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Development of AE monitoring system for optimal sintering conditions of ceramics

Research Project

Project/Area Number 07555215
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section展開研究
Research Field Material processing/treatments
Research InstitutionResearch Center for Advanced Science and Technology, The University of Tokyo

Principal Investigator

ENOKI Manabu  The University of Tokyo, RCAST,Associate Professor, 先端科学技術研究センター, 助教授 (70201960)

Co-Investigator(Kenkyū-buntansha) MIYA Takekazu  Sonnotec, Senior Manager, 研究開発部, 部長
SHIMIZU Yuhoh  NF Circuit Design Block, Senior Researcher, 主任研究員
KISHI Teruo  National Institute for Advanced Interdisciplinary Research, Director General, 産業技術融合領域研究所, 社長 (40011085)
岸 照雄  工業技術院, 産業技術融合領域研究所, 所長
Project Period (FY) 1995 – 1997
Project Status Completed (Fiscal Year 1997)
Budget Amount *help
¥6,400,000 (Direct Cost: ¥6,400,000)
Fiscal Year 1997: ¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 1996: ¥3,000,000 (Direct Cost: ¥3,000,000)
Fiscal Year 1995: ¥2,800,000 (Direct Cost: ¥2,800,000)
KeywordsAcoustic Emission / Ceramics / Hot-Press / Sintering / アコースティックエミッション
Research Abstract

It becomes a severe problem that many microcracking occur due to the stress induced by the different of thermal coefficients between matrix and particles during cooling period of processing of ceramics and ceramics matrix composites by hot-press. The sintering conditions of processing or cooling rate are determined by try and error to avoid these microcracks. However, these processies are not efficient and there are a lot of loss in energy. Non-destructive monitoring of sintering is promising to avoid this problem. Acoustic emission (AE) is an emission of elastic wave due to cracking and it has been used for the research of microfracture of materials and the monitoring of integrity of components. Many research have been reported on the processing of particle dispersed ceramic and glass matrix compoxites. However, there were a few reports on the detail of microfracture mechanism. More experimental analysis of microfracture and quantitative eveluation are needed to develop these materials. In this research, several types of particle dispersed ceramic and glass composites were fabricated and AE signals during bending test and fracture toughness test were analyzed. Micrlfracture of these materials were eveluated by inverse analysis of AE waveform. Finally microfracture process and mechanical properties of these materials were quantitatively evaluated and the mechanism of strenthening and thoghening were quantitatively discussed. These results will lead the improvement of these materials.

Report

(4 results)
  • 1997 Annual Research Report   Final Research Report Summary
  • 1996 Annual Research Report
  • 1995 Annual Research Report
  • Research Products

    (21 results)

All Other

All Publications (21 results)

  • [Publications] K.Kageyama, M.Enoki and T.Kishi: "Numerical Simulation of Toughening by Crack Deflection and Bowing of Glass Matrix-Alumina Particulate Composite" Journal of the Ceramic Society of Japan. 103. 1237-1243 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] B.-K.Jang, H.K.Oh, M.Enoki and T.Kishi: "Effect of Second Phase on Mechanical Properties and Toughening of Al_2O_3 Based Ceramic Composites" Composites Engineering. 5. 1275-1286 (1995)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] B.-N.Kim, Y.Katsukawa, M.Enoki and T.Kishi: "The Stable Crack Growth in SiC Particle-Dispersed Al_22O_3 Composites" Journal of the Ceramic Society of Japan. 104. 974-978 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] M.Enoki and T.Kishi: "Evaluation of Stochastic Microfracture Process of Particle Dispersed Composites" Materials Transactions,JIM. 37. 399-403 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] H.Fujita, M.Enoki and T.K: "Microfracture Analysis of SiC Reinforced Glass Composites by Acoustic Emission" Materials Transactions,JIM. 37. 776-781 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] T.Kishi and M.Enoki: "Development of Ceramic Matrix Composites and the Meaning of Microcracks" Key Engineering Materials. 127-131. 63-72 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] B.-N.Kim, M.Watanabe, M.Enoki and T.Kishi: "2-Dimensional Simulation of Crack Propagation in Al_2O_3 MatrixComposites Dispersed with SiC Particles" Key Engineering Materiales. 127-131. 1153-1158 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] K.Kageyama, M.Enoki and T.Kishi: "Numerical Simulation of Toughening by Crack Deflection and Bowing of Glass Matrix-Alumina Particulate Composite" Journal of the Ceramic Society of Japan. 103. 1237-1243 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] B.-K.Jang, H.K.Oh, M.Enoki and T.Kishi: "Effects of Second Phase on Mechanical Properties and Toughening of Al_2O_3 Based Ceramic Composites" Composites Engineering. 5. 1275-1286 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] B.-N.Kim, Y.Katsukawa, M.Enoki and T.Kishi: "The Stable Crack Growth in SiC Particle-Dispersed Al_2O_3 Composites" Journal of the Ceramic Society of Japan. 104. 974-978 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] M.Enoki and T.Kishi: "Evaluation of Stochastic Microfracture Process of Particle Dispersed Composites" Materials Transactions, JIM. 37. 399-403 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] H.Fujita, M.Enoki and T.Kishi: "Microfracture Analysis of SiC Reinforced Glass Composites by Acoustic Emission" Materials Transactions, JIM. 37. 776-781 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] T.Kishi and M.Enoki: "Development of Ceramic Matrix Composites and the Meaning of Microcraks" Key Engineering Materials. 127-131. 63-72 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] B.-N.Kim, M.watanabe, M.Enoki and T.Kishi: "2-Dimensional Simulation of Crack Propagation in Al_2O_3 Matrix Composites Dispersed with SiC Particles" Key Engineering Materials. 127-131. 1153-1158 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] B.-N.Kim, Y.Katsukawa, B.-W.Ahn, M.Enoki and T.Kishi: "Evaluation of R-Curve Behavior from Indented Strength in SiC Particle-Dispersed Al_2O_3 Composite" Key Engineering Materials. 127-131. 889-894 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] A.Rabiei, B.-N.Kim, M.Enoki and T.Kishi: "A New-Method Based on Simultaneous Acoustic-Emission and insitu SEM Observation to Evaluate the Fracture-Behavior of Metal-Matrix" Composites,Scripta Materialia. 37. 801-808 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] M.Enoki and T.Kishi: "Evaluation of Stochastic Microfracture Process of Particle Dispersed Composites" Materials Transactions,JIM. 37. 399-403 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] B.-N.Kim,M.Watanabe,M.Enoki and T.Kishi: "Simulation of Crack PropagationProcess in Particle-Dispersed Composites." Materials Transactions,JIM. 37. 404-408 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] M.C.Nandy,T.Nose,M.Enoki and T.Kishi: "R-Curve and Cyclic Fatigue Behavior in Alumina-Particles-Reinforced Silicon Carbide." Materials Transactions,JIM. 37. 769-775 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] M. Enok: "Acoustic Emission Analysis of TiAl Intermetallics" Journal. of Acoustic Emission.13. 29-34 (1995)

    • Related Report
      1995 Annual Research Report
  • [Publications] 榎 学: "AEによる粒子分散ガラス基複合材料の微視破壊評価" 第10回アコースティックエミッション総合コンファレンス論文集. 219-224 (1995)

    • Related Report
      1995 Annual Research Report

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Published: 1995-04-01   Modified: 2016-04-21  

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