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DEVELOPMENT OF HIGH SENSITIVITY LASER ICP MASS SPECTROMETER FOR ZIRCON CHRONOLOGY

Research Project

Project/Area Number 08554017
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section展開研究
Research Field Petrology/Mineralogy/Science of ore deposit
Research InstitutionTOKYO INSTITUTE OF TECHNOLOGY

Principal Investigator

YURIMOTO Hisayoshi  Department of Earth and Planetary Sciences, Tokyo Institute of Technology, Associate Professor, 理学部, 助教授 (80191485)

Co-Investigator(Kenkyū-buntansha) MARUYAMA Shigenori  Department of Earth and Planetary Sciences, Tokyo Institute of Technology, Profe, 理学部, 教授 (50111737)
MATSUMOTO Kazuya  Olympus Optical Co., Ltd., Development Group 1, Chief Manager, 応用研究部・電子デバイス室, 室長
HIRATA Takafumi  Department of Earth and Planetary Sciences, Tokyo Institute of Technology, Assia, 理学部, 助手 (10251612)
Project Period (FY) 1996 – 1997
Project Status Completed (Fiscal Year 1997)
Budget Amount *help
¥16,500,000 (Direct Cost: ¥16,500,000)
Fiscal Year 1997: ¥4,900,000 (Direct Cost: ¥4,900,000)
Fiscal Year 1996: ¥11,600,000 (Direct Cost: ¥11,600,000)
KeywordsZircon U-Pb Chronology / Laser Sampling / ICP Mass Spectrometry / Sensitive Ion Detection / 2 Dimensional Ion Detector / ジルコン / レーザー質量分析法 / レーザーサンプリング / 質量分析計 / レーザー / イオン検出器
Research Abstract

We have been developing a new analytical method for precise U-Pb age determinations using an inductively coupled plasma mass spectrometry coupled with newly developed laser microprobe technique. In order to determine the precise U-Pb age data from 10 microns spot of the zircon samples, laser ablation sampling technique using 266nm UV laser beam was developed. Resultant sample volume for the analysis was decreased down to 1/50 level compared with conventional laser sampling technique using IR fundamental Nd-YAG laser, and therefore enhancement of elemental sensitivity of the mass spectrometer was inevitable for the U-Pb age determinations. In this study this was achieved by different three techniques ; (a) modification of ion extraction lens, (b) improving the vacuum for first ion extraction stage by applying the high capacity rotary pump, and (c) sensitive ion detection using 2 dimensional solid ion detector called AMI (Amplified MOS Imager). The basic isotopic data obtained here demonstrate clearly that U-Pb chronology using Laser-ICPMS has a potential to become a significant and cost-effective tool for use in U-Pb zircon chronology.

Report

(3 results)
  • 1997 Annual Research Report   Final Research Report Summary
  • 1996 Annual Research Report
  • Research Products

    (22 results)

All Other

All Publications (22 results)

