2mum accuracy. Also, movement of visual field during fatigue test can be cancelled by the computer-controlled automatic stage.
(4) Because a special rotation jig is set, the whole circumference of the specimen can be observed.
By using this system, fatigue process of the TiAl intermetallic compounds are observed in detail. To study a basic S-N characteristics, fatigue tests attended with surface observation were carried out under sine wave of stress ratio R=-1, by using a Ti-33.8wt.% Al.
Although TiAl hardly deformed plastically, several types of slip (single slip, double slip, twin) which were the evidence of the plastic deformation were oberved in some of gamma-TiAl grain. Also, number of slip lines were increased as number of stress cycles increased. It is concluded that the accumulated slip deformation causes the fatigue fracture of TiAl, as well as the fatigue in traditional metallic materials.
It is confirmed that the newly developed fatigue testing machine and the improved scanning laser microscope type in situ observation system function well. By setting up additional apparatus, in situ observation will be able to carry out in water or at elevated temperature.

Report

(3 results)
  • 1995 Annual Research Report   Final Research Report Summary
  • 1994 Annual Research Report
  • Research Products

    (15 results)

All Other

All Publications (15 results)

  • [Publications] 上野 明: "レーザー顕微鏡による表面観察I(素材試験への応用)" 材料学会. 31. 62-69 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 上野 明・岸本秀弘他1名: "金属間化合物TiAlの疲労き裂進展特性" 日本材料学会第22回疲労シンポジウム講演論文集. 181-184 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 上野 明・岸本秀弘他1名: "金属間化合物TiAlの応力腐食割れ" 日本機械学会東海支部第44期総会講演会講演論文集. No.953-1. 118-119 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 上野 明・岸本秀弘他1名: "金属間化合物TiAlの中高温下における疲労き裂成長挙動" 日本材料学会第44期学術講演会講演論文集. 179-180 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] A.Ueno,K.Kishimoto: "Fatigue Crack Propagation Behavior in TiAl Intermetallic Compounds" 国際会議(Fatigue 96,1996年5月Berlin). (発表予定).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] A.Ueno: "Surface observation by laser microscope I (Application for materials testing)" J.of Society of Materials Science. Vol.31, No.2. 62-69 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] A.Ueno et.al.: "Fatigue Crack Propagation Behaviro in TiAl Intermetallic Compounds" Proc of the 22th Sympo.on Fatigue. JSMS,Vol.22. 181-184 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] A.Ueno et.al.: "Stress Corrosion Cracking In TiAl Intermetallic Compounds" Proc.of the 44th Sympo.on General Meeting, JSME Tokai subdivision. No.953-1. 118-119 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] A.Ueno et.al.: "Fatigue Crack Propagation Behavior in TiAl Intermetallic Compounds at Middle-high Temperature" Proc.of the 44th Sympo.on General Meeting, JSMS. Vol.44. 179-180 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] A.Ueno and H.Kishimoto: "Fatigue Crack Propagation Behavior in TiAl Intermetallic Compounds" Proc.of Fatigue 96 Berlin. (in press). (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 上野 明・岸本秀弘他1名: "金属間化合物TiAlの中高温下における疲労き裂成長挙動" 日本材料学会第44期学術講演会講演論文集. 179-180 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] A. Ueno, K. Kishimoto: "Fatigue Crack Propagation Behavior in TiAl Intermetallic Compounds" 国際会議(Fatigue 96, 1996年5月Berlin). (発表予定).

    • Related Report
      1995 Annual Research Report
  • [Publications] 上野,明: "レーザー顕微鏡による表面観察I(素材試験への応用)" 材料科学. 31. 62-69 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] 上野 明,岸本秀弘他1名: "金属間化合物TiAlの疲労き裂進展特性" 日本材料学会第22回疲労シンポジウム講演論文集. 181-184 (1994)

    • Related Report
      1994 Annual Research Report
  • [Publications] 上野 明,岸本秀弘他1名: "金属間化合物TiAlの応力腐食割れ" 日本機械学会東海支部第44期総会講演会講演論文集. No.953-1. 118-119 (1995)

    • Related Report
      1994 Annual Research Report

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Published: 1995-04-01   Modified: 2016-04-21  

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