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Development of Control Method of Interface of h-BN Composites by Fracto-emission Analysis

Research Project

Project/Area Number 07555204
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section試験
Research Field Composite materials/Physical properties
Research InstitutionTokyo Institute of Technology

Principal Investigator

MATSUO Yahtaro  Tokyo Institute of Technology Dept.Inorg.Mater.Prof., 工学部, 教授 (70016608)

Co-Investigator(Kenkyū-buntansha) YASUDA Kouichi  Tokyo Institute of Technology, Dept.Inorg.Mater.Ass, Prof, 工学部, 助教授 (20191306)
FUKUNAGA Osamu  Tokyo Institute of Technology, Dept.Inorg.Mater.Prof., 工学部, 教授 (20199251)
Project Period (FY) 1995 – 1996
Project Status Completed (Fiscal Year 1996)
Budget Amount *help
¥15,700,000 (Direct Cost: ¥15,700,000)
Fiscal Year 1996: ¥3,000,000 (Direct Cost: ¥3,000,000)
Fiscal Year 1995: ¥12,700,000 (Direct Cost: ¥12,700,000)
KeywordsCeramic Composite / Interface Control / h-BN / fracto-emission / フラクトエミッション / フラクトミッション
Research Abstract

The aim of this research is to develop a high performance long fiber reinforced ceramic matrix composites which has excellent oxidation resistance, high strength and high toughness than C/C composites by controlling interfaces using fracto-emission analysis method. The main results obtained in this research are as follows ;
1. Main equipment, the fracto-emission analysis system, was designed and produced. This equipment has probes for detecting electrons and photons.
2. The optimum condition for making the most dense h-BN matrix system was found as h-BN : 60wt%, Si3N4 : 28wt%, SiO2 : 12wt% and Y203 : 3wt% under the hotpressing temperature 1,800゚C.
3. Carbon fiber reinforced h-BN matrix composites were fabricated. The strength of this new composite was measured under the conditions from the room temperature to 1,600゚C.The strength at 1,600゚C was double the value of room temperature, namely, 350MPa. A model based on the special natures of interfaces was presented for describing this phenomena.
4. The optimum condition for fabricating the h-BN matrix composites was tried and succeeded in improving the room temperature strength significantly.

Report

(3 results)
  • 1996 Annual Research Report   Final Research Report Summary
  • 1995 Annual Research Report
  • Research Products

    (24 results)

All Other

All Publications (24 results)

  • [Publications] Sang-Dong KIM: "Evaluation of High-temperature Properties of Cf/hBN Composites" Proc. of the 12th Japan-Korea Seminor on Ceramics. 425-428 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] 関口豊: "き裂と分散粒子の相互作用とその場観察" セラミックス基礎討論会予稿集. IA-2. 4-5 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] 松尾陽太郎: "微小引張り試験片を用いたセラミックスの界面破壊じん性評価" 第4回機械材料・材料加工技術講演会予稿集. 151-152 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] 田中諭: "C/Cコンポジットの引張りおよび層間せん断破壊エネルギーと黒鉛化度" 日本セラミックス協会1996年会講演予稿集. 3B03. 478- (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] 石本卓二: "BおよびCを焼結助剤に用いた高強度hBNの作製" 日本セラミックス協会第12回関東支部研究発表会. 1B15. 34- (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] 安田公一: "Introduction to Fractoemission" 第34回炭素材料に関する夏季セミナー予稿集. 76-87 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] J.Tatami, et al.: "Influence of Crack Propagation Path on the Fracture Toughness of Ceramic Composite" Proc.Japan-US CCM-VII. 135-142 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] S-D.Kim, et al.: "Evaluation of High-temperature Properties of Cf/hBN Composites" Proc.of the 12^<th> Japan-Korea Seminar on Ceramics. 425-428 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] K.Yasuda, et.al.: "Introduction to Fracto-emission" Proc.of The 34^<th> Summer Seminar on Carbon. 76-87 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] L.Yasuda, et al.: "Influence of Crack Path on Fracture Toughness of Polycrystaline A1203" Fracture Mechanics of Ceramics. Vol.11(Plenum Press). 315-330 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Akatsu, Et.al: "The R-curve Behavior of Vickers-Indentation Cracks in an SiC-Whisker Re-inforced Alumina Composite" Rept.of the Res.Lab.of Eng.after., T.I.T.No.21. 55-61 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] F.Takase, et.al: "Analysis of Change of Coordination Numbers of Particles compacted by Cyclic CIP using Marcov process" Proceeding of Ceramic basic science. 256-257 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] A.Miyata, et al.: "Compressive Deformation Properties of Ceramic Granule and the Relation with Compaction and Sinterability" Annual meeting of The Ceramic Society of Japan. 183 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Sang-Dong KIM: "Evaluation of High-temperature Properties of Cf/hBN Composites" Proc.of the 12th Japan-Korea Seminor on Ceramics. 425-428 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] 関口 豊: "き裂と分散粒子の相互作用とその場観察" セラミックス基礎討論会予稿集. IA-2. 4-5 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] 松尾陽太郎: "微小引張り試験片を用いたセラミックスの界面破壊じん性評価" 第4回機械材料・材料加工技術講演会予稿集. 151-152 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] 田中 諭: "CICコンポジットの引張りおよび層間せん断破壊エネルギーと黒鉛化度" 日本セラミックス協会1996年会講演予稿集. 3B03. 478- (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] 石本 卓二: "BおよびCを焼結助剤に用いた高強度hBNの作製" 日本セラミックス協会第12回関東支部研究発表会. 1B15. 34- (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] 安田 公一: "Introduction to Fractoemission" 第34回炭素材料に関する夏季セミナー予稿集. 76-87 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] 松尾陽太郎: "長繊維強化セラミック複合材料の実破壊エネルギー評価" 日本機械学会講演論文集. 95-14. 74-75 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] 熊谷祥: "反応性焼結助剤を用いたhBNの焼結" 日本セラミックス協会1995年会講演予稿集. 32 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] 田中諭: "C/Cコンポジットの破壊エネルギーのモード分離" 日本セラミックス協会1995年会講演予稿集. 70 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] 安田公一: "C/C複合材料の力学的性質に及ぼすSiC被覆の影響" 日本複合材料学会1995年度年会講演予稿集. 65-66 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] 田中諭: "長繊維強化複合材料の破壊エネルギーの新評価法" 日本複合材料学会1995年度年会講演予稿集. 73-74 (1995)

    • Related Report
      1995 Annual Research Report

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Published: 1995-04-01   Modified: 2016-04-21  

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