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BRITTLENESS,TOUGHNESS AND DUCTILITY OF CERAMICS -THE MICROSCOPIC PROCESSES AND CHARACTERIZATION.

Research Project

Project/Area Number 07555194
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section試験
Research Field Inorganic materials/Physical properties
Research InstitutionTOYOHASHI UNIVERSITY OF TECHNOLOGY

Principal Investigator

SAKAI Mototsugu  TOYOHASHI UNIVERSITY OF TECHNOLOGY,FUCULTY OF ENGINEERING,PROFESSOR, 工学部, 教授 (50124730)

Co-Investigator(Kenkyū-buntansha) SUGANUMA Motohiro  AICHI INDUSTRIAL RESEARCH INSTITUTE,SENIOR RESEARCHER, 材料部, 主任研究員
PEZZOTTI G.  豊橋技術科学大学, 工学部, 助手 (70262962)
Project Period (FY) 1995 – 1996
Project Status Completed (Fiscal Year 1996)
Budget Amount *help
¥12,500,000 (Direct Cost: ¥12,500,000)
Fiscal Year 1996: ¥3,700,000 (Direct Cost: ¥3,700,000)
Fiscal Year 1995: ¥8,800,000 (Direct Cost: ¥8,800,000)
KeywordsCERAMICS / BRITTLENESS / TOUGHNESS / DOUCTILIGY / CHARACTERIZATION,ANALYSIS / 靱性 / 圧子力学 / 高温変形 / クリープ / 応力緩和
Research Abstract

1) The brittleness and the ductility as characteristic material parameters were defind and derived based on an energry principle of indentation contact mechanics. The brittleness/ductility parameter gives a quantitative measure for characterizing the machinability of brittle materials.
2) An apparatus was designed for characterizing the brittleness/ductility parameter and the degree of indentation-induced damage in a wide range of temperatures ranging from room temperature to 1,400゚C.
3) Conducted were the theoretical consideration and experimental work of viscoelatic indentation contact deformation of brittle materials at elevated temperatures. The indentation hysteresis energy was successfully utilized to characterize the viscoelastic behavior of surface deformation.
4) An acoustic microscopy was applied to the surface damage introduced by indentation contact. An analytical method for characterizing the damage evolution has been established.
5) A nonlinear rheological constitutive equation was proposed based on considerations of the grain-boundary sliding and grain interlocking of polycrystalline ceramics with grain-boundary melt at elevated temperatures.
6) An experimental apparatus was designed for examining viscoelastic behavior of polycrystalline materials at elevated temperatures up to 1600゚C.A novel test specimen geometry (double shear geometry) under compressive loading mode makes possible to conduct rheological testing under simple shear deformation. An experimental scrutiny confirmed that the constituteve equation proposed in Item 5) quantitatively predicts the nonlinear viscoelastic behavior associated with grain-boundary sliding and grain interlocking.
7) Toughening processes and mechanisms have been examined via experimental as well as theoretical studies on the mixed-mode fracture and R-curve behavior of several types of ceramics. A novel test technique and a fracture mechanics-based size-effect law were proposed to estimate process zone/wake zone sizes.

Report

(3 results)
  • 1996 Annual Research Report   Final Research Report Summary
  • 1995 Annual Research Report
  • Research Products

    (19 results)

All Other

All Publications (19 results)

  • [Publications] Mototsugu Sakai: "Indentation-Induced Contact Deformation and Damage of Glassy Carbon" J. American Ceramic Society. 78. 1006-1012 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Motohiro Suganuma: "Scanning Acoustic Microscopy of Indentation Damage in Y_2O_3Stabilized Tetragonal Zirconia" J. American Ceramic Society. 78. 2889-2896 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Ming Li: "Mixed-Mode Fracture of Ceramics in Asymmetric Four-Point Ben ding" J. American Ceramic Society. 79. 2718-2726 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Mototsugu Sakai: "Size-Effect on the Fracture Toughness and R-CUrve of Carbon" J. American Ceramic Society. 79. 3177-3184 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Morotsugu Sakai: "Double Shear Geometry for the Deformation and Flow of Ceramics at Elevated Temperatures" J. American Ceramics Society. 79. 449-454 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] 武藤浩行: "多結晶セラミックスの粒界すべりに関するレオロジー" セラミックス協会学術論文誌. 105(印刷中). (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] M.Sakai: "Indentation-Induced Contact Deformation and Damage of Glasslike Carbon" J.Am.Ceram.Soc.78 [4]. 1006-1012 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] M.Suganuma: "Scanning Acoustic Microscopy of Indentation Damage in Y_2O_3-Stabilized Tetragonal Zirconia" J.Am.Ceram.Soc.78 [11]. 2889-2896 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] M.Li: "Mixed-Mode Fracture of Ceramics in Asymmetric Four-Point Bending : Effect of Crack-Face Grain Interlocking/Bridging" J.Am.Ceram.Soc.79 [10]. 2718-2726 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] M.Sakai: "Size-Effect on the Fracture Toughness and the R-Curve of Carbon Materials" J.Am.Ceram.Soc.79 [12]. 3177-3184 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] M.Sakai: "Double-Shear Geometry for the Deformation and Flow of Ceramics at Elevated Temperatures" J.Am.Ceram.Soc.79 [2]. 449-454 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Mototsugu Sakai: "Indentation-Induced Contact Deformation and Damage of Glassy Carbon" J.American Ceramic Society. 78・4. 1006-1012 (1995)

    • Related Report
      1996 Annual Research Report
  • [Publications] Motohiro Suganuma: "Scanning Acoustic Microscopy of Indentation Damage in Y_2O_3-Stabilized Tetragonal Zirconia" J.American Ceramic Society. 78・11. 2889-2896 (1995)

    • Related Report
      1996 Annual Research Report
  • [Publications] Ming Li: "Mixed-Mode Fracture of Ceramics in Asymmetric Four-Point Bending" J.American Ceramic Society. 79・10. 2718-2726 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] Mototsugu Sakai: "Size-Effect on the Fracture Toughness and R-curve of Carbon" J.American Ceramic Society. 79・12. 3177-3184 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] Mototsugu Sakai: "Double Shear Geometry for the Deformation and Flow of Ceramics at Elevated Temperatures" J.American Ceramic Society. 79・2. 449-454 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] 武藤浩行: "多結晶セラミックスの粒界すべりに関するレオロジー" セラミックス協会学術論文誌. 105(印刷中). (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] M.Sakai,H.Mutoh and M.Haga: "Double-Shear Geometry for the Deformation and Flow of Ceramics at Elevated Temperatures" J.Am.Ceram.Soc.79(in press). (1996)

    • Related Report
      1995 Annual Research Report
  • [Publications] M.Suganuma: "Scanning Acoustic Microscopy of Indentation Damage in Y_2O_3-Stabilized Tetragonal Zirconia" J.Am.Ceram.Soc.78. 2889-2896 (1995)

    • Related Report
      1995 Annual Research Report

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Published: 1995-04-01   Modified: 2016-04-21  

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