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Micro-tribological study of metal surfaces using scanning probe microscope

Research Project

Project/Area Number 08650856
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Material processing/treatments
Research InstitutionHiroshima-Denki Institute of Technology

Principal Investigator

SUMOMOGI Tsunetaka  Hiroshima-Denki Institute of Technology, Faculty of Engineering, Associate Professor, 工学部, 助教授 (10136129)

Co-Investigator(Kenkyū-buntansha) ENDO Toshiro  Hiroshima-Denki Institute of Technology, Faculty of Engineering, Professor, 工学部, 教授 (60069200)
HIDAKA Yasuharu  Hiroshima-Denki Institute of Technology, Faculty of Engineering, Professor, 工学部, 教授 (20228737)
NAKATA Mikiko  Hiroshima-Denki Institute of Technology, Faculty of Engineering, Lecturer, 工学部, 講師 (60237302)
Project Period (FY) 1996 – 1997
Project Status Completed (Fiscal Year 1997)
Budget Amount *help
¥2,100,000 (Direct Cost: ¥2,100,000)
Fiscal Year 1997: ¥400,000 (Direct Cost: ¥400,000)
Fiscal Year 1996: ¥1,700,000 (Direct Cost: ¥1,700,000)
Keywordsscanning probe microscope / atomic force microscope / scanning tunneling microscope / micro-machining / micro-tribology / metal surface / マイクロトライボロジ / 金属材料
Research Abstract

Micro-tribological studies are made using a scanning probe microscope (SPM) which can measure the lateral force as well as the normal force images. The SPM is placed in an atmosphere control apparatus and the relative humidity around the tip-sample is controlled from 30% to 70%. Measurements are also performed in a high purity water bath. Samples investigated are the cleaved surfaces of mica, HOPG and MoS_2, and the polished metal surfaces of Ni, Cu and Al. In order to discuss the micro-tribological effects of adsorbed water molecules and the capillary condensation of water, the lateral force images are examined quantitatively as a function of the normal load on the sample surface. For surfaces of mica, HOPG and MoS_2, lateral force images with the lattice periodicity are obtained in the same manner as atomic scale topography images. The dependence of lateral force magnitude on the normal force is found to be affected by the atmosphere around the tip and the sample. At low relative humidity, 30%, the lateral force magnitude in atomic scale imaging is almost independent of the normal load. At high relative humidity, 70%, the lateral force magnitude exhibits dependence on the normal load. In water, the lateral force magnitude is approximately in proportion to the normal load. For surfaces of metal almost same behavior is obtained in the average value of lateral force. We conclude that the adhesive force due to the presence of water has severe influence upon the lateral force. From discussion on the viewpoints of Hertz analysis, Elasto-Hydrodynamic Lubrication and capillary condensation of water, the contact mechanism of the tip-sample is revealed.

Report

(3 results)
  • 1997 Annual Research Report   Final Research Report Summary
  • 1996 Annual Research Report
  • Research Products

    (22 results)

All Other

All Publications (22 results)

