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Fatigue Fracture Mechanism of Advanced Composite Materials (Micro-, Meso- and Macroscopic Approach)

Research Project

Project/Area Number 09305010
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionOsaka University

Principal Investigator

JONO Masahiro  Graduate School of Engineering, Osaka University, Professor, 大学院・工学研究科, 教授 (20029094)

Co-Investigator(Kenkyū-buntansha) UEMATSU Yoshihiko  Graduate School of Engineering, Osaka University, Research Associate, 大学院・工学研究科, 助手 (80273580)
SUGETA Atsushi  Graduate School of Engineering, Osaka University, Associate Professor, 大学院・工学研究科, 助教授 (60162913)
Project Period (FY) 1997 – 1999
Project Status Completed (Fiscal Year 1999)
Budget Amount *help
¥29,400,000 (Direct Cost: ¥29,400,000)
Fiscal Year 1999: ¥2,600,000 (Direct Cost: ¥2,600,000)
Fiscal Year 1998: ¥3,900,000 (Direct Cost: ¥3,900,000)
Fiscal Year 1997: ¥22,900,000 (Direct Cost: ¥22,900,000)
KeywordsFatigue Strength / Fatigue Crack Growth / Delamination Crack / FRP / MMC / 3% Silicon Iron / Microscopic Observation / Slip Deformation / き裂開閉口 / 微少き裂 / 層間はく離き裂進展 / FRP / き裂開閉口挙動
Research Abstract

Mixed mode delamination crack growth tests at elevated temperature (473K) were carried out using unidirectionally carbon fiber reinforced thermoplastics (CFRTP) under static creep condition. The crack propagation rate, da/dt, became higher in terms of mode I component of total energy release rate, GィイD2IィエD2, as mixed mode ratio, GィイD2IィエD2/GィイD2IIィエD2, decreased. This implied that crack propagation rate was accelerated by mode II component of total energy release rate, GィイD2IIィエD2. It was found that creep deformation area around the crack tip by mode II component was larger than that by mode I. Fractographic observation showed that matrices were elongated along the direction of main stress and fracture occurred at the interface between fiber and matrix.
Reversed plane bending tests were conducted on three kinds of SiC reinforced aluminum composites, namely whisker reinforced casting 6061 aluminum composite, and particle reinforced P/M and casting 2024 aluminum composites, with shallow … More surface-notched specimens. Initiation and growth behavior of small fatigue cracks were continuously monitored by a plastic replication technique and investigated in detail. Crack initiation mechanism on a whisker reinforced casting composite was found characterized by the interface cracking between matrix and SiC whiskers, where the lump of SiC whiskers was composed in a manufacturing process, and that on particle reinforced P/M composite was cycle slip deformation in matrix in the vicinity of SiC reinforcement particle. Fatigue strength of both materials was higher than that of unreinforced alloy due to the fact that SiC whiskers or tightly bounded matrix/particle interface restricted cyclic deformation of matrix, which resulted in the delay or fatigue crack initiation. While in a particle reinforced casting composite fatigue crack easily initiated at a casting defect at matrix/particle interface, and this premature crack initiation resulted in the lowest crack initiation strength.
Fatigue crack growth test under constant amplitude loading was conduced on a grain-oriented 3% silicon iron using servo-hydraulic fatigue loading system. The configuration of specimen surface around fatigue crack tip was transferred to a thin replica film and examined by means of an atomic force microscope (AFM). Discrete slip lines which emanated from crack edges were observed clearly along the two preferred slip directions (±55°). It implies that two preferential slips operated to almost identical extent simultaneously and fatigue crack grew in near mode I. The slip deformation during loading and unloading was observed successively and it was found that the operation of slips behind the fatigue crack tip resulted in crack closure and that at the crack tip brought about crack growth. The surface displacement during one cycle was measured quantitatively by using image processing technique. The pattern of the relationship between load and slip deformation was correlated well with that between load and crack tip opening displacement, CTOD, and the slipping distance near the crack tip corresponded to the ideal CTOD. Less

Report

(4 results)
  • 1999 Annual Research Report   Final Research Report Summary
  • 1998 Annual Research Report
  • 1997 Annual Research Report
  • Research Products

    (24 results)

All Other

All Publications (24 results)

  • [Publications] 城野政弘: "AFMによる疲労き裂先端近傍のすべり変形の微視的観察"日本材料学会第47期学術講演会. 73-74 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 城野政弘: "AFMによる3%ケイ素鋼板の疲労き裂進展挙動の微視的観察"日本材料学会第24回疲労シンポジウム. 207-210 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 城野政弘: "一方向強化AS4/PEEK積層板の高温混合モードき裂進展に及ぼすモード比の影響"日本材料学会第28回FRPシンポジウム. 175-178 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 城野政弘: "AFMによる疲労き裂先端の微視的観察と画像処理解析"日本機械学会 関西支部第75期定時総会. 1-15-1-16 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 城野政弘: "Mode I 疲労き裂先端近傍すべり変形のAFM観察と画像処理援用による定量解析"日本機械学会論文集A編.

