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Process Development for the Orientation Control of the(α_2+γ)Lamellar Microstructure in TiAl Intermetallic Compounds

Research Project

Project/Area Number 09450259
Research Category

Grant-in-Aid for Scientific Research (B).

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionYokohama National University

Principal Investigator

FUKUTOMI Hiroshi  Yokohama National University, Faculty of Engineering, Professor, 工学部, 教授 (90142265)

Project Period (FY) 1997 – 2000
Project Status Completed (Fiscal Year 2000)
Budget Amount *help
¥13,700,000 (Direct Cost: ¥13,700,000)
Fiscal Year 2000: ¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 1999: ¥1,600,000 (Direct Cost: ¥1,600,000)
Fiscal Year 1998: ¥4,600,000 (Direct Cost: ¥4,600,000)
Fiscal Year 1997: ¥6,900,000 (Direct Cost: ¥6,900,000)
Keywordslamellar microstructure / TiAl intermetallic compounds / texture / orientation control / reactive diffusion / 拡散反応 / 結晶集合組織 / 積層材料 / 反応焼結 / α単相領域 / Ti-46mol%Al
Research Abstract

Two basic processes designed for controlling the orientaion of lamellar microstructure of with the constituents of α_2+γ phases in the TiAl based alloys are theoreticall and experimentally examined. The first process consists of the high-temperature deformation in α single phase region followed by the annealing and deformation in α_2+γ region. The uniaxial compression in the α single phase region resulted in the formation of a fiber texture, though dynamic recrystallization occurred. The maximum pole density for the compression plane appeared about 35 degrees away from(0001)of α_2 phase. The heat treatment generates the lamellar microstructure reflecting the texture formed by the uniaxial deformation in the α single phase region. Work softening was observed at the deformation of the specimen with fully lamellar microstructure formed by the deformation in the α single phase region and the annealing in the two phase region. The deformation in the two phase region brought about the rotation of the lamellae. The lamellar interface lied almost parallel to the compression plane after the deformation of about-0.8 in true strain.
The second process is designed on the basis of the reactive diffusion between the textured titanium foils and aluminum foils. Thermal process consists of four heating stages and a cooling stage for lamellar construction. The phases are examined after the heat treatments by EDX.It was found that 40-60% of the orientations of the lamellae are dominated by the texture of the starting titanium foils. It was concluded that the combination of the reactive diffution process and the thermomechanical treatment described above is promising for the manufacturing process of TiAl sheet materials with the oriented lamellar microstructure.

Report

(5 results)
  • 2000 Annual Research Report   Final Research Report Summary
  • 1999 Annual Research Report
  • 1998 Annual Research Report
  • 1997 Annual Research Report
  • Research Products

    (25 results)

All Other

All Publications (25 results)

