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A study on the micro-fracture-process and the role of microstructure in the hydrogen induced fracture

Research Project

Project/Area Number 09450052
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionKEIO UNIVERSITY

Principal Investigator

YAMADA Kunihiro  Keio University, Department of Mechanical Engineering, Professor, 理工学部, 教授 (40051742)

Co-Investigator(Kenkyū-buntansha) SUZUKI Tetsuya  Keio University, Department of Mechanical Engineering, Associate Professor, 理工学部, 助教授 (10286635)
YAMADA Kunihiro  Keio University, Department of Mechanical Engineering, Professor (40051742)
Project Period (FY) 1997 – 1998
Project Status Completed (Fiscal Year 1998)
Budget Amount *help
¥10,500,000 (Direct Cost: ¥10,500,000)
Fiscal Year 1998: ¥2,500,000 (Direct Cost: ¥2,500,000)
Fiscal Year 1997: ¥8,000,000 (Direct Cost: ¥8,000,000)
KeywordsHydrogen Embrittlement / Delayed Fracture / Crack Propagation / Quasi-Cleavge Crack / Intergranular Crack / Microstructure / 脆性破壊 / 4340鋼 / 破壊条件 / 安定き裂成長
Research Abstract

Since most of studies in delayed fracture have dealt with the propagation behavior of macroscopic cracks, no particular attempts to elucidate the behavior of crack initiation and early stage of crack propagation, which is the essential process of hydrogen related fracture, have been made. In this study, to solve the short crack problems of hydrogen induced "brittle fracture" which have been still unsettled, the initiation and propagation behavior of microscopic cracks which start at a weakest site in the microstructure was investigated with a special emphasis on an interaction between mechanical and metallurgical aspects of delayed fracture process.
The experimental analyses have revealed crucial facts which have been remained unknown. The authors had shown in the previous studies that the initial stage of the delayed fracture was not intergranular (IG) but the quasi-cleavage (OC) crack starting from non-metallic inclusions in the subsurface, and that the QC crack triggered IG cracks after a substantial subcritical growth. In this study, it has been revealed that the critical condition for the development of IG cracks is dependent on an increase in the stress intensity at the crack tip (mechanical factor) and the metallurgical changes due to tempering treatment as well as the hydrogen condensation at the crack tip. Consequently, the critical aspects of delayed fracture is related to the material resistance to the transgranular QC crack which should trigger the onset of growth of IG crack, together with the contribution of hydrogen.

Report

(3 results)
  • 1998 Annual Research Report   Final Research Report Summary
  • 1997 Annual Research Report
  • Research Products

    (38 results)

All Other

All Publications (38 results)

  • [Publications] 中谷・山田: "水素脆化した高強度鋼の粒界き裂形成を支配する要因について" 日本機械学会論文集A編. 63-611. 1392-1397 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 中谷・靱・山田: "薄肉形状を持つ高強度鋼材の遅れ破壊挙動について" 日本機械学会論文集A編. 64-626. 2561-2566 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Nakatani, T.Higashi and K.Yamada: "Effect of Tempering Treatment on Hydrogen Induced Cracking in High Strength Steel" Fatigue and Fracture of Engineering Materials and Structure. (印刷中).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] A.Kimura, Y.Nakatani, K.Yamada and T.Suzuki: "Hydrogen Detection in CVD Diamond Films by Elastic Recoil Detection Analysis" Diamond and Related Materials. (印刷中).

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 尾崎・中谷・山田: "平滑材遅れ破壊過程における擬へき開割れき裂挙動のAE解析" 日本機械学会第75期通常総会講演会講演論文集(II). 98-1. 393-394 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 細貝・中谷・山田: "粗粒化した高強度鋼を用いた水素誘起型き裂生成進展過程の解析" 日本機械学会第75期通常総会講演会講演論文集(II). 98-1. 395-396 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 中谷・山田: "水素雰囲気下にある鋼の脆性破壊挙動" 第28回安全工学シンポジウム講演予稿集. 303-304 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Nakatani, H.Matsuoka and K.Yamada: "Formation and Characteristics of Quasi-cleavage Crack in Hydrogen Damaged Low Strength Steel" Fracture from Defects(ESIS)Ed.M.W.Brown, E.R.de los Rios and K.J.Miller. Vol.III. 1121-1126 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 大井・中谷・山田: "水素脆性破壊における初期き裂の生成・進展メカニズムの実験解析" 日本機械学会第76期全国大会講演論文集Vol.1. 98-3. 151-152 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 松岡・中谷・山田: "遅れ破壊感受性に及ぼす降伏強度レベルの影響" 日本機械学会第76期全国大会講演論文集Vol.1. 98-3. 153-154 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 小柳・中谷・鈴木・山田: "遅れ破壊における擬へき開割れ挙動のTEM解析" 日本機械学会第76期全国大会講演論文集Vol.1. 98-3. 155-156 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 木村・渡辺・中谷・鈴木: "ERDAによるダイヤモンド膜中の水素濃度測定" ニューダイヤモンドフォーラム第11回ダイヤモンドシンポジウム講演要旨集. 94-95 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] "Y.Nakatani and K.Yamada: "Intergranular Cracking in Hydrogen-Charged High Strength Steel"" Transactions of the Japan Society of Mechanical Engineers, (JSME). 63-611, A. 1392-1397 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Nakatani, K.Utsubo and K.Yamada: ""Delayed Fracture of High Strength Steel having Thin Thickness"" Transactions of the Japan Society of Mechanical Engineers, (JSME). 64-626, A. 2561-2566 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Nakatani, T.Higashi and K.Yamada: ""Effect of Tempering Treatment on Hydrogen Induced Cracking in High Strength Steel"" Fatigue and Fracture of Engineering Materials and Structure. (in press.).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] A.Kimura, Y.Nakatani, K.Yamada and T.Suzuki: ""Hydrogen Detection in CVD Diamond Films by Elastic Recoil Detection Analysis"" Diamond and Related Materials. (in press.).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] K.Ozaki, Y.Nakatani and K.Yamada: ""AE Analysis of Quasi-Cleavage Crachikgin Delayed Fracture of High Strength Steel"" Proceeding of The 75th JSME Spring Annual Meeting. Vol.II,98-1. 393-394 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] T.Hosokai, Y.Nakatani and K.Yamada: ""The crack Formation in Delayed Fracture of Coarse Grained High Strength Steel"" Proceeding of The 75th JSME Spring Annual Meeting. Vol.II,98-1. 395-396 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] Y.Nakatani, H.Matsuoka and K.Yamada: ""Formation and Characteristics of Quasi-cleavage Crack in Hydrogen Damaged Low Strength Steel"" in "Fracture from Defects", Vol.III,Ed.M.W.Brown, E.R.de los Rios and K.J.Miller, pp.1121-1126, Sheffield (1998), The European Structural Integrity Society.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Ohi, Y.Nakatani and K.Yamada: ""Experimental Analysis of Crack Formation Mechanism in Early-Stage under Hydrogen Environment"" Proceeding of The 76th JSME Fall Annual Meeting. Vol.I,98-3. 151-152 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] H.Matsuoka, Y.Nakatani and K.Yamada: ""Effect of Yield Strength Level in Delayed Fracture Sensitivity"" Proceeding of The 76th JSME Fall Annual Meeting. Vol.I,98-3. 153-154 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] M.Oyanagi, Y.Nakatani and K.Yamada: ""TEM Observation of Quasi-cleavage Crack Morphology in Delayed Fracture"" Proceeding of The 76th JSME Fall Annual Meeting. Vol.I,98-3. 155-156 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1998 Final Research Report Summary
  • [Publications] 中谷・山田: "水素脆化した高強度鋼の粒界き裂形成を支配する要因について" 日本機械学会論文集A編. 63-611. 1392-1397 (1997)

