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Preparation of composite ultrastrong permanent magnet composed of hard and soft magnetic materials by MA

Research Project

Project/Area Number 08650844
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Material processing/treatments
Research InstitutionOsaka University

Principal Investigator

MAJIMA Kazuhiko  Osaka University・Faculty of Engineering Associate Professor, 大学院・工学研究科, 助教授 (60029270)

Project Period (FY) 1996 – 1998
Project Status Completed (Fiscal Year 1998)
Budget Amount *help
¥2,400,000 (Direct Cost: ¥2,400,000)
Fiscal Year 1998: ¥400,000 (Direct Cost: ¥400,000)
Fiscal Year 1997: ¥400,000 (Direct Cost: ¥400,000)
Fiscal Year 1996: ¥1,600,000 (Direct Cost: ¥1,600,000)
Keywordsexchange-spring magnet / mechanical alloying / hard and soft composite magnet / nanocomposite magnet / single magnetic domain size / ultragiant magnetization / remanence / rare-earth magnet
Research Abstract

The purpose of this research is to develop the ultrastrong permanent magnet composed of hard and soft magnets by MA, and we succeeded in (Sm-Co)+Fe system. The results obtained are summarized as follows : The powder annealed at comparatively low temperature in vacuum after MA was composed of fine grains whose size was 10-30 nm in diameter and showed superior magnetic properties. When the annealing temperature was raised to 1073 K, most of Fe was consumed for the growth of 2-17 phase. This consumption of Fe and the growth of 2-17 phase resulted in the decrease of the remanence and coercivity. The powder without Fe showed low remanence and its maximum energy product was very low. On the other hand, remanence enhancement was found in the powder to which Fe was added, and the remanece increased with increasing Fe concentration. Though the shape of demagnetization curve varied with Fe concentration, the maximum product of about 100 kj/m^3 was obtained for both high and low Fe concentration samples. Such superior magnetic properties seemed to be the result of exchange interaction between hard and soft phase. The specimen obtained in this experiment was magnetically isotropic. And it is under investigation how to get the Sm_2Fe_<17>N_<2x> specimen with magnetic anisotropy.

Report

(4 results)
  • 1998 Annual Research Report   Final Research Report Summary
  • 1997 Annual Research Report
  • 1996 Annual Research Report
  • Research Products

    (24 results)

All Other

All Publications (24 results)

