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ELECTRON,ION AND PHOTON EMISSION FROM FRESH SURFACES OF METAL ACCOMPANYING DEFORMATION AND FRACTURE

Research Project

Project/Area Number 08455047
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Applied physics, general
Research InstitutionKANSAI UNIVERSITY

Principal Investigator

NAKAHARA Sumio  KANSAI UNIVERSITY,FACULTY OF ENGINEERING,ASSOCIATE PROFESSOR, 工学部, 助教授 (90067760)

Co-Investigator(Kenkyū-buntansha) OWAKI Shigehiro  UNIVERSITY OF OSAKA PREFECTURE,COLLEGE OF INTEGRATED ARTS AND SCIENCE,PROFESSOR, 総合科学部(平成8年度), 教授 (50029873)
KIMURA Yoshitake  KONAN UNIVERSITY,FACULTY OF SCIENCE,PROFESSOR, 理学部(平成9年度,10年度), 教授 (30068085)
Project Period (FY) 1996 – 1998
Project Status Completed (Fiscal Year 1998)
Budget Amount *help
¥7,700,000 (Direct Cost: ¥7,700,000)
Fiscal Year 1998: ¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 1997: ¥1,900,000 (Direct Cost: ¥1,900,000)
Fiscal Year 1996: ¥5,200,000 (Direct Cost: ¥5,200,000)
KeywordsDEFORMATION / FRACTURE / ELECTRON EMISSION / ATOMIC FORCE MICROSCOPY / LOW TEMPERATURES / ELECTRONIC SPECKLE PATTERN INTERFEROMETRY / STRAIN / THERMAL EXPANSION / スペックルパターン干渉法 / 熱,ひずみ / 熱膨張率 / 電子放出 / 新生面 / 真空 / スペックル干渉法 / 熱ひずみ / スペックルパターン / ひずみ / AFM(原子間力顕微鏡)
Research Abstract

We examined the use of chemisorptive emission (electron emission accompanying the adsorption of a reactive gas on a metal surface) and atomic force microscopy as measures of plastic deformation during fracture along a metallic Mg/glass interface. Localized ductile deformation in the metallic phase enhances the fracture energy, exposes metallic Mg to the reactive O_2 atmosphere, and produces intense emission. The number of electrons emitted following fracture in low-pressure oxygen atmospheres is strongly correlated with the total energy expended during failure (peel energy). The presence of localized ductile deformation is verified by atomic force microscopy (AFM) : voids are observed on surfaces yielding significant emissions and enhanced fracture energies. These voids are not observed on samples yielding the lowest peel energies and emission intensities, i.e., where the contribution of deformation to the peel energy is negligible. The potential for chemisorptive electron emission (CS … More E) as a probe of deformation along interfaces involving Mg, Ti, and Al is promising.
Electronic speckle pattem inteferometry (ESPI) has been applied to the measurement of deformation, strain, and thermal expansion during the cooling down and warming up processes between room temperature and low temperatures (minimum -20K). Samples are several commercial available metallic (SUS, Al, and Ti) and non-metallic (FRP, Alunina, Teflon, and SiO_2) materials. The ESPI method offers a non-contact and temperature-independent method to measure the displacement of materials subject to large temperature changes, as long as the correlations of the speckle patterns are kept. This metod presents an essential advantage over the conventional ones in that the information remains recorded on the video tape recorder for further analysis. The mechanical behavior of structural materials due to the thermal deformation are successfully measured during the cooling down or warming up processes, and applicability of ESPI methods to the low temperature engineering are experimentally confirmed. Less

Report

(4 results)
  • 1998 Annual Research Report   Final Research Report Summary
  • 1997 Annual Research Report
  • 1996 Annual Research Report
  • Research Products

    (28 results)

All Other

All Publications (28 results)

