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Effect of interlaminar and intralaminar structure on fracture of high strength CFRP and optimization of mesoscopic structure

Research Project

Project/Area Number 08650106
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionKYOTO UNIVERSITY

Principal Investigator

HOJO Masaki  Kyoto University, Mesoscopic Materials Res.Ctr., Associate Professor, 工学部, 助教授 (70252492)

Co-Investigator(Kenkyū-buntansha) OCHIAI Shojiro  Kyoto University, Mesoscopic Materials Res.Ctr., Professor, 工学部, 教授 (30111925)
Project Period (FY) 1996 – 1997
Project Status Completed (Fiscal Year 1997)
Budget Amount *help
¥2,500,000 (Direct Cost: ¥2,500,000)
Fiscal Year 1997: ¥800,000 (Direct Cost: ¥800,000)
Fiscal Year 1996: ¥1,700,000 (Direct Cost: ¥1,700,000)
KeywordsComposite materials / Interlaminar fracture / Intralaminar fracture / Fatigue strength / Fracture toughness / Mesoscopic structure / Interface / Resin
Research Abstract

Effects of interlaminar and intralaminar mesoscopic structures on the fracture toughness and fatigue crack growth resistance were investigated for CFRP laminates. In the present study, resin layrs at the prepreg interfaces and fiber/matrix interfacial strength were controlled. Comparison of interlaminar and intralaminar fracture properties was carried out to find out the role of resin rich layrs at the prepreg interface. A new type of heterogeneous resin for resin rich layrs which is composed of thermoplastic fine particles and epoxy of base lamina was also investigated. Finally, the effect of thickness and toughness of the resin rich layrs at the prepreg interface was separately analyzed, and the optimization of the resin rich layrs was discussed. The results are summarized as follows :
1.Mode II interlaminar properties of CFRP laminates with heterogeneous resin at prepreg interface
Fracture toughness and fatigue crack growth resistance were improved up to the level of CFRP laminates wi … More th tough thermoplastic resin. This high toughness was kept with the increment of crack growth.
2.Mode I and II interlaminar properties of thermoplastic resin interleaved CFRP
Polyethylene base thermoplastic resin was put at the prepreg interface of CFRP laminates. The mode I fracture toughness was almost the same as that for CFRP laminates with thermoplastic resin matrix. This high toughness was kept with the increment of crack growth. For the case of mode II,the toughness was more than 10kJ/m^2, which was much higher than that for CFRP laminates with thermoplastic resin matrix.
3.Effect of fiber/matrix interfacial strength on interlaminar and intralaminar fracture properties
The fracture toughness for mode I intralaminar tests increased with increasing surface treatment levels. The effect of the surface treatment on the fracture toughness for mode II interlaminar tests was smaller than that for mode I intralaminar tests. The fracture toughness for mode I interlaminar tests was insensitive to the surface treatment level for CF/epoxy laminates. The mesoscopic fracture mechanism was well correlated to the effect of the surface treatment on the basis of SEM observation. Less

Report

(3 results)
  • 1997 Annual Research Report   Final Research Report Summary
  • 1996 Annual Research Report
  • Research Products

    (24 results)

All Other

All Publications (24 results)

  • [Publications] 北條 正樹: "一方向強化CF/PEEK積層板のモードII層間はく離疲労き裂伝ぱの破壊機構" 材料. 46. 366-373 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] 北條 正樹: "破壊力学とその特性評価" 材料. 46. 568-574 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Masaki Hojo: "Delamination Fatigue Crack Growth in CFRP Laminates under Mode I and II Loadings-Effect of Mesoscopic Structure on Fracture Mechanism-" Proceedings of International Conference on Fatigue of Composites. 15-26 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] 松田 聡: "層間高靱化CFRPのモードII層間はく離疲労のメゾ破壊機構" 日本機械学会論文集,A編. 63. 39-45 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] 日下 貴之: "層間高靱化CFRP材のモードI層間破壊じん性の負荷速度依存性" 日本機械学会論文集,A編. 63. 2359-2365 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] 松田 聡: "先進CFRPのモードII層間はく離疲労に及ぼす樹脂靱性の効果" 強化プラスチックス. 42. 49-53 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] 三木 光範: "複合材料,機械システム入門シリーズ8" 共立出版,