  • [Publications] 野本明義、福富洋志: "高温二段階加工による金属間化合物TiAlにおけるa_2+γラメラ組織の配向制御"日本金属学会誌. 61. 378-384 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H. Fukutomi, K. Nonomura, et. al.: "Effect of stress Change on the Behavior of Grain Boundary Sliding of Aluminium Bicrystals"Materials Science Forum. 233. 399-404 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H. Fukutomi and T. Yamamoto: "Grain Boundary Slide Hardening in Aluminium Bicrystals Examined by Stress Change Test"Proceedings of Intrenational Seminar on Microstructure, Micromechanics and Processing of Superplastic Materials. 31-37 (1997)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H. Fukutomi, T. Yamamoto, K. Nonomura and K. Tkada: "Examination of Dislocation Mechanism on Grain Boundary Sliding in High Angle Grain Boundaries by Stress Change Test"Interface Science. 7. 141-146 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H. Fukutomi, M. Ueno, M. Nakamura, T. Suzuki and S. Kikuchi: "Production of TiAl Sheet with Oriented Lamellar Microstructure by Diffusional Reaction of Aluminium and Textured Titanium Foils"Mat. Trans. JIM. 40. 654-658 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T. Suzuki, H. Fukutomi, Y. Tomota and T. Tsujimoto: "Formation Process of Oriented Lmellar Colonies in a TiAlMn Alloy Produced by Reactive Sintering Method"Mat. Trans. JIM. 40. 1032-1037 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H. Fukutomi, M. Ueno, M. Nakamura, T. Suzuki and S. Kikuchi: "Formation of Oriented Lamellae in TiAl Alloys by Diffusional Reaction"Proceedings of ICOTOM12. 1190-1195 (1999)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H. Fukutomi, M. Nakamura, et. al: "Void Formation during the Production of TiAl Intermetallic Compound by Reactive Diffusion of Titanium and Alminum Foils"Mat. Trans. JIM.. 41. 1244-1246 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] 福富洋志、長谷川誠、山本光宏: "純ニッケルにおける動的再結晶下での集合組織形成"日本金属学会誌. 65・2. 71-77 (2001)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Fukutomi and T.Yamamoto: "Grain Boundary Slide Hardening in Aluminium Bicrystals Examined by Stress Change Test"Proceedings of International Seminar on Microstructure, Micromechanics and Processing of Superplastic Material. 31-36 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] A.Nomoto and H.Fukutomi: "Orientation Control of(α_2+γ)Lamellae in TiAl Intermetallic compounds by Two-Step Compression at High Temperature"J.Japan Inst.Metals. 61. 378-384 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Fukutomi, K.Nonomura, Y.Takada and T.Yamamoto: "Effect of Stress Change on the Behavior of Grain Boundary Sliding of Aluminium Bicrystals of Grain Boundary Sliding of Aluminium Bicrystals"Materials Science Forum. 233. 399-404 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Fukutomi, T.Yamamoto, K.Nonomura and K.Takada: "Examination of Dislocation Mechanism on Grain Boundary Sliding in High Angle Grain Boundaries by Stress Change Test"Interface Science. 7. 141-146 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Fukutomi, M.Ueno, M.Nakamura, T.Suzuki and S.Kikuchi: "Production of TiAl Sheet with Oriented Lamellar Microstructure by Diffusional Reaction of Aluminum and Textured Titanium Foils"Mat.Trans.JIM. 40. 654-658 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] T.Suzuki, H.Fukutomi, Y.Tomota and T.Tsujimoto: "Formation Process of Oriented Lamellar Colonies in a TiAlMn Alloy Produced by Reactive Sintering Method"Mat.Trans.JIM. 40. 1032-1037 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Fukutomi, M.Ueno, M.Nakamura, T.Suzuki and S.Kikuchi: "Formation of Oriented Lamellae in TiAl Alloys by Diffusional Reaction"Proceedings of ICOTOM. 12. 1190-1195 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Fukutomi, M.Nakamura, T.Suzuki, S.Takagi and S.Kikuchi: "Void Formation during the Production of TiAl Intermetallic Compound by Reactive Diffusion of Titanium and Aluminum Foils"Mat.Trans.JIM. 41. 1244-1246 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Fukutomi, M.Hasegawa and M.Yamamoto: "Texture Formation during the Dynamic Recrystallization of Pure Nickel"J.Japan Inst.Metals. 65. 71-77 (2001)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2000 Final Research Report Summary
  • [Publications] H.Fukutomi,M.Nakamura, et. al: "Void Formation during the Production of TiAl Intermetallic Compound by Reactive Diffusion of Titanium and Aluminum Foils"Mat.Trans.JIM.. 41. 1244-1246 (2000)

    • Related Report
      2000 Annual Research Report
  • [Publications] 福富洋志,長谷川誠,山本光宏: "純ニッケルにおける動的再結晶下での集合組織形成"日本金属学会誌. 65・2. 71-77 (2001)

    • Related Report
      2000 Annual Research Report
  • [Publications] H.Fukutomi,M.Ueno等: "Formation of Oriented Lamellae in TiAl Alloys by Diffusional Reaction"Proceedings of ICOTOM 12. 1190-1195 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] T.Suzuki,H.Fukutomi等: "Formation Process of Oriented Lamellar Colonies in a TiAlMn Alloy Produced by Reactive Sintering Method"Mat.Trans. JIM. 40. 1032-1037 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] H.Fukutomi,M.Ueno等: "Production of TiAl Sheet with Oriented Lamellar Microstructure by Diffusional Reaction of Aluminum and Textured Titanium Foils"Mat.Trans. JIM. 40. 654-658 (1999)

    • Related Report
      1999 Annual Research Report
  • [Publications] 野本明義、福富洋志: "高温二段階加工による金属間化合物TiAlにおけるα_2+γラメラ組織の配向制御" 日本金属学会誌. 61. 378-384 (1997)

    • Related Report
      1997 Annual Research Report
  • [Publications] H.Fukutomi, K.Nonomura, et.al.: "Effect of Stress Change on the Behavior of Grain Boundary Sliding of Aluminium Bicrystals" Materials Science Forum. 233. 399-404 (1997)

    • Related Report
      1997 Annual Research Report

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Published: 1997-04-01   Modified: 2016-04-21  

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