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Ultrasonic Microspectroscopy for High-Precision Surface Characterization of Substrates for Electronics Devices

Research Project

Project/Area Number 09450120
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Electronic materials/Electric materials
Research InstitutionTOHOKU UNIVERSITY

Principal Investigator

KUSHIBIKI Jun-ichi  Graduate School of Engineering, Tohoku University, Professor, 大学院・工学研究科, 教授 (50108578)

Co-Investigator(Kenkyū-buntansha) MATSUMOTO Yasushi  Graduate School of Engineering, Tohoku University, Associate Professor, 大学院・工学研究科, 助教授 (20312598)
SUEMITSU Maki  Research Institute of Electrical Communications, Tohoku University, Associate Professor, 電気通信研究所, 助教授 (00134057)
NIWANO Michio  Research Institute of Electrical Communications, Tohoku University, Professor, 電気通信研究所, 教授 (20134075)
ONO Yuu  Graduate School of Engineering, Tohoku University, Research Associate, 大学院・工学研究科, 助手 (70271880)
Project Period (FY) 1997 – 1999
Project Status Completed (Fiscal Year 1999)
Budget Amount *help
¥14,000,000 (Direct Cost: ¥14,000,000)
Fiscal Year 1999: ¥3,000,000 (Direct Cost: ¥3,000,000)
Fiscal Year 1998: ¥3,000,000 (Direct Cost: ¥3,000,000)
Fiscal Year 1997: ¥8,000,000 (Direct Cost: ¥8,000,000)
KeywordsUltrasonic microspectroscopy / Line-focus-beam acoustic microscopy / V(z) curve analysis / Leaky surface acoustic wave velocity / Electronics materials / Device fabrication process / Layered structures / Acoustic inhomogeneity / 漏洩弾性表面波 / 半導体材料評価
Research Abstract

Ultrasonic microspectroscopy technology, using the line-focus-beam (LFB) and plane-wave ultrasonic material characterization system, has been applied to resolve material problems concerned with single crystal substrate (LiNbOィイD23ィエD2, LiTaOィイD23ィエD2, Si, GaAs) for electronic devices and with proton-exchanged, implanted layers, epitaxial or amorphous films on the substrates used in the device fabrication processes.
1. The reliable LFB system with high accuracy in leaky surface-acoustic-wave (LSAW) velocity measured on the water-loaded specimen surface has been established for accurate and efficient characterization of material properties, by developing a temperature-controlled pure water supply system and a sample transfer system. For the system calibration, the standard specimens of GGG, Si, Ge, LiNbOィイD23ィエD2, and LiTaOィイD23ィエD2 has been developed.
2. A method of super-precision measurements of lattice parameters by the X-ray diffractometer using the Bond method has been developed, resulting in a very high accuracy of Δd/d<10ィイD1-6ィエD1 for a wide Bragg angle range.
3. To eliminate a serious problem of the back reflection effect, occurring for thin specimens such as wafer substrates, a moving average method to obtain a true velocity from apparent LSAW velocities measured as a function of frequency and an approximated correction method useful for a number of measurement points have been developed.
4. A method of evaluating single crystals such as LiNbOィイD23ィエD2, LiTaOィイD23ィエD2, and GaAs by the LFB system has been established.
5. A method of evaluating and selecting LiNbOィイD23ィエD2 and LiTaOィイD23ィエD2 substrates for SAW devices by the LFB system has been established.
6. A method of analyzing and evaluating proton-exchanged layers on Z-cut LiTaOィイD23ィエD2 crystal substrates and ion-implanted layers on Si crystal substrates has been developed and demonstrated.

Report

(4 results)
  • 1999 Annual Research Report   Final Research Report Summary
  • 1998 Annual Research Report
  • 1997 Annual Research Report
  • Research Products

    (44 results)

All Other

All Publications (44 results)