  • [Publications] Sumio Nakahara, et. al.: "Deformation measurement of several materials in cooling processes from room temperature to 77K using electronic speckle pattern interferometry" Akademie Verlag Series in Optical Metrology. Vol.2. 170-175 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Fukuda, et. al.: "Estimation of ultraviolet radiation dose using CaF_2 : Tb phosphor" Radiation Protection Dosimetry. Vol.65 No.1-4. 325-328 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Narayanan Srinivasan, et. al.: "Tunable hear-infrared and visible all-solid-state optical parametric oscillator amplifier system based on potassium titanyl phosphate crystal" Japanese Journal Applied Physics. Vol.35 No.9A. 4639-4644 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Sumio Nakahara, et. al.: "Strain measurements of stainless steel at low temperatures using electronic speckle pattern interferometry" Proceeding of the 16th ICEC/ICMC (Elsevier Science). Part.1. 665-668 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Shigehiro Owaki, et. al.: "Metallic Na formation in/on NaCl crystals with irradiation by electron or vacuum ultraviolet photons" Radiation Physics and Chemistry. Vol.49 No.6. 609-615 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 満富慎介 他: "レーザーアブレイションを用いたイオン源の開発に関する研究" Memoirs of Konan University, Science Series. Vol.44 No.1. 113-120 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 松下 晃 他: "レーザーアブレイションを用いたイオン源の開発に関する研究II" Memoirs of University, Science Series. Vol.44 No.2. 35-44 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Sumio Nakahara, et. al.: "Thermal contraction coefficient measurement technique of several materials at low temperatures using electronic speckle pattern interferometry" Advances in Cryogenic Engineering (Materials). Vol.44A. 359-366 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 中原住雄 他: "フラクト放射を用いた低温下の有機複合材料の変形・破壊の検出" 技苑. No.97. 14-17 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Sumio Nakahara, et.al.: "Deformation measurement of several materials in cooling processes from room temperature to 77K using electronic speckle pattern interferometry" Akademie Verlag Series in Optical Metrology. Vol.2. 170-175 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Yasunori Fukuda, et.al.: "Estimation of ultraviolet radiation dose using CaF2 : Tb phosphor" Radiation Protection Dosimetry. Vol.65, No.1-4. 325-328 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Narayanan Srinivasan, et.al.: "Tunable near-infrared and visible all-solid-state optical parametric oscillator amplifier system based on potassium titanyl phosphate crystal" Japanese Journal Applied Physics. Vol.35, No.9A. 4639-4644 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Sumio Nakahara, et.al.: "Strain measurements of stainless steel at low temperatures using electronic speckle pattern interferometry" Proceeding of the 16th ICEC/ICMC (Elsevier Science). Part 1. 665-668 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Shigehiro Owaki, et.al.: "Metallic Na formation in/on NaCl crystals with irradiation by electron or vacuum ultraviolet photons" Radiation Physics and Chemistry. Vol.49, No.6. 609-615 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Sinsuke Mitsutomi, et.al.: "Study on development of an ion source by pulsed laser ablation (in Japanese)" Memoirs of Konan University, Science Series. Vol.44, No.1. 113-120 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Akira Matsushita, et.al.: "Study on development of an ion source by pulsed laser ablation II (in Japanese)" Memoirs of Konan University, Science Series. Vol.44, No.2. 35-44 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Sumio Nakahara, et.al.: "Thermal contraction coefficient measurement technique of several materials at low temperatures using electronic speckle pattern interferometry" Advances in Cryogenic Engineering(Materials). Vol.44A. 359-366 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Sumio Nakahara, et.al.: "Deformation and fracture detection of FRP at low temperatures using fracto-emission (in Japanese)" Gien(Kansai University). No.97. 14-17 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Sumio Nakahara et al.: "Thermal Contraction Coefficient Measurement Technique of Several Materials at Low Temperatures Using Electronic Speckle Pattern Interferometry" Advances in Cryogenic Engineering Materials. Vol.44. 359-366 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 中原,住雄 他: "フラクト放射を用いた低温下の有機複合材料の変形・破壊の検出" 技苑. 97号. 14-17 (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] Sumio Nakahara, et al.: "Thermal contraction coefficient measurement technique of several materials at low temperatures using electronic speckle pattern interferometry" Advances in Cryugenic Engineering Materials. Vol.44. in print (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] 松下,晃, 他: "レーザーアブレーションを用いたイオン源の開発に関する研究II" 甲南大学紀要 理学部編. 44(2). 35-44 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] 満冨,慎介, 他: "レーザーアブレーションを用いたイオン源の開発に関する研究" 甲南大学紀要 理学部編. 44(1). 113-120 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Sumio Nakahara, et al.: "Strain measurements of stainless steel at low temeperatures using electronic speckle pattern interferometry" Proceedings of the 16th ICEC/ICMC(Elsevier Science). part1.665-668 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Sumio Nakahara et al.: "Strain Measurements of Stainless Steel at Low Temperatures Using Electronic Speckle Pattern Interferometry" The ICEC 16/ICMC Proceedings. (in print). (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] Sumio Nakahara et al.: "Deformation Measurement of Several Materials in Cooling Processes from Room Temperature to 77K using Electronic Speckle Pattern Interferometry" Akademic Verlag Series in Optical Metrology Simulation and Experiment in Laser Metrology. 2. 170-175 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] Yasunori Fukuda et al.: "Estimation of ultraviolet radiation dose using CaF2 : Tb phosphor" Radiation Protection and Dosimetry. 65. 325-328 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] Narayanan Srinivasan et al.: "Tunable near-infrared and visible all-solid-state optical parametric oscillator amplifier system based on pottasium titanyl phosphate crystal" Japanese Journal of Applied Physics. 35. 4639-4644 (1996)

    • Related Report
      1996 Annual Research Report

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Published: 1996-04-01   Modified: 2016-04-21  

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