    • Related Report
      1998 Annual Research Report
  • [Publications] 中谷・靱・山田: "薄肉形状を持つ高強度鋼材の遅れ破壊挙動について" 日本機械学会論文集A編. 64-626. 2561-2566 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] Y.Nakatani,T.Higashi and K.Yamada: "Effect of Tempering Treatment on Hydrogen Induced Cracking in High Strength Steel" Fatigue and Fracture of Engineering Materials and Structure. 印刷中.

    • Related Report
      1998 Annual Research Report
  • [Publications] A.Kimura,Y.Nakatani.K.Yamada and T.Suzuki: "Hydrogen Detection in CVD Diamond Films by Elastic Recoil Detection Analysis" Diamond and Related Materials. 印刷中.

    • Related Report
      1998 Annual Research Report
  • [Publications] 尾崎・中谷・山田: "平滑材遅れ破壊過程における擬へき開割れき裂挙動のAE解析" 日本機械学会第75期通常総会講演会講演論文集(II). 98-1. 393-394 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 細貝・中谷・山田: "粗粒化した高強度鋼を用いた水素誘起型き裂生成進展過程の解析" 日本機械学会第75期通常総会講演会講演論文集(II). 98-1. 395-396 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 中谷・山田: "水素雰囲気下にある鋼の脆性破壊挙動" 第28回安全工学シンポジウム講演予稿集. 303-304 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] Y.Nakatani,H.Matsuoka and K.Yamada: "Formation and Characteristics of Quasi-cleavage Crack in Hydrogen Damaged Low Strength Steel" Fracture from Defects(ESIS) Ed.M.W.Brown, E.R.de los Rios and K.J.Miller. Vol.III. 1121-1126 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 大井・中谷・山田: "水素脆性破壊における初期き裂の生成・進展メカニズムの実験解析" 日本機械学会第76期全国大会講演論文集Vol.1. 98-3. 151-152 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 松岡・中谷・山田: "遅れ破壊感受性に及ぼす降伏強度レベルの影響" 日本機械学会第76期全国大会講演論文集Vol.1. 98-3. 153-154 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 小柳・中谷・鈴木・山田: "遅れ破壊における擬へき開割れ挙動のTEM解析" 日本機械学会第76期全国大会講演論文集Vol.1. 98-3. 155-156 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] 木村・渡辺・中谷・鈴木: "ERDAによるダイヤモンド膜中の水素濃度測定" ニューダイヤモンドフォーラム第11回ダイヤモンドシンポジウム講演要旨集. 94-95 (1997)

    • Related Report
      1998 Annual Research Report
  • [Publications] 細貝・中谷・山田: "粗粒化した高強度鋼を用いた水素誘起型き裂生成・進展過程の解析" 日本機械学会第75期通常総会講演会講演論文集. (未定). (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] 尾崎・中谷・山田: "平滑材遅れ破壊過程における擬へき開割れき裂挙動のAE解析" 日本機械学会第75期通常総会講演会講演論文集. (未定). (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] 中谷・山田: "水素雰囲気下にある鋼の脆性的破壊挙動" 第28回安全工学シンポジウム講演論文集. (未定). (1998)

    • Related Report
      1997 Annual Research Report
  • [Publications] Nakatani,Matsuoka,Yamada: "FORMATION AND CHARACTERISTICS OF QUASI-CLEAVAGE CRACK IN HYDROGEN DAMAGED LOW STRENGTH STEEL" PROC.OF THE 12th EUROPEAN CONF.ON FRACTURE. (未定). (1998)

    • Related Report
      1997 Annual Research Report

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Published: 1997-04-01   Modified: 2016-04-21  

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