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High-Temperature Deformation and Diffusional Relaxation of Particle-Dispersion Hardened Alloys

Research Project

Project/Area Number 07455278
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionTokyo Institute of Technology

Principal Investigator

KATO Masaharu  Tokyo Institute of Technology, Interdisciplinary Graduate School of Science and Engineering, Professor, 大学院・総合理工学研究科, 教授 (50161120)

Co-Investigator(Kenkyū-buntansha) ONAKA Susumu  Tokyo Institute of Technology, Interdisciplinary Graduate School of Science and, 大学院・総合理工学研究科, 助教授 (40194576)
FUJII Toshiyuki  Tokyo Institute of Technology, Interdisciplinary Graduate School of Science and, 大学院・総合理工学研究科, 助手 (40251665)
KAJIHARA Masanori  Tokyo Institute of Technology, Interdisciplinary Graduate School of Science and, 大学院・総合理工学研究科, 助教授 (10161035)
Project Period (FY) 1995 – 1997
Project Status Completed (Fiscal Year 1997)
Budget Amount *help
¥7,500,000 (Direct Cost: ¥7,500,000)
Fiscal Year 1997: ¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 1996: ¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 1995: ¥6,300,000 (Direct Cost: ¥6,300,000)
KeywordsDispersion-hardened alloys / High-temperature deformation / Diffusional relaxation / Orowan mechanism / Creep / Elasticity
Research Abstract

The main purpose of this research is to understand the role of diffusional relaxation on high-temperature deformation of dispersion-hardened alloys. High-temperature tensile tests were conducted using Cu-SiO_2, Cu-GeO_2 and Cu-Fe alloy single crystals and bicrystals and various stress-strain curves were obtained. In addition, intergranular brittle fracture was found to be very sensitive to the nature of grain boundaries. To quantitatively discuss these experimental results, it was necessary to obtain information on the shape change of dispersed particles that occurs during the deformation. Misorientation-dependent grain-boundary energy must also be characterized. Therefore, basic data on these quantities were also obtained.
As theoretical studies, diffusional relaxation around dispersed particles was analyzed by combining mechanics, thermodynamics and kinetics and the rate equations for the relaxation process could be obtained sucessfully. Furthermore, stable shape of dispersed particles and precipitates under a given set of conditions was quantitatively analyzed using micromechanics.
In comparison with the high-temperature deformation tests, low-cycle fatigue of Cu-Fe alloy single crystals were performed to reveal the effect of dispersed particles on the development of stable dislocation structure. The similarities and differences in the dislocation structure between high-temperature deformation and cyclic deformation were found very clearly.
It is true that this research project has been successfully completed in a sense that it has greatly improved our understanding. What is more important, however, is that this project resulted in the discovery of various new research areas that are essential to understand the high-temperature deformation of dispersion-hardened alloys.

Report

(4 results)
  • 1997 Annual Research Report   Final Research Report Summary
  • 1996 Annual Research Report
  • 1995 Annual Research Report
  • Research Products

    (21 results)

All Other

All Publications (21 results)

  • [Publications] Susumu Onaka: "Effect of Diffusional Relaxation on the Shape of B203 Particles in a Deforming Copper Matrix" Acta Metallurgica et Materialia. 43. 1577-1585 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Masaharu Kato: "Elastic Strain Energies of Sphere,Plate and Needle Inclusions" Materials Science and Engineering A. A211. 95-103 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] 尾中 晋: "ステレオ観察による楕円体粒子の軸比と方位の決定" 日本金属学会誌. 61. 574-579 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Hiromi Miura: "Intermdciate-Temperature Embrittlement of Cu Bicrystals with Dispersed Fe Particles" Interface Science. 4. 329-338 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Tsutomu Mori: "Determination of the Energies of [001] Symmetric Tilt Boundaries in Cu from the Shape of Boundary SiO2 Particles" Philosophical Magazine Letters. 75. 367-370 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Masaharu Kato: "Low Cycle Fatigue of Cu-Fe Alloy Single Crystals Containing Transformable Fe Particles" ISIJ International. 37. 1224-1229 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] 加藤 雅治: "メゾスコピック二相組織形成の熱力学とシミュレーションに関する調査研究報告書" 材料の不均一性研究会, 137 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Susumu Onaka, Satoshi Hashimoto, Sei Miura and Masaharu Kato: "Effect of Diffusional Relaxation on the Shape of B_2O_3 Particles in a Deforming Copper Matrix" Acta Metallurgica et Materialia. 43 [4]. 1577-1585 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Masaharu Kato, Toshiyuki Fujii and Susumu Onaka: "Elastic Strain Energies of Sphere, Plate and Needle Inclusions" Materials Science and Engineering A. A211 [3]. 95-103 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Susumu Onaka, Tatsuro Hirose, Hiroyuki Kato and Satoshi Hashimoto: "Determination of Aspect Ratio and Orientation of Ellipsoidal Particle by Stereo Observation" Journal of Japan Institute of Metals. 61 [7]. 574-579 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Hiromi Miura, Shin Watanabe, Taku Sakai and Masaharu Kato: "Intermediate-Temperature Embrittlement of Cu Bicrystals with Dispersed Fe Particles" Interface Science. 4 [1]. 329-338 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Tsutomu Mori, Toshio Ishii, Masanori Kajihara and Masaharu Kato: "Determination of the Energies of [001] Symmetric Tilt Boundaries in Cu from the Shape of Boundary SiO_2 Particles" Philosophical Magazine Letters. 75 [6]. 367-370 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Masaharu Kato, Noriyuki Honjo and Toshiyuki Fujii: "Low Cycle Fatigue of Cu-Fe Alloy Single Crystals Containing Transformable Fe Particles" ISIJ International. 37 [12]. 1224-1229 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] 尾中 晋: "ステレオ観察による楕円体粒子の軸比と方位の決定" 日本金属学会誌. 61・7. 574-579 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Hiromi Miura: "Intermediate-Temperature Embrittlement of Cu Bicrystals with Dispersed Fe Particles" Interface Science. 4・1. 329-338 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Tsutomu Mori: "Determination of the Energies of [001] Symmetric Tilt Boundaries in Cu from the Shape of Boundary SiO2 Particles" Philosophical Magazine Letters. 75・6. 367-370 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Masaharu Kato: "Low Cycle Fatigue of Cu-Fe Alloy Single Crystals Containing Transformable Fe Particles" ISIJ International. 37・12. 1224-1229 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Masaharu Kato: "Elastic States of Inhomogeneous Spheroidal Inclusions" Materials Transactions, JIM. 37巻3号. 314-318 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] Hiromi Miura: "Intermediate-Temperature Embrittlement of Cu Bicrystals with Dispersed Fe Particles" Interface Science. 4巻1号. 329-338 (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] Hiromi Miura: "Temperature Dependence of Embrittlement of Cu[001] Tilt Boundaries Induced by Bi Segregation and Its Correlation with Grain-Boundary Energy" Proceedings of the 8th JIM International Symposium on Interfacial Science and Materials Interconnection. (印刷中). (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] M. Kajihara, J. Nakayama, M. Kato and T. Mori: "Orientation Dependence of Mechanical Properties of [110]Twist Boundaries in Cu Bicrystals cloped with Bi" Proceedings of International Conference on Mechanical Properties of Interfacial Materials. (1996)

    • Related Report
      1995 Annual Research Report

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Published: 1995-04-01   Modified: 2016-04-21  

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