  • [Publications] J.Kushibiki and M.Miyashita: "Characterization of Domain-Inverted Layers in LiTaO_3 by Line-Focus-Beam Acoustic Microscopy"Jpn.J.Appl.Phys.. 36・7B. L959-L961 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J.Kushibiki and M.Arakawa: "A Method for Calibrating the Line-Focus-Beam Acoustic Microscopy System"IEEE Trans.UFFC. 45・2. 421-430 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J.Kushibiki,Y.Ohashi and M.Arakawa: "Precise Velocity Measurement for Thin Specimens by Line--Focus-Beam Acoustic Microscopy"Jpn.J.Appl.Phys.. 38・1A/B. L89-L91 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J.Kushibiki and Y.Ohashi: "Theoretical and Experimental Considerations on Line-Focus-Beam Acoustic Microscopy for Thin Specimens"Jpn.J.Appl.Phys.. 38・3B. L342-L344 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] I.Takanaga,J.Hirohashi and J.Kushibiki: "Homogeneity Evaluation of LiNbO_3 and LiTaO_3 Single Crystals for Determining Acoustical Physical Constants"Jpn.J.Appl.Phys.. 38・5B. 3201-3203 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J.Kushibiki,T.Kobayashi,H.Ishiji and C.K.Jen: "Surface-Acoustic-Wave Properties of MgO-doped LiNbO_3 Single Crystals Measured by Line-Focus-Beam Acoustic Microscopy"J.Appl.Phys.. 85・11. 7863-7868 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J.Kushibiki and T.Okuzawa: "Line-Focus-Beam Acoustic Microscopy Detection of Variations of Growing Conditions of LiTaO_3 Crystals"Jpn.J.Appl.Phys.. 38・8B. L964-L966 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Ohashi and J.Kushibiki: "Correction of Velocity Profiles on Thin Specimens Measured by Line-Focus-Beam Acoustic Microscopy"Jpn.J.Appl.Phys.. 38・10B. L1197-L1200 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] I.Takanaga and J.Kushibiki: "Elastic Constants of Multidomain LiTaO_3 Crystal"J.Appl.Phys. 86・6. 3342-3346 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J.Kushibiki,I.Takanaga,M.Arakawa and T.Sannomiya: "Accurate Measurements of the Acoustical Physical Constants of LiNbO_3 and LiTaO_3 Single Crystals"IEEE Trans.UFFC. 46・5. 1315-1323 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 櫛引淳一、小野雄、高長和泉: "SAWデバイス用LiNbO_3,LiTaO_3単結晶の超音波マイクロスペクトロスコピー(招待論文)"電子情報通信学会誌. J82-C-I・12. 715-727 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J.Kushibiki,Y.Ohashi and M.Arakawa: "Influence of Reflected Waves from the Back Surface of Thin Solid-Plate Specimen on Velocity Measurements by Line-Focus-Beam Acoustic Microscopy"IEEE Trans.UFFC. 47・1. 274-284 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J.Kushibiki,T.C.Wei,Y.Ohashi and A.Tada: "Ultrasonic Micro-Spectroscopy Characterization of Silica Glass"J.Appl.Phys.. 87・6. 3113-3121 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Ono and J.Kushibiki: "Experimental Study of Construction Mechanism of V(z)Curves Obtained by Line-Focus-Beam Acoustic Microscopy"IEEE Trans.UFFC. (in press) (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J.Kushibiki,Y.Ohashi and Y.Ono: "Evaluation of LiNbO_3 and LiTaO_3 Substrates for SAW Devices by the LFB Ultrasonic Material Characterization System"IEEE Trans.UFFC. (in press) (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J. Kushibiki and M. Miyashita: "Characterization of Domain-Inverted Layers in LiTaOィイD23ィエD2 by Line-Focus-Beam Acoustic Microscopy"Jpn. J. Appl. Phys.. Vol. 36, No. 7B. L959-L961 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J. Kushibiki and M. Miyashita: "A Method for Calibrating the Line-Focus-Beam Acoustic Microscopy System"IEEE Trans. UFFC. Vol. 45, No. 2. 421-430 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J. Kushibiki, Y. Ohashi, and M. Arakawa: "Precise Velocity Measurement for Thin Specimens by Line-Focus-Beam Acoustic Microscopy"Jpn. J. Appl. Phys.. Vol. 38, No. 1A/B. L89-L91 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J. Kushibiki and Y. Ohashi: "Theoretical and Experimental Considerations on Line-Focus-Beam Acoustic Microscopy for Thin Specimens"Jpn. J. Appl. Phys.. Vol. 38, No. 3B. L342-L344 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] I. Takanaga, J. Hirohashi, and J. Kuxhibiki: "Homogeneity Evaluation of LiNbOィイD23ィエD2 and LiTaOィイD23ィエD2 Single Crystals for Determining Acoustical Physical Constants"Jpn. J. Appl. Phys.. Vol. 38, No. 5B. 3201-3203 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J. Kushibiki, T. Kobayashi, H. Ishiji, and C.-K. Jen: "Surface-acoustic-wave properties of MgO-doped LiNbOィイD23ィエD2 single crystals measured byline-focus-beam acoustic microscopy"J. Appl. Phys.. Vol. 85, No. 11. 7863-7868 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J. Kushibiki, and T. Okuzawa: "Line-Focus-Beam Acoustic Microscopy Detection of Variations of Growing Conditions of LiTaOィイD23ィエD2 crystals"Jpn. J. Appl. Phys.. Vol. 38, No. 8B. L964-L966 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y. Ohashi and J. Kushibiki: "Correction of Velocity Profiles on Thin Specimens Measured by Line-Focus-Beam acoustic Microscopy"Jpn. J. Appl. Phys.. Vol. 38, No. 10B. L1197-L1200 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] I. Takanaga, and J. Kushibiki: "Elastic constants of multidomain LiTaOィイD23ィエD2 crystal"J. Appl. Phys.. Vol. 86, No. 6. 3342-3346 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J. Kushibiki, I. Takanaga, M. Arakawa, and T. Sannomiya: "Accurate measurements of the acoustical physical constants of LiNbOィイD23ィエD2 and LiTaOィイD23ィエD2 single crystals"IEEE Trans. UFFC.. Vol. 46, No. 5. 1315-1323 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J. Kushibiki, Y. Ono, and I. Takanaga: "Ultrasonic micro-spectroscopy of LiNbOィイD23ィエD2 and LiTaOィイD23ィエD2 single crystals for SAW devices (Invited)"IEICE Trans. on Electron.. Vol. J82-C-I, No. 12. 715-727 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J. Kushibiki, Y. Ohashi, and M. Arakawa: "Influence of reflected waves from the back surface of thin solid-plate-specimen on velocity measurements by line-focus-beam acoustic microscopy"IEEE Trans. UFFC. Vol. 47, No. 1. 274-284 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J. Kushibiki, T. C. Wei, Y. Ohashi, and A. Tada: "Ultrasonic micro-spectroscopy characterization of silica glass"J. Appl. Phys.. Vol. 87, No. 6. 3113-3121 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y. Ono and J. Kushibiki: "Experimental study of construction mechanism of V(z) curves obtained y line-focus-beam acoustic microscopy"IEEE Trans. UFFC.. (in press). (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J. Kushibiki, Y. Ohashi, and Y. Ono: "Evaluation of LiNbOィイD23ィエD2 and LiTaOィイD23ィエD2 substrates for SAW devices by the LFB ultrasonic material characterization system"IEEE Trans. UFFC.. (in press). (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] Y.Ohashi and J.Kushibiki: "Correction of Velocity Profiles on Thin Specimens Measured by Line-Focus-Beam Acoustic Microscopy"Jpn. J. Appl. Phys.. 38・10B. L1197-L1200 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] J.Kushibiki,I.Takanaga,M.Arakawa,and T.Sannomiya: "Accurate Measurements of the Acoustical Physical Constants of LiNbO_3 and LiTaO_3 Single Crystals"IEEE Trans. UFFC. 46・5. 1315-1323 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 櫛引淳一,小野雄,高長和泉: "SAWデバイス用LiNbO_3, LiTaO_3単結晶の超音波マイクロスペクトロスコピー(招待論文)"I電子情報通信学会誌. J82-C-I・12. 715-727 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] J.Kushibiki,Y.Ohashi,and M.Arakawa: "Influence of Reflected Waves from the Back Surface of Thin Solid-Plate Specimen on Velocity Measurements by Line-Focus-Beam Acoustic Microscopy"IEEE Trans. UFFC. 47・1. 274-284 (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] J.Kushibiki,T.C.Wei,Y.Ohashi,and A.Tada: "Ultrasonic Micro-Spectroscopy Characterization of Silica Glass"J. Appl. Phys.. in press. (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] Y.Ono and J.Kushibiki: "Experimental Study of Construction Mechanism of V(z) Curves Obtained by Line-Focus-Beam Acoustic Microscopy"IEEE Trans. UFFC. in press. (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] J.Kushibiki,Y.Ohashi,and Y.Ono: "Evaluation of LiNbO_3 and LiTaO_3 Substrates for SAW Devices by the LFB Ultrasonic Material Characterization System"IEEE Trans. UFFC. in press. (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] J.Kushibiki and M.Arakawa: "A Method for Calibrating the Line-Focus-Beam Acoustic Microscopy System" IEEE Trans.UFFC. 45・2. 421-430 (1998)

