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Bulk nano-multilayerd materials produced by the repeated plastic deformat and its physical properties

Research Project

Project/Area Number 09305049
Research Category

Grant-in-Aid for Scientific Research (A).

Allocation TypeSingle-year Grants
Section一般
Research Field Material processing/treatments
Research InstitutionKYOTO UNIVERSITY

Principal Investigator

SHINGU P.hides  Graduate School of Energy Science Engineering, Kyoto University, Professor, エネルギー科学研究科, 教授 (20026024)

Co-Investigator(Kenkyū-buntansha) OTSUKI Akira  Institute of Advanced Energy, Kyoto University Asistant Professor, エネルギー理工学研究所, 助教授 (10026148)
ISHIHARA Keiichi n.  Graduate School of Energy Science Engineering, Kyoto University, Asistant Professor, エネルギー科学研究科, 助教授 (30184550)
Project Period (FY) 1997 – 2000
Project Status Completed (Fiscal Year 2000)
Budget Amount *help
¥37,700,000 (Direct Cost: ¥37,700,000)
Fiscal Year 2000: ¥2,300,000 (Direct Cost: ¥2,300,000)
Fiscal Year 1999: ¥3,800,000 (Direct Cost: ¥3,800,000)
Fiscal Year 1998: ¥6,500,000 (Direct Cost: ¥6,500,000)
Fiscal Year 1997: ¥25,100,000 (Direct Cost: ¥25,100,000)
Keywordsnanocrystal / nano structure / mechanical alloying / layer stracture / interface reaction / fine grained structure
Research Abstract

Nano scale multi-layerd materials of Ag and Fe have been manufactured. This material contains alternate layers of Ag and Fe more than several hundred thousand in number. As one of the characteristic properties of such nanolayerdmaterials ofmagnetic and non-magnetic metals, the giant magnetoresistivity (GMR) has been measured. The GMR for electrical current parallel to the layers is about 8% and for the current perpendicular to the layers is about 45%. The experimental confirmation of such large GMR for the case of current perpendicular to the layers has not been, as far as the authors' knowledge, reported previously. Similar multi-layerd materials for the Cu and Fe system has also been manufactured and GMR has also been confirmed. The mechanical strength in tension experiment have been carried out for these materials. The ultimate tensile strength as high as 1.5 GPa have been obtained when the layer thickness is less than about 50 nano meters. The average layer thickness for these materials for which the GMR effect have been observed were in the range of 10 to 50 nano-meters. This thickness range is nearly one order of magnitude greater than that for the samples prepared by the gas deposition method. For the purpose of investigation into the reason for such difference in the thickness of layers necessary for the activation of GMR effect, the sputtering method was used to produce nano-layerd materials of Ag and Fe with irregularities in the layer thickness which simulates the present rolling and folding technique. The average layer thickness in this case have been revealed to be greater than for the samples of regularly deposited nano-layerd materials.
From such experimental results, in the scope of the present experiment, the irregularity in the layer thickness is responsible for the occurrence of GMR for relatively large average layer thickness materials.

Report

(5 results)
  • 2000 Annual Research Report   Final Research Report Summary
  • 1999 Annual Research Report
  • 1998 Annual Research Report
  • 1997 Annual Research Report
  • Research Products

    (17 results)

All Other

All Publications (17 results)

  • [Publications] 新宮秀夫: "鉄製粉末冶金材料におけるアクティブディスアセンブリー志向のリサイクル技術の開発"粉体および粉末冶金. 47・4. 364-368 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] P.H.Shingu: "Formation of nanoscale Fe/Ag multilayer by repeated Press-rolling and its layer thickness dependence of magnetores, stance"Materials Science and Engineering. A285. 412-417 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 新宮秀夫: "SHS-Pseudo-HIP法によるTi-Al-C系複合材料の作製とその評価"粉体および粉末冶金. 47・8. 921-926 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 新宮秀夫: "メカニカルアロイング状態図の制約なしに合金を作る技術."金属. 71・1. 43-46 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] P.H.Shingu: "Bulk Metallic Multilayers Produced by Repeated Press-rolling and Their Perpendicular Magnetoresistance"J.Appl. Phys. Vol. 82, No. 5. 2435-243 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] P.H.Shingu: "Bulk Nano-scale Multilayers Prepared by Repeated Pressing-rolling"Acta Metallurgica. Vol. 34, No. 5. 455-458 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] P.H.Shingu: "Nano-scaled Multilayered Bulk Materials by Repeated Pressing and Rolling in the Ag-Fe and Cu-Fe Systems"Materials Science Forum. Vols. 312-314. 293-298 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] P.H.Shingu: "Nano-scale Metal Mulutilayers Produced by Repeated Press-rolling"Radiation Effects & Defects in Solids. Vol. 148. 555-562 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] P.H.Shingu: "Formaition of Nanoscale Fe/Ag Multilayer by Repeated Press-rolling and its Layer Thicness Dependence of Magnetoresistance"Materials Science and Engineering. Vol. A285. 412-417 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 新宮秀夫: "鉄製粉末冶金材料におけるアクティブディスアセンブリー志向のリサイクル技術の開発"粉体および粉末冶金. 47・4. 364-368 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] P.H.Shingu: "Formaition of nanoscale Fe/Ag multilayer by repeated Press-rolling and its layer thickness dependence of magneto-resistance"Materials Science and Engineering. A285. 412-417 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 新宮秀夫: "SHS-Pseudo-HIP法によるTi-Al-C系複合材料の作製とその評価"粉末および粉末冶金. 47・8. 921-926 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 新宮秀夫: "メカニカルアロイング状態図の制約なしに合金を作る技術"金属. 71・1. 43-46 (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] P.H.Shingu: "Nano-Scaled Multilayered Bulk Materials Manufactured by Repeated Pressing and Rolling in the Ag-Fe and Cu-Fe Systems"Materials Science Forum. 312-314. 293-298 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] P.H.Shingu: "Nano-Scale Metal Multilayers Produced by Repeated Press-Rolling"Radiation Effects & Defects in Solids. 148. 555-562 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] P.H.Shingu: "BULK NANO-SCALE MULTILAYERS PREPAREO BY REPEATED PRESSING-ROLLING" ACTA METALLURGICA SINICA. 34・5. 455-458 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] P.H.Shingu: "Bulk metallic multilayers produced by repeated press-rolling and their perpendicular magnetoresistance" J.Appl.Phys.82・5. 2435-2438 (1997)

    • Related Report
      1997 Annual Research Report

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Published: 1997-04-01   Modified: 2016-04-21  

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