  • [Publications] T.Sumomogi et al: "Influence of atomosphere on tribological properties of scanning probe microscope observation" 4th Int'l Conf.on Nanometer-scale Sci.& Technol.September 8-12,1996,Beijing,China,. (Program No.18-Wep48). (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] 比枝 克徳 他: "ナノトライボロジーの研究を目的とした走査型プローブ顕微鏡システムの構成" 広島電機大学・広島自動車工業短期大学研究報告. 29. 41-48 (1996)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] T.Endo et al: "Preparation of Matallic Nanocluster on Graphite by Laser Ablation in STM/STS Apparatus at Low Temperatures" 9th Int'l Conf. on STM/STS,July 20-25,1997,Hamburg,Germany. (Program No Th12.2P05). (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] M.Yasuda. et al: "Correction of surface roughness in nano-scalemeasurements with scanning probe microscope" Mem.Hiroshima-Denki Inst.& Hiroshima Jun.Col.Auto.Engi.,. 30. 47-54 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] T.Sumomogi et al: "Nanoscale Evaluation of Roughness on Metal Films Prepared by Laser Ablation" Appl. Phys. A. 66(印刷中). (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] T.Sumomogi et al: "Influence of atomosphere on tribological properties in scanning probe microscope observation" Appl. Phys. A. 66(印刷中). (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] T.Sumomogi, K.Hieda, T.Endo and K.Kuwahara: "Influence of atmosphere on tribological properties of scanning probe microscope observation" 4th International Conference on Nanometer-Scale Science and Technology Beijin, China, September 8-12. Program No.18-WeP48. (1996)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] T.Endo, T.Sumomogi, M.Nakata, Y.Hidaka, H.Tsujikawa and S.Tateyama: "Preparation of metalic nanoclusters on graphite by laser ablation in STM/STS apparatus at low temperatures" 9th International Conference on Scanning Tunneling Microscopy/Specroscpy and Related Techniques Hamburg, Germany, July 20-25. Program No.Th12.2P05. (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] M.Yasuda, T.Saiki and T.Sumomogi: "Correction of surface roughness in nano-scale measurements with scanning probe microscope" Mem.Hiroshima-Denki Inst.& Hiroshima Jun.Col.Auto.Enji.30. 47 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] T.Sumomogi, K.Hieda, T.Endo and K.Kuwahara: "Influence of atmosphere humidity on tribological properties in scanning probe microscope observation" Appl.Phys.A. 66(in press). (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] T.Sumomogi, H.Sakai, M,Nakata and T.Endo: "Nanoscale evaluation of surface roughness of metal films prepared by laser ablation" Appl.Phys.A. 66(in press). (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1997 Final Research Report Summary
  • [Publications] T. Sumomogi et al: "Influence of atmosphere on tribological properties of scanning probe microscope observation" 4th Int′l Conf. on Nanometer-scale Sci. & Technol. September 8-12, 1996, Beijing, China,. (Program No. 18-Wep48). (1996)

    • Related Report
      1997 Annual Research Report
  • [Publications] 比枝克徳 他: "ナノトライボロジーの研究を目的とした走査プローブ顕微鏡システムの構成" 広島電機大学・広島自動車工業短期大学研究報告. 29. 41-48 (1996)

    • Related Report
      1997 Annual Research Report
  • [Publications] T. Endo et al: "Preparation of Matallic Nanocluster on Graphite by Laser Ablation in STM/STS Apparatus at Low Temperatures" 9th Int′l Conf. on STM/STS, July 20-25, 1997, Hamburg, Germany. (Program No Th12. 2P05. (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] M. Yasuda et al: "Correction of surface roughness in nano-scalemeasurements with scanning probe microscope" Mem. Hiroshima-Denki Inst. & Hiroshima Jun. Col. Auto. Engi.,. 30. 47-54 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] T. Sumomogi et al: "Nanoscale Evaluation of Roughness on Metal Films Prepared by Laser Ablation" Appl. Phys. A. 66(印刷中). (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] T. Sumomogi et al: "Influence of atomosphere on tribological properties in scanning probe microscope observation" Appl. Phys. A. 66(印刷中). (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] T.Sumomogi et al: "Influence of atmosphere on tribological properties of scanning probe microscope observation" 4th Int'l Conf.on Nanometer-scale Sci. & Technol. September 8-12,1996,Beijing,China,. Program No.18-Wep48 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] 比枝克徳他: "ナノトライボロジーの研究を目的とした走査プローブ顕微鏡システムの構成" 広島電機大学・広島自動車工業短期大学研究報告. 29. 41-48 (1996)

    • Related Report
      1996 Annual Research Report
  • [Publications] T.Sumomogi et al: "Nanoscale Evaluation of Roughness on Metal Films Prepared by Laser Ablation" 9th Int'l Conf.on STM/STS,July 20-25,1997,Hamburg,Germany. (発表予定). (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] T.Sumomogi et al: "Influence of atmosphere on tribological properties in scanning probe microscope observation" 9th Int'l Conf.on STM/STS,July 20-25,1997,Hamburg,Germany. (発表予定). (1997)

    • Related Report
      1996 Annual Research Report
  • [Publications] T.Endo et al: "Preparation of Matallic Nanocluster on Graphite by Laser Ablation in STM/STS Apparatus at Low Temperatures" 9th Int'l Conf.on STM/STS,July 20-25,1997,Hamburg,Germany. (発表予定). (1997)

    • Related Report
      1996 Annual Research Report

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Published: 1996-04-01   Modified: 2016-04-21  

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