    • Related Report
      1998 Annual Research Report
  • [Publications] J.Kushibiki,Y.Ohashi and M.Arakawa: "Precise Velocity Measurement for Thin Specimens by Line-focus-Beam Acoustic Microscopy" Jpn.J.Appl.Phys.38・1A/B. L89-L91 (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] J.Kushibiki and Y.Ohashi: "Theoretical and Experimental Considerations on Line-focus-Beam Acoustic Microscopy for Thin Specimens" Jpn.J.Appl.Phys.(in press). (1999)

    • Related Report
      1998 Annual Research Report
  • [Publications] A.Tourlog, J.D.Achenbach, and J.Kushibiki: "Line-focus acoustic microscopy measurements of acoustic properties of LiTaO_3 crystal plates with an inversion layer" J.Appl.Phys.81・10. 6616-6621 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] J.Kushibiki and I.Takanaga: "Elastic properties of single-and multi-domain crystals of LiTaO_3" J.Appl.Phys. 81・10. 6906-6910 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] J.Kushibiki and M.Miyashita: "Characterization of Domain-Inverted Layers in LiTaO_3 Line-Focus-Beam Acoustic Microscopy" Jpn.J.Appl.Phys.Part2Letters. 36・7B. 959-961 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] J.Kushibiki and M.Arakawa: "Characterization of Domain-Inverted Layers in LiTaO_3 Line-Focus-Beam Acoustic Microscopy" Jpn.J.Appl.Phys.Part2Letters. 45・2 (in press). (1998)

    • Related Report
      1997 Annual Research Report

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Published: 1997-04-01   Modified: 2016-04-21  

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