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Development of a Large-Diameter Thermal Plasma Processing Device and its Application to Synthesis of Thermoelectric Materials

Research Project

Project/Area Number 07558066
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section試験
Research Field プラズマ理工学
Research InstitutionYamaguchi University

Principal Investigator

FUKUMASA Osamu  Yamaguchi University, Faculty of Engineering, Professor, 工学部, 教授 (20026321)

Co-Investigator(Kenkyū-buntansha) MIYAMURA Koh  Japan Ultra-high Temperature Materials Research Center (JUTEM), Chief Researcher, 山口研究所, 研究部長
SAKIYAMA Satoshi  Yamaguchi University, Faculty of Engineering, Research Associate, 工学部, 助手 (60162327)
KOYANAGI Tsuyoshi  Yamaguchi University, Faculty of Engineering, Associate Professor, 工学部, 助教授 (90178385)
Project Period (FY) 1995 – 1996
Project Status Completed (Fiscal Year 1996)
Budget Amount *help
¥6,700,000 (Direct Cost: ¥6,700,000)
Fiscal Year 1996: ¥1,800,000 (Direct Cost: ¥1,800,000)
Fiscal Year 1995: ¥4,900,000 (Direct Cost: ¥4,900,000)
Keywordsplasma jet / low-pressure thermal plasma processing / plasma spraying / alkari metal thermoelectric converter / beta" -alumina / computer tomography / diamond synthesis / アルカリ金属熱電変換 / β"アルミナ / コンピュータートモグラフィー
Research Abstract

Thermal plasma jet operated under reduced pressure has a great potential for synthesizing new materials, because of its high speed, high gas temperature and large plasma volume. Therefore, we have newly designed the plasma reactor composed of the forced constricted type plasma jet generator and the feed ring. In order to clarify the application feasibility of this reactor to fine plasma processing for materials, the behavior of the plasma jet has been discussed.
Findings are as follows :
(1) Under low pressure, high temperature and high velocity regions of the plasma jet are expanded. With the use of this expanding plasma jet, the dense film without vesicles is obtained and the film thickness is easily controlled.
(2) Under low pressure, the hardness and the adhesion strength of functionally gradient materials are found to be high.
(3) Under not only atmospheric pressure but also low pressure, thin-films of beta" -alumina are successfully synthesized from the powder mixtures, i.e.alpha-Al_2O_3, Na_2CO_3 and MgO.Synthesis of beta" -alumina depends on jet power and the distance from the feed ring exit to the substrate.
(4) When pure diamond films are synthesized, the ratio of CH_4 flow rate to H_2 flow rate is lower than a certain critical value. Namely, the intensity of CH/H_<alpha> in the vicinity on the substrate has strong effect on pure diamond film deposition.
(5) The computer tomography technique should be applicable to the diagnostics of asymmetric plasma jets.

Report

(3 results)
  • 1996 Annual Research Report   Final Research Report Summary
  • 1995 Annual Research Report
  • Research Products

    (14 results)

All Other

All Publications (14 results)

  • [Publications] 福政 修: "直流熱プラズマとその材料プロセスへの応用" プラズマ・核融合学会誌. 72. 236-242 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] S.Sakiyama: "Diagnostics of the Plasma Jet using Computer Tomography" Proc.Inter.Conf.Plasma Physics. (in press). (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] S.Sakiyama: "Spectroscopic Measurement of DC Plasma Jet in Diamond Synthesis" Jpn.J.Appl.Phys.36(in Press). (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] 福政 修 他: "熱プラズマ材料プロセシング基礎と応用" (株)信山社サイテック, 351 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Osamu Fukumasa: "Synthesis of Thermoelectric Materials Using Low Pressure Plasma Jet (II)" Proc.13th Symp.Plasma Processing. Vol.13. 157-160 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Satoshi Sakiyama: "Fabrication of Functionally Gradient Materials by Plasma Spraying" Proc.13th Symp.Plasma Processing. Vol.13. 263-266 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Osamu Fukumasa: "DC Thermal Plasma and their Application to Plasma Processing for Materials" Journal of Plasma and Fusion Research. Vol.72. 236-242 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Satoshi Sakiyama: "Diagnostics of the Plasma Jet using Computer Tomography" Proc.Inter.Conf.Plasma Physics. (in press). (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Satoshi Sakiyama: "Spectroscopic Measurement of DC Plasma Jet in Diamond Synthesis" Japanese Journal of Applied Physics. Vol.36 (in press). (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] Osamu Fukumasa et al.: Introduction and Application to Thermal Plasma Material Processing (in Japanese). Shinzansya Saitekku Co., 351 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1996 Final Research Report Summary
  • [Publications] S.Sakiyama: "Diagnostics of the Plasma Jet using Computer Tomography" Proc.Inter.Conf.Plasma Physics. (in press). (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] S.Sakiyama: "Spectroscopic Measurement of DC Plasma Jet in Diamond Synthesis" Jpn.J.Appl.Phys.36(in press). (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] 福政 修: "直流熱プラズマとその材料プロセスへの応用" プラズマ・核融合学会誌. 72. (1996)

    • Related Report
      1995 Annual Research Report
  • [Publications] 福政 修 他: "熱プラズマ材料プロセシングの基礎と応用" (株)信山社サイテック, (1996)

    • Related Report
      1995 Annual Research Report

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Published: 1995-04-01   Modified: 2016-04-21  

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