  • [Publications] K.Majima et al.: "Preparation of Anisotropic Sm-Fe-N Magnetic Powders Nitrided in(NH_3+H_2)Mived Gav and Their Magnetic Properties" Journal of the Japan Society of Powder and Powder Metallurgy. 43・5. 624-628 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] K.Majima et al.: "Preparation of(Sm-Co)+Fe Magnetic Powders by MA and Their Magnetic Propertics" Journal of the Japan Society of Powder and Powder Metallurgy. 43・5. 629-633 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Ito et al.: "Effect of Milling Atmosphere on the Preparation of Sm_2Fe_<17>Nx Powder by Mechanical Griding" Materials Trans.JIM. 37・11. 1704-1709 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Ito et al.: "Improvement of Magnetic Properties of Mechanically Ground Sm_2Fe_<17>Nx Powders by Vacuum Heat Treatment" Materials Trans.JIM. 38・2. 142-147 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] K.Majima et al.: "Structure and Magnetic Properties of Sm_2(Fe,Mn)_<17>Nx Coarse Powders with High Coercivity" J.Appl.Phys.81・8. 4530-4532 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] K.Majima et al.: "New Mechanical Grinding Process for Anisotropic Sm_2Fe_<17> Nx Powder with Nanocrystalline Structure" J.Appl.Phys.81・8. 4536-4538 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Ito, K.Majima, S.Katsuyam and H.Nagai: "Improvement of Magnetic Properties of Sm_2Fe_<17>N_x Powder Prepared by MG" Journal of the Japan Society of Powder and Powder Metallurgy. 43-5. 619-623 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] K.Majima, M.Ito, K.Matsukado, S.Katsuyam and H.Nagai: "Preparation of Anisotropic Sm-Fe-N Magnetic Powders Nitrided in (NH_3+H_2) Mixed Gas and Their Magnetic Properties" Journal of the Japan Society of Powder and Powder Metallurgy. 43-5. 624-628 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] K.Majima, M.Ito, T.Umemoto, S.Katsuyam and H.Nagai: "Preparation of (Sm-Ci) +Fe Magnetic Powder by MA and Their Magnetic Properties" Journal of the Japan Society of Powder and Powder Metallurgy. 43-5. 629-633 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Ito, K.Majima, S,Katsuyam and H.Nagai: "Magnetic Properties f Sm_2Fe_<17>N_x Powders Prepared by Mechanical Griding" Materials Trans.JIM. 37-2. 163-169 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Ito, K.Majima, S.Katsuyam and H.Nagai: "Effect of Milling Atmosphere on the Preparation of Sm_2Fe_<17>N_x Powder by Mechanical Grinding" Materials Trans.JIM. 37-11. 1704-1709 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Ito, K.Majima, S.Katsuyam and H.Nagai: "Improvement of Magnetic Properties of Mechanically Ground Sm_2Fe_<17>N_x Powders by Vacuum Heat Treatment" Materials Trans.JIM. 38-2. 142-147 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Ito, K.Majima, S.Katsuyam and H.Nagai: "Preparation of Sm_2Fe_<17>N_x Anisotropic Powder by Mechanical Grinding in NH_3 Atmosphere" J.Japan Inst.Metals. 61-3. 225-234 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] K.Majima, M.Ito, S.Katsuyam and H.Nagi: "Structure and Magnetic Properties of Sm_2(Fe, Mn)_<17>N_x Coarse Powders with High Coercivity" J.Appl.Phys.81-8. 4530-4532 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] K.Majima, M.Ito, S.Katsuyama and H.Nagai: "New Mechanical Grinding Process for Anisotropic Sm_2Fe_<17>N_x Powder with Nanocrystalline Structure" J.Appl.Phys.81-8. 4536-4538 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] K.Majima: "Structure and Magnetic Properties of Sm_2(Fe,Mn)_<17>N_x Coarse Powders with High Coercirity" J.Appl.Phys.81・8. 4530-4532 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] K.Majima: "New Mechanical Grinding Process for Anisotropic Sm_2Fe_<17>N_x Powder with a Nanecrystalline Structure" J.Appl.Phys.81・8. 4536-4538 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] 眞嶋一彦: "先端磁性材料" 生産と技術. 49・3. 13-18 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] 眞嶋一彦: "MA法により作製されたナノ結晶を有する希土類磁石粉末の磁気特性" 材料技術. 15・3. 74-77 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] 真島一彦: "MA法による(Sm-Co)+Fe磁石粉末の作製と磁気特性" 粉体粉末冶金. 43・5. 629-633 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] 真島一彦: "(NH_3+H_2)ガスによる異方性Sm_2Fe_<17>Nx粉末の作製および磁気特性" 粉体粉末冶金. 43・5. 624-628 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] M.Ito: "Magnetic Poperties of Sm_2Fe_<17>Nx Powders Prepared by Mechenical Grinding" Mater.Trans.JIM. 37・2. 163-169 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] 井藤幹夫: "メカニカルグライディング法によるSm_2Fe_<17>Nx粉末の作製に及ぼすミル雰囲気の影響" 日本金属学会誌. 60・4. 427-432 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] 井藤幹雄: "NH_3雰囲気中でのメカニカルグラィデング(MG)法によるSm_2Fe_<17>Nx粉末の作製と磁気特性" 日本金属学会誌. 60・8. 765-774 (1996)

    • Related Report
      1996 Annual Research Report

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Published: 1996-04-01   Modified: 2016-04-21  

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