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Characterization of fuzzy interface in biomaterials by HREM

Research Project

Project/Area Number 07045053
Research Category

Grant-in-Aid for international Scientific Research

Allocation TypeSingle-year Grants
SectionUniversity-to-University Cooperative Research
Research Field 補綴理工系歯学
Research InstitutionNagasaki University

Principal Investigator

HISATSUNE Kunihiro (1996-1997)  Nagasaki University, professor, 歯学部, 教授 (20037526)

安田 克廣 (1995)  長崎大学, 歯学部, 教授 (50013884)

Co-Investigator(Kenkyū-buntansha) VAN Tendeloo  アントワープ大学, 理学部, 教授
VAN Landuyt  アントワープ大学, 理学部, 教授
HASAKA Masayuki  Nagasaki University, professor, 工学部, 教授 (30039698)
UDOH Koh-ichi  Nagasaki University, Instructor, 歯学部, 助手 (60145266)
TANAKA Yasuhiro  Nagasaki University, Instructor, 歯学部, 助手 (10217086)
VAN LANDUYT Joseph  University of Antwerp, Professor
VAN TENDELOO Gustaaf  University of Antwerp, Professor
GUSTAAF Van  アントワープ大学, 理学部, 教授
JOSEPH Van L  アントワープ大学, 理学部, 教授
SCHRYVERS Do  アントワープ大学, 理学部, 教授
VAN DYCK Dir  アントワープ大学, 理学部, 教授
VAN TENDELOO  アントワープ大学, 理学部, 教授
VAN LANDUYT  アントワープ大学, 理学部, 教授
岩永 浩  長崎大学, 教養部, 教授 (40039772)
福永 博俊  長崎大学, 工学部, 教授 (10136533)
藤山 寛  長崎大学, 工学部, 教授 (20112310)
DYCK Dirk Va  アントワープ大学, 理学部, 教授
SCHRYVCRS Do  アントワープ大学, 理学部, 教授
TCHDCLOO Gus  アントワープ大学, 理学部, 教授
LANDUYT Josc  アントワープ大学, 理学部, 教授
久恒 邦博  長崎大学, 歯学部, 助教授 (20037526)
Project Period (FY) 1995 – 1997
Project Status Completed (Fiscal Year 1997)
Budget Amount *help
¥5,700,000 (Direct Cost: ¥5,700,000)
Fiscal Year 1997: ¥1,900,000 (Direct Cost: ¥1,900,000)
Fiscal Year 1996: ¥1,900,000 (Direct Cost: ¥1,900,000)
Fiscal Year 1995: ¥1,900,000 (Direct Cost: ¥1,900,000)
KeywordsHigh resolution electron microscopy / Functionally graded material / Interface / Biomaterial / Composite material / Ion engineering / Ceramics / Metal bond porcelain / 複合材料 / イオン工学 / 歯科用金合金 / 白金 / 規則格子変態 / 相分解 / 時効硬化 / 制限視野電子回折 / X線回折
Research Abstract

The present study was planned to evaluate the bond characteristics in a metal-ceramic composite with better bio-compatibility. It is very important to understand nature of the interface. The investigation of the formation process and the fundamental structure within the interface between metal and ceramics is an important requirement for improving the bonding technique. Two signiticant conclusions were mainly obtained as follows ;
1. It was constructed how to produce better specimen for high resolution transmission electron microscopic observations on the interface of the composite materials. This technique is very effective to perform a direct observation. Especially, the present study was employed for the interface of the materials with remarkably different mechanical properties.
2. It is determined that the dental gold alloy and the dental porcelain were directly bonded without any intermediate layrs. This is new evidence for the system. It means that previous conclusion was rejected. The previous data were not obtained at interface itself but at the vicinity. The EPMA data which were previously obtained, correspond to the information in micrometer scale, while the present HREM data were obtained in nanometer scale.

