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X-Ray Emission Spectroscopic Analysis using Electric Charging and Discharging

Research Project

Project/Area Number 09450309
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field 工業分析化学
Research InstitutionKYOTO UNIVERSITY

Principal Investigator

KAWAI Jun  Kyoto University, Associate Professor, 工学研究科, 助教授 (60191996)

Co-Investigator(Kenkyū-buntansha) HAYASHI Kouichi  Kyoto University, Research Associate, 工学研究科, 助手 (20283632)
TANABE Teruo  Kyoto University, Research Associate, 工学研究科, 助手 (90026237)
ASAKI Zenjiro  Kyoto University, Professor Emeritus, 顧問 (90026005)
Project Period (FY) 1997 – 1999
Project Status Completed (Fiscal Year 1999)
Budget Amount *help
¥11,800,000 (Direct Cost: ¥11,800,000)
Fiscal Year 1999: ¥2,800,000 (Direct Cost: ¥2,800,000)
Fiscal Year 1998: ¥4,000,000 (Direct Cost: ¥4,000,000)
Fiscal Year 1997: ¥5,000,000 (Direct Cost: ¥5,000,000)
KeywordsIndustrial Chemical Analysis / Novel Phenomena / X-Ray Analysis / Elemental Analysis
Research Abstract

X-Ray Emission due to electrification of insulator has been confirmed experimentally. The experimental conditions of X-ray emission due to the electric charge-up effect have been extensively studied with the change of pressure, vacuum, insulator material, atmospheric gas, applied voltage, electric current (DC or AC), and so on. It is found that the X-rays are only strongly emitted when the vacuum is a very narrow range on the 10ィイD1-2ィエD1 Torr. The X-ray emission is very unstable even though we changed the experimental conditions as far as we could control. The physical mechanism of this X-ray emission has been clarified; it is due to electron bombardment.
Using this phenomena, we have constructed an X-ray generating device using a 1.5 V battery and high voltage inverter. This device is quite small, and it has been observed that significant strength of X-rays were generated. The X-rays produced by this device was again very unstable, and we tried to find a condition by which the stable X-rays were generated. However, at the present stage of our work, we have not yet found such an experimental condition. We believe that the study of charge-up effect should be needed in the future.

Report

(4 results)
  • 1999 Annual Research Report   Final Research Report Summary
  • 1998 Annual Research Report
  • 1997 Annual Research Report
  • Research Products

    (6 results)

All Other

All Publications (6 results)

  • [Publications] 河合潤 他: "帯電によるX線の発生"X線分析の進歩. 29. 203-222 (1998)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 河合潤: "はかってなんぼ X線分析"丸善. 119-128 (2000)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J. Kawai, S. Inada, K. Maeda: "X-Ray Emission due to Charge-up"Adv. X-Ray Chem. Anal. Japan. Vol.29. 203-222 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] J. Kawai: Maruzen, Tokyo. J. Kawai and T. Hinoue(Eds.). 119-128 (2000)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1999 Final Research Report Summary
  • [Publications] 河合潤: "第11章X線分析 「はかってなんぼ-分析化学入門-」"丸善. 10 (2000)

    • Related Report
      1999 Annual Research Report
  • [Publications] 河合潤, 稲田伸哉, 前田邦子: "帯電によるX線の発生" X線分析の進歩. 29. 203-222 (1998)

    • Related Report
      1997 Annual Research Report

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Published: 1997-04-01   Modified: 2016-04-21  

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