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Microstructural Design of Two Phase Titanium Aluminides for High Temperature Applications

Research Project

Project/Area Number 08455313
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionTOHOKU UNIVERSITY

Principal Investigator

MARUYAMA Kouichi  Tohoku University, Graduate School of Engineering, Professor, 大学院・工学研究科, 教授 (90108465)

Co-Investigator(Kenkyū-buntansha) SATO Hiroyuki  Tohoku University, Graduate School of Engineering, Lecturer, 大学院・工学研究科, 講師 (10225998)
KOIKE Jun-ichi  Tohoku University, Graduate School of Engineering, Associate Professor, 大学院・工学研究科, 助教授 (10261588)
OIKAWA Hiroshi  Tohoku University, Graduate School of Engineering, Professor, 大学院・工学研究科, 教授 (30005243)
Project Period (FY) 1996 – 1998
Project Status Completed (Fiscal Year 1998)
Budget Amount *help
¥7,700,000 (Direct Cost: ¥7,700,000)
Fiscal Year 1998: ¥1,100,000 (Direct Cost: ¥1,100,000)
Fiscal Year 1997: ¥3,100,000 (Direct Cost: ¥3,100,000)
Fiscal Year 1996: ¥3,500,000 (Direct Cost: ¥3,500,000)
KeywordsHigh Temperature Structural Materials / High Temperature Creep / Titanium Aluminides / Alloy Design / Microstructural Control / Lamellar Microstructure / Materials Database / データベース
Research Abstract

TiAl alloys consists of gammaTiAl and alpha_2Ti_3Al phases, and are considered to be a candidate for high temperature structural applications. A further improvement of their high temperature mechanical properties is required for their engineering applications, For the improvement, it is important to know how to optimize their microstructure. In this research, the correlation between the microstructures and high temperature mechanical properties were studied, and the following results were obtained.
1. Creep strength of TiAl alloys is independent of grain size for grain sizes greater then 100mum. In the grain size range smaller than 100mum, their creep strength may decrease with decreasing grain size.
2. Creep strength of TiAl alloys is insensitive to the volume fraction of constituent phases, in other words, aluminum concentration.
3. Creep strength of fully lamellar TiAl alloys is improved by the refinement of their lamellar spacing. At low stresses, however, the high creep strength of f … More ine lamellar microstructure disappears due to the significant degradation of the fine lamellar microstructure. Dynamic recrystallization and discontinuous coarsening of lamellar microstructure during creep are responsible for the degradation, and the consequent weakening of the fine lamellar microstructure.
4. The lamellar microstructure can be stabilized by annealing at a high temperature. The stabilization treatment prevent the microstructural degradation during creep, and the strengthening by lamellar refinement becomes effective even at low stresses.
5. Creep strength of PST crystals, having only one lamellar colony, depends strongly on the angle between the stress axis and the lamellar plates. The hard oriented crystal, whose lamellar plates are aligned parallel or perpendicular to the stress axis, provides substantially higher creep strength than randomly oriented polycrystalline TiAl alloys. The soft oriented crystal, having an intermediate angle of stress axis to the lamellar plates, shows similar creep strength to the polycrystals. This result suggests that creep strength of polycrystalline TiAl alloys can be improved by the control of their texture. Less

Report

(4 results)
  • 1998 Annual Research Report   Final Research Report Summary
  • 1997 Annual Research Report
  • 1996 Annual Research Report
  • Research Products

    (33 results)

All Other

All Publications (33 results)