  • [Publications] Takafumi Hirata: "Lead Isotopic Analysis using Multiple Collector-Inductively Coupled Plasma Mass Spectrometry coupled with Modified External Correction Method for Mass Discrimination Effect" Analyst. 121. 1407-1411 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Barrat, J.A., Keller, F., Amosse J., Taylor, R.N., Nesbitt, R.W.and Hirata, T.: "Determination of rare earth elements in sixteen silicate reference samples by ICP-MS after Tm addition and ion-exchange separation" Geostandard Newsletter. 20. 133-139 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Yurimoto H., Matsumoto, K.Kim.K, Kitajima, H., Kosaka, K.and Hrata, H.: "Development of solid-state two-dimensional ion imaging device and new computer control system for SIMS. in Secondary Ion Mass Spectrometry SIMS X" Wiley. 987-990 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Ito, M., Yurimoto, H., Morioka, W.and Nagawsawa, H.: "REE diffusivities in melilite : A preliminary study by SIMS-depth profile method" Lunar Planet. Sci.28. 627-628 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Yurimoto, H.and Kuramoto, K.: "Si fractionation of chondrite Parent bodies by bipolar outflow." Lunar Planet. Sci.28. 1615-1616 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] T.Hirata and R.W.Nebitt: "Distribution of platinum group elements and rhenium between metallic phases of iron meteorites." Earth and Planetary Science Letters. Vol.,147. 11-24 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Takafumi Hirata: "Lead Isotopic Analysis using Multiple Collector-Inductively Coupled Plasma Mass Spectrometry coupled with Midified External Correction Method for Mass Discrimination Effect." Analyst. 121. 1407-1411 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Barrat, J.A., Keller, F., Amosse J., Taylor, R.N., Nesbitt, R.W.and Hirata, T.: "Determination of rare earth elements in sixteen silicate reference samples by ICP-MS after Tm addition and ion-exchange separation" Geostandards Newsletter. 20. 133-139 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Yurimoto, H., Matsumoto, K., Kim, K,Kitajima, H., Kosaka, K.and Hirata, H.: "Development of solid-state two-dimensional ion imaging device and new computer control system for SIMS.in Secondary Ion Mass Spectrometry SIMS X" Wiley. 987-990 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Ito, M., Yurimoto, H., Morioka, M.and Nagasawa, H.: "REE diffusivities in melilite : A preliminary study by SIMS-depth profile method" Lunar Planet.Sci.28. 627-628 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Yurimoto, H.and Kuramoto, K.: "Si fractionation of chondrite parent bodies by bipolar outflow." Lunar Planet.Sci.28. 1615-1616 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Hirata, T.and R.w.Nesbitt: "Distribution of platinum grou pelements and rhenium between metallic phases of iron meteorites." Earth and planetary Science Letters. 147. 11-24 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Yurimoto,H., Matsumoto,K., Kim,K, Kitajima,H., Kosaka,K. and Hrata,H.: "Development of solid-state two-dimensional ion imaging device and new computer control system SIMS. in Secondary Ion Mass Spectrometry SIMS X" Wiley. 987-990 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Ito,M., Yurimoto,H., Morioka,M. and Nagawsawa,H.: "REE diffusivities in melilite : A preliminary study by SIMS-depth profile method" Lunar Planet. Sci.28. 627-628 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Yurimoto,H. and Kuramoto,K.: "Si fractionation of chondrite parent bodies by bipolar outfow." Lunar Planet. Sci.28. 1615-1616 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] 圦本尚義: "同位体顕微鏡-全地球ダイナミクスを診る次世代分析装置-" 科学. 67. 560-566 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Kurosawa,M., Yrimoto,H. and Sueno,S.: "Patterns in the hydrogen and trace element compositions of mantle olivines." Phys. Chem. Min.24. 385-395 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] T. Hirata and R. W. Nebitt: "Distribution of platinum group elements and rhenium between metallic phases of iron meteorites." Earth and Planetary Science Letters. Vol.. 147. 11-24 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] 圦本尚義、松本一哉: "粒子線用二次元固体撮像素子" Bunseki Kagaku. 45. 493-500 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] Ohtani,E.,Yurimoto,H.: "Element Pertitioning between Metallic Liquid,Magnesiowustite,and Silicate Liquid at 20GPa and 2500C-A Secondary ion mass-Spectrometric Study" Geophy.Res.Lett. 23. 1993-1996 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] Yarimoto,H.and Kuramoto,K.: "Cosmochemical fractionation by bipolar outflow" Proc.29th ISAS Lunar Planet Symp.29. 148-149 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] Ohtani,E.,Suzuki,A.,Kato,T.,Yurimoto,H.: "Floatation of Diamond in magmas at high pressure and its implications for diamond genesis and fractionation in the deep mantle" Advanced Materials 96′,Proceedings of the 3rd NIRIM International symposium on Advances Materials. 345-350 (1996)

    • Related Report
      1996 Annual Research Report

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Published: 1996-04-01   Modified: 2016-04-21  

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