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Property-Control of Titanium Alloys by Spark Sintering

Research Project

Project/Area Number 06650840
Research Category

Grant-in-Aid for General Scientific Research (C)

Allocation TypeSingle-year Grants
Research Field Metal making engineering
Research InstitutionHIROSHIMA UNIVERSITY

Principal Investigator

YANAGISAWA Osamu  Hiroshima Univ.Faculty of Engi, Prof., 工学部, 教授 (50034393)

Co-Investigator(Kenkyū-buntansha) MATSUGI Kazuhiro  Hiroshima Univ.Faculty of Engi., Researcher, 工学部, 助手 (30253115)
Project Period (FY) 1994 – 1995
Project Status Completed (Fiscal Year 1995)
Budget Amount *help
¥2,000,000 (Direct Cost: ¥2,000,000)
Fiscal Year 1995: ¥300,000 (Direct Cost: ¥300,000)
Fiscal Year 1994: ¥1,700,000 (Direct Cost: ¥1,700,000)
KeywordsTitanium Alloys / Spark Sintering / property-Control / Titanium-Aluminide / Powder Metallurgy / Tensile Properties / Impact Value / Fracture Toughness / 粉末治金 / チタン / 比抵抗 / パルス通電
Research Abstract

The relationship between the number of pulses and the specific resistivity of titanium alloy compacts has been investigated to reveal the phenomena which are caused between powders in the early stage of the spark sintering process. The specific resistivity of the compacts decreased with the number of pulses. The reasons for the decrease of these values during pulse discharge are considered as follows : (1) The metallic contact area is created due to the dielectric breakdown of an oxide film on the powder surface. (2) The heat is generated due to a high current density in the metallic contact area which was already created between powder particles by initial compaction or the prior pulse discharges, and the metallic contact area is spread. It is suggested that the in situ sbility of dielectric breakdown between powder particles and the heat generation in the metallic contact area during pulse discharge process leads to improved particle sinterability.
The investigations for property-control have been performed on titanium alloys such as Ti, Ti-6Al-4V,TiAl, Ti_3Al produced by spark sintering technique. Fine grained compacts are obtained by controlling of resistance sintering temperature, pressure and time. The mechanical properties such as tensile, impact and fracture toughness properties are revealed on the compacts with fine grains. Furthermore, specimens with high densities and approaching the equilibrium state can be obtained in a shorter time by spark sintering than conventional sintering. Such shorter high temperature exposure is important to prevent grain growth.

Report

(3 results)
  • 1995 Annual Research Report   Final Research Report Summary
  • 1994 Annual Research Report
  • Research Products

    (18 results)

All Other

All Publications (18 results)

  • [Publications] 柳沢平: "放電焼結法に関する最近の研究" 日本金属学会会報 "まてりあ". 33. 1489-1496 (1994)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Kazuhiro Matsugi: "Effect of Direct Current Pulse Discharge on the Change of the Specific Resistivity of a Titanium Powder Compact" Proceedings of the 2nd Pacific Rim Int.Conf.on Advanced Materials and Processing. 1. 371-376 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 松木一弘: "銅および鉄圧粉体の比抵抗に及ぼす直流パルス通電の効果" 日本金属学会誌. 59. 740-745 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 隠岐貴史: "真空焼結後HIP処理した純チタン材の金属組織と引張性質" 日本金属学会誌. 59. 746-753 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Kazuhiro Matsugi: "Microstructure of Spark Sintered Titanium-Aluminide Compacts" INTERMETALLICS. 4(in press). (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 隠岐貴史: "真空焼結後HIP処理したTi-6Al-4V合金の引張性質" 軽金属. (投稿中).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Osamu Yanagisawa: "Recent Research on Spark Sintering Process" Bulletin Jpn.Inst.Metals. 33-12. 1489-1496 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Kazuhiro Matsugi: "Effect of Direct Current Pulse Discharge on the Change of the Specific Resistivity of a Titanium Powder Compact" Proc.2nd Pacific Int.Conf.on Advanced Materials & Processing. 1. 371-376 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Kazuhiro Matsugi: "Effect of Direct Current Pulse Discharge on Specific Resistivity of Copper and Iron Powder Compacts" J.Jpn.Inst.Metals. 59-7. 740-745 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Takashi Oki: "Microstructure and Tensile Properties of Vacuum Sintered/HIP'ed Pure Titanium" J.Jpn.Inst.Metals. 59-7. 746-753 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Kazuhiro Matsugi: "Microstructure of Spark Sintered Titanium-Aluminide Compacts" INTERMETALLICS. 4 (in press.). (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] Takashi Oki: "Tensile properties of Vacuum Sintered/HIP'ed Ti-6Al-4V Alloys" J.Jpn.Inst.Light Metals. (to be published.).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1995 Final Research Report Summary
  • [Publications] 柳沢 平: "放電焼結法に関する最近の研究" 日本金属学会会報“まてりあ". 33. 1489-1496 (1994)

    • Related Report
      1995 Annual Research Report
  • [Publications] Kazuhiro Matsugi: "Effect of Direct Current Pulse Discharge on the Change of the Specific Resistivity of a Titanium Powder Compact" Proceedings of the 2nd Pacific Rim Int. Conf. on Advanced Materials and Processing. 1. 371-376 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] 松木 一弘: "銅および鉄圧粉体の比抵抗に及ぼす直流パルス通電の効果" 日本金属学会誌. 59. 740-745 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] 隠岐 貴史: "真空焼結後HIP処理した純チタン材の金属組織と引張性質" 日本金属学会誌. 59. 746-753 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] Kazuhiro Matsugi: "Microstructure of Spark Sintered Titanium-Aluminide Compacts" INTERMETALLICS. 4(in press). (1996)

    • Related Report
      1995 Annual Research Report
  • [Publications] Kazuhiro Matsugi: "Effect of Direct Current Pulse Discharge on the Change of the Specific Resistivity of a Titanium Powder Compact" Proc. of 2nd Pacific Rim International Conf. on Advanced Materials and Processing (PRICM-2). (in press). (1995)

    • Related Report
      1994 Annual Research Report

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Published: 1994-04-01   Modified: 2016-04-21  

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