  • [Publications] Y.Nagae: "General Creep Characteristics of α_2 Single-Phase Polycrystalline Intermetallics" Mater.Sci.Eng.A213. 32-36 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] K.Maruyama: "Effects of Lamellar Spacing, Volume Fraction and Grain Size on Creep Strength of Fully Lamellar TiAl alloys" Mater.Sci.Eng.A239/240. 419-428 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] R.Yamamoto: "Effects of Stress and Temperature on Lamellar Spacing Dependent Creep Strength of Fully Lamellar TiAl Alloys" Proc.International Conference on Thermomechanical Processing. 1559-1565 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] R.Yamamoto: "Effects of Volume Fraction of Constituent Phases of Fully Lamellar TiAl Alloys on Creep Strength" Proc.Third Pacific Rim International Conference on Advanced Materials and Processing. 2343-2348 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] R.Yamamoto: "Effects of Discontinuous Coarsening of Lamellae on Creep Strength of Fully Lamellar TiAl Alloys" Intermetallics. 6・7-8. 699-702 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 後藤時政: "TiAl金属間化合物のX線応力測定における粗大結晶粒対策および加工表面への適用限界" 材料. 47・11. 1170-1177 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 丸山公一: "高温強度の材料科学・クリープ理論と実用材料への適用" 内田老鶴圃, 329 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Nagae: "General Creep Characteristics of alpha_2 Single-Phase Polycrystalline Intermetallics" Mater.Sci.Eng.vol.A213. 32-36 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] K.Maruyama: "Effects of Lamellar Spacing, Volume Fraction and Grain Size on Creep Strength of Fully Lamellar TiAl alloys" Mater.Sci.Eng.vol.A239/240. 419-428 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] R.Yamamoto: "Effects of Stress and Temperature on Lamellar Spacing Dependent Creep Strength of Fully Lamellar TiAl Alloys" Proc.International Conference on Thermomechanical Processing. 1559-1565 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] R.Yamamoto: "Effects of Volume Fraction of Constituent Phases of Fully Lamellar TiAl Alloys on Creep Strength" Proc.Third Pacific Rim International Conference on Advanced Materials and Processing. 2343-2348 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] R.Yamamoto: "Effects of Discontinuous Coarsening of Lamellae on Creep Strength of Fully Lamellar TiAl Alloys" Intermetallics. vol.6, No.7-8. 699-702 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] T.Goto: "Coarse Grain Measures and Limit of Application to Worked Surface on X-ray Stress Measurement for TiAl Intermetallic Compound" J.Soc.Mater.Sci.Japan. vol.47, No.11. 1170-1177 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] K.Maruyama: Materials Science of High Temperature Strength - Creep Theories and its Practical Applications. Uchida Rokakuho, 329 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Ryuichi Yamamoto: "High Temperature Mechanical Properties of Hot Pressed TiN with Fine Grain Size" J.Materials Science. 33・8. 2047-2052 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] R.Yamamoto: "Effects of Volume Fraction of Constituent Phases of Fully Lamellar TiAl Alloys on Creep Strength" Proc.Third Pacific Rim International Conference on Advanced Materials and Processing. 2343-2348 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] R.Yamamoto: "Effects of Discontinuous Coarsening of Lamellae on Creep Strength of Fully Lamellar TiAl Alloys" Intermetallics. 6・7-8. 699-702 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 後藤時政: "TiAl金属間化合物のX線応力測定における粗大結晶粒対策および加工表面への適用限界" 材料. 47・11. 1170-1177 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] R.Yamamoto: "Importance of Microstructural Stability to Creep Strength of Fully Lamellar TiAl Alloy" Gamma Titanium Aluminides. (印刷中). (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] G.Wegmann: "Effect of the Lamellar Orientation on the Creep Resistance in Polysynthetically Twinned(PST)Ti-48mol%Al" Gamma Titanium Aluminides. (印刷中). (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] J.Koike: "Influence of Liquid-Phase Inclusion on High-Temperature Deformation Behavior in Al-Bi Alloys" Mater.Sci.Eng. A234-236. 525-528 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] 丸山公一: "TiAl基軽量耐熱金属間化合物" 日本学術振興会第123委員会研究報告. 38・3. 287-297 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] K.Maruyama: "Examination of Deformation Mechanism Maps in 2.25Cr-1Mo Steel by Creep Tests at Strain Rates of 10^<-11>_s^<-1> TO 10^<-6>_s^<-1>" Mater.Sci.Eng.A224. 166-172 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] K.Maruyama: "Effects of Lamellar Spacing,Volnme Fraction and Grain Size on Creep Strength of Fully Lamellar TiAl alloys" Mater.Sci.Eng.A(印刷中). (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] R.Yamamoto: "Effects of Stress and Temperature on Lamellar Spacing Dependent Creep Strength of Fully Lamellar TiAl Alloys" Proc.International Conference on Thermomechanical Processing. (印刷中). (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] Ryuichi Yamamoto: "High Temperature Mechanical Properties of Hot Pressed TiN with Fine Grain Size" J.Materials Science. (印刷中). (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] 丸山公一: "高温強度の材料科学-クリープ理論と実用材料への適用" 内田老鶴圃, 329 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Y. Nagae: "General Creep Characteristics of α_2 Single-Phase Polycrystalline Intermetallics" Mater. Sci. Eng.A213. 32-36 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] J. Koike: "High Temperature Strength of αTi-Al Alloys with a Locally Ordered Structure" Mater. Sci. Eng.A213. 98-102 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] 丸山公一: "TiAlのクリープ変形とクリープ強度" まてりあ. 35. 1070-1076 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] 山本隆一: "完全ラメラ組織TiAl合金の高温使用を目的として組織設計" 日本学術振興会第123委員会研究報告. 37. 203-210 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] K. Maruyama: "Influence of composition on creep of alpha-two Ti_3Al polycrystals" Proc. of the 8th World conference on Titanium (The Inst. Mat.). 348-355 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] 丸山公一: "TiAl系単相材および2相材のクリープ" 金属間化合物-新高温材料としての可能性-(日本金属学会). 194-202 (1996)

    • Related Report
      1996 Annual Research Report

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Published: 1996-04-01   Modified: 2016-04-21  

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