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Investigation of effect of stress on formation of omega-phase crystals in beta-Ti alloys using in-situ HREM method

Research Project

Project/Area Number 08650825
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionOkayama University of Science

Principal Investigator

SUKEDAI Eiichi  Okayama University of Science, Department of Mechanical Engineering, Professor, 工学部, 教授 (00090217)

Project Period (FY) 1996 – 1997
Project Status Completed (Fiscal Year 1997)
Budget Amount *help
¥1,700,000 (Direct Cost: ¥1,700,000)
Fiscal Year 1997: ¥900,000 (Direct Cost: ¥900,000)
Fiscal Year 1996: ¥800,000 (Direct Cost: ¥800,000)
Keywordsbeta-Ti allovs. / omega-phase transformation. / HREM. / In-situ observation. / aging under stress. / hvdrostatic pressure. / critical pressure. / initial structure of omega-phase crystals / ω相変態 / 静水圧負荷 / 高分解電子顕微鏡 / 原子半径差 / 格子歪
Research Abstract

In beta-Ti alloys, omega-phase transformations are occurred due to three ways, that is, quenching from temperature above beta-transus, aging and stressing. omega-phase crystals make beta-Ti alloys harder and more brittle. Recently, it was found that omega-phase crystals become nucleation sites of alpha-transformation by means of longer-time aging or higher temperature aging. beta-Ti alloys including fine alpha-phase particles, (beta+alpha) duplex Ti alloys are stronger and more ductile. The purpose of this research is to develop new methods to make higher density of omega-phase crystals in beta-Ti alloys as nucleation-siters of alpha-phase particles and to clarify the omega-phase transformation mechanism. A high resolution erectron microscope method was used to clarify the beta to omega transformation behaviors at atomic level. The results obtained are as follows :
(1). As-quenched omega-phase crystals were unstable, and almost of them disappeared during the heating.
(2). Aged omega-phase crystals grew from the remained as-quenched omega-phase crystals as nucleation sites.
(3). A tensile stress during the aging and hydrostatic pressurizing were effective to promote high density aged omega-phase crystals.
(4). It was recognized that the critical hydrostatic pressure to make omega-phase crystals was between 0.5 and 0.7 GPa.

Report

(3 results)
  • 1997 Annual Research Report   Final Research Report Summary
  • 1996 Annual Research Report
  • Research Products

    (22 results)

All Other

All Publications (22 results)

  • [Publications] H.Mizuta, E. Sukedai: "Investigation about aging behaviours of as-quenched ω-phase crystals in β-type Ti-Mo alloy using in-situ dark field and high resolution electron microscopy" Proc. Sixth Asia-Pacific Conf. on Electron Microscopy. 183-184 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] E. Sukedai, M. Shimoda: "High-resolution electron microscopy investigation about effect of stress on formation of ω-phase crystals in β-type Ti-Mo alloys" Proc. Microscopy and microanalysis 1996. 1006-1007 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] E. Sukedai, M. Shimoda: "Electron microscopy investigation about effect of some kinds of stresses on formation of ω-phase crystals in β-titanium alloys" Proc. EUREM '96. (in press). (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] E. Sukedai, Y. Kitano: "Investigation of initial structures of aged ω-phase crystals in β-type Ti-Mo alloys using high resolution electron microscopy" Micron.28. 269-277 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] E. Sukedai, H. Nishizawa: "Investigation of the effects of stresses on the formation of ω-phase crystals in β-type Ti-Mo alloys" Inst. Phys. Conf. Ser. 153,. 569-572 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] E. Sukedai, H. Nishizawa: "Investigation of the ω-phase transformation induced along {112}〈111〉 twin boundaries in β-Ti alloys using HREM and EELS" International Centennial Symposium on the Electron. 309-315 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] 第8回電顕サマー・スクール実行委員会、: "電子顕微鏡 基礎技術と応用1997〜ナノ世界への道〜" 佐藤武雄, 240 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] H.Mizuta, E.Sukedai and H.Hashimoto: "Investigation about aging behaviors of as-quenched omega-phase crystals in beta-type Ti-Mo alloy using in-situ dark field and high resolution electron microscopy" Proc.Sixth Asia-Pacific Conf.on Electron Microscopy. 183-184 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] E.Sukedai, M.Shimoda, A.Fujita, H.Nishizawa et al: "High-resolution electron microscopy investigation about effect of stress on formation of omega-phase crystals in beta-type Ti-Mo alloys" Proc.Microscopy and microanalysis 1996. 1006-1007 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] E.Sukedai, M.Shimoda, H.Nishizawa and H.Hashimoto: "Electron microscopy investigation about effect of some kinds of stresses on formation of omega-phase crystals in beta-Ti alloys" Proc.EUREM '96. (in press). (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] E.Sukedai, Y.Kitano and A.Ohnishi: "Investigation of initial structures of aged omega-phase crystals in beta-type Ti-Mo alloys using high resolution electron microscopy" Micron. Vol.28, No.4. 269-277 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] E.Sukedai, H.Nishizawa, J.Okuhara and H.Hashimoto: "Investigation of the effects of stresses on the formation of omega-phase crystals in beta-type Ti-Mo alloys" Inst.Phys.Conf.Ser.153. 569-572 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] E.Sukedai, H.Nishizawa, M.Shimoda and H.Hashimoto: "Investigation of the omega-phase transformation induced along {112}<111> twin boundaries in beta-Ti alloys using HREM and EELS" International Centennial Symposium on the electron. 309-315 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] E.Sukedai, Y.Kitano: "Investigation of initial structures of aged ω-phase crystals in β-type Ti-Mo alloys using high resolution electron microscopy" Micron,. 28・4. 269-277 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] E.Sukedai, H.Nishizawa: "Investigation of the effects of stresses on the formation of ω-phase crystals in β-type Ti-Mo alloys" Inst. Phys. Conf. Ser. 153,. 569-572 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] E.Sukedai, H.Nishizawa: "Investigation of the ω-phase transformation induced along {112} 〈111〉 twin boundaries in β-Ti alloys using HREM and EELS" International Centennial Symposium on the Eletron. 309-315 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] 第8回電顕サマー・スクール実行委員会、: "電子顕微鏡 基礎技術と応用1997〜ナノ世界への道〜" 佐藤武雄、,

    • Related Report
      1997 Annual Research Report
  • [Publications] T.Horiuchi,E.Sukedai,: "In-situ high resolution electron microscope observation of ω-phase precipitation in β-type titanium alloys" Material Transaction, JIM.36. 1455-1462 (1995)

    • Related Report
      1996 Annual Research Report
  • [Publications] E.Sukedai,M.Shimoda: "Investigation about the effects of stress on ω-phase transformation in β-titanium alloy using high resolution electron microscopy" 6th Asia-Pacific Conference on Electron Microscopy. 201-202 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] E.Sukedai,M.Shimoda: "Electron microscopy investigation about effect of some kinds of stresses on formation of ω-phase crystals in β-Ti alloys" XI European Congress on Microscopy. (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] E.Sukedai,M.Shimoda: "High resolution electron microscopy investigation about effect of stress on formation of ω-phase crystals on β-Ti alloys" Microscopy and Microanalysis 1996. 1006-1007 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] E.Sukedai,H.Nishizawa: "Investigation of the effects of stress on the formation of ω-phase crystals in β-titanium alloys" Proc.of Japan-China Workshop on Ti Alloys and Ti Intermetallics. 117-121 (1997)

    • Related Report
      1996 Annual Research Report

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Published: 1996-04-01   Modified: 2016-04-21  

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