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Masahiro Jono, Atsushi Sugeta and Yoshihiko Uematsu: "Microscopic Observation of Slip Deformation around Fatigue Crack Tip using AFM"JSMS 47ィイD1thィエD1 Annual Meeting. 73-74 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Masahiro Jono, Atsushi Sugeta and Yoshihiko Uematsu: "Microscopic Observation of Fatigue Crack Growth Behavior in 3% Silicon iron"JSMS 24ィイD1thィエD1 Symposium on Fatigue. 207-210 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Masahiro Jono, Atsushi Sugeta and Yoshihiko Uematsu: "Creep Delamination Crack Propagation in Unidirectionally Reinforced AS4/PEEK Laminate under Mixed Mode Condition at Elevated Temperature"JSMS 28ィイD1thィエD1 Symposium on FRP. 175-178 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Masahiro Jono: "Initiation and Growth Mechanism of Small Fatigue Cracks in SiC/Al Composites"Small Fatigue Cracks : Mechanical and Mechanisms. 289-300 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Masahiro Jono, Atsushi Sugeta and Yoshihiko Uematsu: "Microscopic Observation around Fatigue Crack Tip by AFM and Image Processing Analysis"JSME Kansai 75ィイD1thィエD1 Annual Meeting. 1〜15-1〜16 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Masahiro Jono, Atsushi Sugeta and Yoshihiko Uematsu: "AFM Observation of Slip Deformation near Mode I Fatigue Crack Tip and Quantitative Analysis Using Image Processing Technique"Transactions of the Japan Society of Mechanical Engineers. (Printing).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 城野 政弘: "疲労き裂先端近傍すべり発生挙動のAFM観察と画像処理による解析"日本材料学会 第48期学術講演会. 199-200 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 城野 政弘: "AFMによる疲労き裂先端のすべり変形観察と画像処理解析"日本機械学会 平成11年度材料力学部門講演会. 545-546 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 城野 政弘: "Initiation and Growth Mechanism of Small Fatigue Cracks in SiC/Al Composites"Small Fatique Cracks : Mechanical and Mechanisms. 289-300 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 城野 政弘: "AFMによる疲労き裂先端の微視的観察と画像処理解析"日本機械学会 関西支部第75期定時総会. (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] 城野政弘: "AFMによる疲労き裂先端近傍のすべり変形の微視的観察" 日本材料学会第47期学術講演会. 73-74 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 城野政弘: "AFMによる3%ケイ素鋼板の疲労き裂進展挙動の微視的観察" 日本材料学会第24回疲労シンポジウム. 250-253 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 城野政弘: "一方向強化AS4/PEEK積層板の高温混合モードき裂進展に及ぼすモード比の影響" 日本材料学会第28回FRPシンポジウム. (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] 城野政弘: "AFMによる疲労き裂先端近傍すべり変形の微視的連続観察と画像処理解析" 日本機械学会第74期関西支部講演会. (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] 城野政弘: "疲労き裂先端近傍すべり発生挙動のAFM観察と画像処理による解析" 日本材料学会第48期学術講演会. (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] 城野政弘: "疲労き裂先端近傍におけるすべり変形の微視的観察" 日本機械学会第73期関西支部講演会. (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] 城野政弘: "一方向CFRTPの高温モードII層間はく離き裂進展" 日本材料学会第27回FRPシンポジウム. (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] 城野政弘: "鉄系焼結材料における表面微小疲労き裂発生および初期進展挙動" 日本機械学会第73期関西支部講演会. (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] 城野政弘: "低炭素二相鋼の疲労き裂進展速度およびき裂開閉口挙動" 日本機械学会第73期関西支部講演会.

    • Related Report
      1997 Annual Research Report

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Published: 1997-04-01   Modified: 2016-04-21  

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