Report

(4 results)
  • 1997 Annual Research Report   Final Research Report Summary
  • 1996 Annual Research Report
  • 1995 Annual Research Report
  • Research Products

    (24 results)

All Other

All Publications (24 results)

  • [Publications] K.Hamasaki: "Ageing behaviour in a dental low gold alloy with high copper content" Journal of Materials Science:Materials in Medicine. 9. (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Y.Tanaka: "Early stage of ordering in stoichiometric AuCu Alloy" Materials Transactions,JIM. 39. 87-94 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] A.Sakrana: "A coherent phase diagram of the [(AuCu)_<0.86>Ag_<0.14>J_<l-x>Pt_xpseudobinary section in Au-Cu-Ag-Pt quaternary system" Dental Materials Journal. 16. 144-155 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] K.Hisatsune: "Phase transformation in a dental gold alloy for soldering" Journal of Alloys & Compounds. 261. 308-312 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] K.Hisatsune: "Site occupation of platinum in CuAu-Pt alloys" Scripta Materialia. 36. 1161-1165 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] K.Hisatsune: "Ageing reactions in a high carat gold alloy for dental porcelain bonding" Journal of Materials Science:Materials in Medicine. 8. 277-282 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] K.Hamasaki: "Ageing behavior in a dental low gold alloy with high copper content" Journal of Materials Science : Materials in Medicine. 9. (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Y.Tanaka: "Early stage of ordering in stoichiometric AuCu alloy" Materials Transactions, JIM. 39. 87-94 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] A.Sakrana: "A coherent phase diagram of the [(AuCu)_<0.86>Ag_<0.14>]_<1-x>Pt_xpseudobinary section in Au-Cu-Ag-Pt quaternary system" Dental Materials Journal. 16. 144-155 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] K.Hisatsune: "Phase transformation in a dental gold alloy for soldering" Journal of Alloys and Compounds. 261. 308-312 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] K.Hisatsune: "Site occupation of platinum in CuAu-Pt alloys" Scripta Materialia. 36. 1161-1165 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] K.Hisatsune: "Ageing reactions in a high carat gold alloy for dental porcelain bonding" Journal of Materials Science : Materials in Medicine. 8. 277-282 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] K.Hamasaki: "Ageing behaviour in a dental low gold alloy with high copper content" Journal of Materials Science:Materials in Medicine. 9(印刷中). (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] Y.Tanaka: "Early stage of ordering in stoichiometric Au Cu Alloy" Materials Transactions,JIM. 39. 87-94 (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] A.Sakrana: "A coherent phase diagram of the〔(AuCu)_<0.86>Ag_<0.14>〕_<1-X>Pt_Xpseudobinary section in Au-Cu-Ag-Pt quaternary system" Dental Materials Journal. 16. 144-155 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] K.Hisatsune: "Phase transformation in a dental gold alloy for soldering" Journal of Alloys & Compounds. 261. 308-312 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] K.Hisatsune: "Site occupation of platinum in CuAu-Pt alloys" Scripta Materialia. 36. 1161-1165 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] K.Hisatsune: "Ageing reactions in a high carat gold alloy for dental porcelain bonding" Journal of Materials Science:Materials in Medicine. 8. 277-282 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] K. Udoh: "Structural aspect of AuCu I or AuCu II and a cuboidal block configuration of fcc disordered phase in AuCu-Pt and AuCu-Ag pseudobinary alloys" Materials Science & Engineering. A203. 154-164 (1995)

    • Related Report
      1996 Annual Research Report
  • [Publications] A. M. El Araby: "Age-hardening characteristics of (AuCu)_<1-X>Pt_X pseudobinary alloys" Materials Science & Engineering. A206. 290-301 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] K. Hisatsune: "Site occuupation of platinum in CuAu-Pt alloys" Scripta Materialia. (in press). (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] K. Hisatsune: "Aging reactions in a high carat gold alloy for dental porcelain bonding" Journal of Materials Science : Materials in Medicine. (in press). (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] K.-I.Udoh: "Structural aspects of AuCu I or AuCu II and a cuboida ; block configuration of f.c.c.disordered phase in AuCu-Pt and AuCu-Ag pseudobinary alloys" Materials Science & Engineering. A203. 154-164 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] A.M.E1 Araby: "Age-hardening characteristics of (AuCu)_<1-X>- Pt_X pseudobinary alloys" Materials Science & Engineering. A206. 290-301 (1996)

    • Related Report
      1995 Annual Research Report

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Published: 1995-04-01   Modified: 2016-04-21  

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