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Hojo, M., Matsuda, S., Higuchi, T., and Ochiai, S.: "Fracture Mechanism for Mode II Propagation of Delamination Fatigue Cracks in CF/PEEK Laminates" Journal of the Society of Materials Science, Japan. Vol.46. 366-373 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Hojo, M.and Kageyama, K.: "Fracture Mechanics and Its Properties" Journal of the Society of Materials Science, Japan. Vol.46. 568-574 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Hojo, M., Matsuda, S.and Ochiai, S.: "Delamination Fatigue Crack Growth in CFRP Laminates under Mode I and II Loadings-Effect of Mesoscopic Structure on Fracture Mechanism-" Proceedings of International Conference on Fatigue of Composites. 15-26 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Matsuda, S., Hojo, M., and Ochiai, S.: "Mesoscopic Fracture Mechanism of Mode II Delamination Fatigue Crack Propagation in Interlayr-Toughened CFRP" Transactions of the Japan Society of Mechanical Engineers, Series A,Vol.63, pp.39-45(1997)JSME International Journal, Series A. Vol.40, No.4. 423-429 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Kusaka, T., Hojo, M., Kurokawa, T.and Ochiai, S.: "Rate Dependence of Mode I Interlaminar Fracture Toughness of Interlayr-Toughened Garbon-Fiber/Epoxy Laminates" Transactions of the Japan Society of Mechanical Engineers, Series A. Vol.63. 2359-2365 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Matsuda, S., Hojo, M., Ochiai, S., and Higuchi, T.: "Effect of Matrix Resin Toughness on Mode II Delamination Fatigue for Advanced CFRP Laminates" Reinforced Plastics. Vol.42. 49-53 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] Miki, M., Fukuda, T., Motogi, S.and Hojo, M.: Composite materials. Kyoritsu Shuppan Co.Ltd., 236 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] 北條正樹: "一方向強化CF/PEEK積層板のモードII層間はく離疲労き裂伝ぱの破壊機構" 材料. 46巻・4号. 366-373 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] 北條正樹: "破壊力学とその特性評価" 材料. 46巻・5号. 568-574 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Masaki Hojo: "Delamination Fatigue Crack Growth in CFRP Laminates under Mode I and II Loadings -Effect of Mesoscopic Structure on Fracture Mechanism-" Proceedings of International Conference on Fatigue of Composites. 15-26 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Satoshi Matsuda: "Mesoscopic Fracture Mechanism of Mode II Delamination Fatigue Crack Propagation in Interlayer-Toughened CFRP" JSME International Journal, Series A. Vol.40,No4. 423-429 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] 日下貴之: "層間高靱化CFRP材のモードI層間破壊じん性の負荷速度依存性" 日本機械学会論文集,A編. 63巻・615号. 2359-2365 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] Takayuki Kusaka: "Rate Effects on Mode I Interlaminar Fracture Toughness in Carbon-Fiber / Epoxy and Carbon-Fiber / Toughened-Epoxy Composite Laminates" Proceedings of the Eleventh International Conference on Composite Materials, Vol.2. 234-243 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] 三木光範: "複合材料,機械システム入門シリーズ8" 共立出版, 236 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] 北條正樹: "一方向強化CF/PEEK積層板のモードII層間はく離疲労き裂伝ぱの破壊機構" 材料. 46巻4号. (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] 松田聡: "層間高靱化CFRPのモードII層間はく離疲労のメゾ破壊機構" 日本機械学会論文集,A編. 63巻603号. 39-45 (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] Masaki Hojo: "Effect of Fiber Surface Treatment and Resin Toughness on Interlaminar and Intralaminar Fracture Toughness of CFRP Laminates" Proceedings of Joint Canada-Japan Workshop on Composites. 30-33 (1996)

    • Related Report
      1996 Annual Research Report

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Published: 1996-04-01   Modified: 2016-04-21  

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